CN206063823U - The distilling apparatus of low-boiling point material in a kind of separating mixture - Google Patents
The distilling apparatus of low-boiling point material in a kind of separating mixture Download PDFInfo
- Publication number
- CN206063823U CN206063823U CN201620934364.1U CN201620934364U CN206063823U CN 206063823 U CN206063823 U CN 206063823U CN 201620934364 U CN201620934364 U CN 201620934364U CN 206063823 U CN206063823 U CN 206063823U
- Authority
- CN
- China
- Prior art keywords
- outlet
- tank
- monomer recovery
- recovery tank
- liquid collecting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
This utility model is related to technical field of chemical, and in particular to a kind of distilling apparatus.The distilling apparatus of low-boiling point material in a kind of separating mixture, including MONOMER RECOVERY tank, the top inlet of MONOMER RECOVERY tank is connected with the outlet of reactor, the top exit of MONOMER RECOVERY tank is connected with condenser, the outlet at bottom of condenser is connected with the import of layering tank, layering tank is connected with the first liquid collecting tank and the second liquid collecting tank respectively, and the outlet of the first liquid collecting tank is connected with the reaction monomers import of reactor, and the outlet of the second liquid collecting tank is connected with wastewater treatment equipment.The outlet at bottom of MONOMER RECOVERY tank is connected with the entrance of filter, and the wet mash outlet of filter is connected with the import of drying machine, and the outlet of drying machine obtains product；The mother liquor outlet of filter is connected with disposing mother liquor tank.Due to adopting above-mentioned technical proposal, this utility model solves the separation problem of low-boiling point material in mixture, such as after polyreaction, excessive lower boiling monomer in recovery mixture.
Description
Technical field
This utility model is related to technical field of chemical, and in particular to a kind of distilling apparatus.
Background technology
In Chemical Manufacture, such as polymerization reaction engineering, in order to promote to react carry out complete, often makes a certain in reaction
Monomer excess.Therefore target product will be obtained, must be except reaction monomers excessive in mixture after dereaction.
Utility model content
The purpose of this utility model is, there is provided the distilling apparatus of low-boiling point material in a kind of separating mixture, solve with
Upper technical problem.
The technical problem solved by this utility model can employ the following technical solutions to realize：
The distilling apparatus of low-boiling point material in a kind of separating mixture, including MONOMER RECOVERY tank, the MONOMER RECOVERY tank
Top inlet is connected with the outlet of reactor, and the top exit of the MONOMER RECOVERY tank is connected with condenser, and the condenser sets
The outlet at bottom for having cooling water inlet and coolant outlet, the condenser is connected with the import of layering tank, the layering tank
Organic outlet is connected with the first liquid collecting tank, and the wastewater outlet of the layering tank is connected with the import of the second liquid collecting tank, and described the
The outlet of one liquid collecting tank is connected with the reaction monomers import of the reactor, and outlet and the wastewater treatment of second liquid collecting tank are filled
Put connected；
The outlet at bottom of MONOMER RECOVERY tank is connected with the entrance of filter, and the wet mash of the filter is exported and done
The import of dry machine is connected, and the outlet of the drying machine obtains product；The mother liquor outlet of the filter is connected with disposing mother liquor tank；
The bottom of the MONOMER RECOVERY tank is provided with steam distributor, and the steam distributor connection is positioned at the MONOMER RECOVERY
Steam pipework outside tank.
During utility model works, the slurry that reactor outlet is flowed out is flowed in MONOMER RECOVERY tank, and steam is in the lump in list
Carry out oil and gas to distill in body recycling can jointly, during distillation, organic monomer steam and water vapour are in the lump by going out at the top of MONOMER RECOVERY tank
Mouth is steamed, and is condensed in condenser, is condensed the mixing lime set for obtaining and is layered in quantizer.It is molten in layering tank
Liquid obtains organic layer and water layer after being layered, wherein organic layer enters the first liquid collecting tank, and water layer enters the second liquid collecting tank.Flow through
Reclaim after first liquid collecting tank and obtain excessive reaction monomers and re-used into reactor.Obtain after flowing through the second liquid collecting tank
Waste water processed through wastewater treatment equipment.The product solution of MONOMER RECOVERY pot bottom abjection is flowed out from outlet at bottom, Jing
The wet mash being filtrated to get of filter after drying machine drying obtains product, and the mother solution for filtering out is returned by mother solution
Closed cans carries out recycling.Using after above-mentioned design, in energy effectively solving mixture, low-boiling point material divides this utility model
From problem, such as after polyreaction, excessive lower boiling monomer in recovery mixture.With reaction mass is saved, energy consumption is reduced,
The advantage of environmental protection.
Agitator is provided with the MONOMER RECOVERY tank, the axial direction of the agitator is vertical, and the agitator connection is located at
Motor outside the MONOMER RECOVERY tank.In order to when oil and gas are distilled jointly, uniform stirring is realized preferably separating.
The MONOMER RECOVERY tank is provided with the temperature sensor of temperature in the sensing MONOMER RECOVERY tank, the temperature sensing
Device connects temperature control instrument；
The steam pipework is provided with control valve, the signal output part connection control valve of the temperature control instrument
Control end.This utility model is adjusted inlet steam flow and then controls the temperature of MONOMER RECOVERY tank by adjusting control valve.
The steam distributor is pipeline structure, is provided with least two steam in the horizontal direction and goes out on the steam distributor
QI KOU, the steam gas outlet is upward.
Beneficial effect：Due to adopting above-mentioned technical proposal, this utility model to solve the separation of low-boiling point material in mixture
After problem, such as polyreaction, excessive lower boiling monomer in recovery mixture.This utility model has saves reaction mass,
Reduce energy consumption, the advantage of environmental protection.
Description of the drawings
Fig. 1 is a kind of overall structure diagram of the present utility model.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that this utility model is realized are easy to understand, under
Face combines to be specifically illustrating and this utility model is expanded on further.
With reference to Fig. 1, the distilling apparatus of low-boiling point material in a kind of separating mixture, including MONOMER RECOVERY tank 1, MONOMER RECOVERY
The top inlet of tank 1 is connected with the outlet of reactor 10, is provided with agitator 2 in MONOMER RECOVERY tank 1, and the axial direction of agitator 2 is perpendicular
To motor of the connection of agitator 2 outside MONOMER RECOVERY tank 1.The bottom of MONOMER RECOVERY tank 1 is provided with steam distributor 3, steam
Steam pipework of the connection of distributor 3 outside MONOMER RECOVERY tank 1, steam pipework are provided with control valve 11.Steam distributor 3 is
Pipeline structure, is provided with several steam gas outlets in the horizontal direction on steam distributor 3, steam gas outlet is upward.Monomer is returned
Closed cans 1 is provided with the temperature sensor of temperature in sensing MONOMER RECOVERY tank 1, temperature sensor connection temperature control instrument 12.Temperature
The control end of the signal output part connection control valve 11 of degree control instrument 12.
The outlet at bottom of MONOMER RECOVERY tank 1 is connected with the entrance of filter 4, wet mash outlet and the drying machine 5 of filter 4
Import be connected, the outlet of drying machine 5 obtains product.The mother liquor outlet of filter 4 is connected with disposing mother liquor tank 13.
The top exit of MONOMER RECOVERY tank 1 is connected with condenser 6, and condenser 6 is provided with cooling water inlet 62 and cooling water goes out
Mouth 61, the outlet at bottom of condenser 6 are connected with the import of layering tank 7, are layered the organic outlet and 8 phase of the first liquid collecting tank of tank 7
Even, the wastewater outlet for being layered tank 7 is connected with the import of the second liquid collecting tank 9, the outlet of the first liquid collecting tank 8 and the reaction of reactor 10
Monomer import is connected, and the outlet of the second liquid collecting tank 9 is connected with wastewater treatment equipment.
During utility model works, the slurry that the outlet of reactor 10 is flowed out is flowed in MONOMER RECOVERY tank 1, and steam exists in the lump
Carry out oil and gas to distill in MONOMER RECOVERY tank 1 jointly, MONOMER RECOVERY tank 1 is provided with temperature control instrument 12, by adjusting control valve 11
Come the temperature for adjusting inlet steam flow and then controlling MONOMER RECOVERY tank 1.During distillation, organic monomer steam and water vapour in the lump by
The top exit of MONOMER RECOVERY tank 1 is steamed, and is condensed in condenser 6, is condensed the mixing lime set for obtaining and is entered quantizer
In be layered.In layering tank 7, solution obtains organic layer and water layer after being layered, and wherein organic layer enters the first liquid collecting tank 8,
Water layer enters the second liquid collecting tank 9.Recovery after flowing through the first liquid collecting tank 8 obtains excessive reaction monomers and obtains weight into reactor 10
It is new to utilize.The waste water obtained after flowing through the second liquid collecting tank 9 is processed through wastewater treatment equipment.1 bottom of MONOMER RECOVERY tank takes off
The product solution for going out from outlet at bottom flow out, through filter 4 the wet mash being filtrated to get by drying machine 5 be dried after, obtain
Product, and the mother solution for filtering out carries out recycling by disposing mother liquor tank 13.After this utility model adopts above-mentioned design,
The separation problem of low-boiling point material in energy effectively solving mixture, such as after polyreaction, excessive low boiling in recovery mixture
Monomer.With reaction mass is saved, energy consumption, the advantage of environmental protection are reduced.
Ultimate principle of the present utility model and principal character and advantage of the present utility model has been shown and described above.One's own profession
The technical staff of industry it should be appreciated that this utility model is not restricted to the described embodiments, described in above-described embodiment and description
Simply illustrate principle of the present utility model, on the premise of without departing from this utility model spirit and scope, this utility model is also
Various changes and modifications are had, these changes and improvements are both fallen within the range of claimed this utility model.This utility model
Claimed scope is by appending claims and its equivalent thereof.
Claims (4)
1. in a kind of separating mixture low-boiling point material distilling apparatus, including MONOMER RECOVERY tank, it is characterised in that the monomer
The top inlet of recycling can is connected with the outlet of reactor, and the top exit of the MONOMER RECOVERY tank is connected with condenser, described
Condenser is provided with cooling water inlet and coolant outlet, and the outlet at bottom of the condenser is connected with the import of layering tank, described
The organic outlet of layering tank is connected with the import of the first liquid collecting tank, described to be layered the wastewater outlet of tank and entering for the second liquid collecting tank
Mouthful it is connected, the outlet of first liquid collecting tank is connected with the reaction monomers import of the reactor, and second liquid collecting tank goes out
Mouth is connected with wastewater treatment equipment；
The outlet at bottom of MONOMER RECOVERY tank is connected with the entrance of filter, and the wet mash of the filter is exported and drying machine
Import be connected, the outlet of the drying machine obtains product；The mother liquor outlet of the filter is connected with disposing mother liquor tank；
The bottom of the MONOMER RECOVERY tank is provided with steam distributor, and the steam distributor connection is outside the MONOMER RECOVERY tank
The steam pipework in portion.
2. in a kind of separating mixture according to claim 1 low-boiling point material distilling apparatus, it is characterised in that it is described
Agitator is provided with MONOMER RECOVERY tank, the axial direction of the agitator is vertical, and the agitator connection is positioned at the MONOMER RECOVERY
Motor outside tank.
3. in a kind of separating mixture according to claim 1 low-boiling point material distilling apparatus, it is characterised in that it is described
MONOMER RECOVERY tank is provided with the temperature sensor of temperature in the sensing MONOMER RECOVERY tank, and the temperature sensor connects temperature control
Instrument processed；
The steam pipework is provided with control valve, the control of the signal output part connection control valve of the temperature control instrument
End.
4. in a kind of separating mixture according to claim 1 low-boiling point material distilling apparatus, it is characterised in that it is described
Steam distributor is pipeline structure, is provided with least two steam gas outlets, the steaming on the steam distributor in the horizontal direction
Vapour gas outlet is upward.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620934364.1U CN206063823U (en) | 2016-08-24 | 2016-08-24 | The distilling apparatus of low-boiling point material in a kind of separating mixture |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620934364.1U CN206063823U (en) | 2016-08-24 | 2016-08-24 | The distilling apparatus of low-boiling point material in a kind of separating mixture |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206063823U true CN206063823U (en) | 2017-04-05 |
Family
ID=58431488
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620934364.1U Active CN206063823U (en) | 2016-08-24 | 2016-08-24 | The distilling apparatus of low-boiling point material in a kind of separating mixture |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206063823U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109293121A (en) * | 2018-12-05 | 2019-02-01 | 孟召阳 | A kind of chemical waste liquid processing reforming unit |
| CN111135782A (en) * | 2019-10-31 | 2020-05-12 | 荆门金贤达生物科技有限公司 | Synthetic reaction system for producing etoxazole |
-
2016
- 2016-08-24 CN CN201620934364.1U patent/CN206063823U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109293121A (en) * | 2018-12-05 | 2019-02-01 | 孟召阳 | A kind of chemical waste liquid processing reforming unit |
| CN111135782A (en) * | 2019-10-31 | 2020-05-12 | 荆门金贤达生物科技有限公司 | Synthetic reaction system for producing etoxazole |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206063823U (en) | The distilling apparatus of low-boiling point material in a kind of separating mixture | |
| CN105175730A (en) | Method for preparing silicone rubber from organosilicon hydrolysate | |
| CN202376983U (en) | Multifunctional reactor for preparing hexene-1 catalyst | |
| CN206127267U (en) | Distillation plant of making wine usefulness | |
| CN108558629A (en) | A kind of production system and production method of refined cyclohexanone | |
| CN107721890A (en) | Reactive distillation produces the method and its process units of isooctyl thioglycolate | |
| CN207418323U (en) | A kind of split type condensing unit | |
| CN203359986U (en) | Sulfur purifying device | |
| CN209501687U (en) | A kind of double-layer glass reaction kettle collection device | |
| CN209010425U (en) | A kind of tetrahydrofuran reaction separating device | |
| CN208182895U (en) | A kind of tetrahydrofuran fractional order reaction separator | |
| CN107501126B (en) | The method and system of high efficiente callback acrylonitrile in a kind of production of high-performance carbon fibre | |
| CN202322584U (en) | Hydrothermal flash evaporation device capable of realizing afterheat recovery | |
| CN109821265A (en) | A kind of thick raffinate rectifier unit of caprolactam and technique | |
| CN105713113B (en) | Method for recovering heat of gas-phase material in condensation kettle | |
| CN107235823A (en) | The recovery process for refining and its equipment of a kind of carbide VCM high-boiling components | |
| CN210646351U (en) | Multifunctional automatic reaction control system | |
| CN203558989U (en) | Extraction system for polyoxymethylene dimethyl ether preparation device | |
| CN102849770A (en) | Method for synthesizing anhydrous aluminum chloride by recycling aluminum chloride hexahydrate | |
| CN208898766U (en) | A kind of epoxide resin reactive diluent methylbenzene recycling system | |
| CN103450376B (en) | A kind of for the synthesis of the distil process in production of resins process | |
| CN207645990U (en) | The device of extraction saturation saline solution in a kind of industrial wastewater | |
| CN103588734B (en) | Recovery method and recovery device of butyl ester and acetone in ketene dimer production | |
| CN207169081U (en) | A kind of chemical industry rectifier unit | |
| CN207126157U (en) | A kind of wire mesh packing rectifying tower |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |