CN204364916U - A kind of distilling apparatus - Google Patents
A kind of distilling apparatus Download PDFInfo
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- CN204364916U CN204364916U CN201520009196.0U CN201520009196U CN204364916U CN 204364916 U CN204364916 U CN 204364916U CN 201520009196 U CN201520009196 U CN 201520009196U CN 204364916 U CN204364916 U CN 204364916U
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- protective cover
- condenser pipe
- head
- temperature
- oil bath
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Abstract
The utility model discloses a kind of distilling apparatus, belong to chemical apparatuses field.A kind of distilling apparatus of the present utility model, comprise evaporation device, rotating mechanism, supporting mechanism and collecting mechanism, evaporation device comprises high-temperature water oil bath pan and protective cover, rotating mechanism comprises revolving bottle, glass axle, put removing nut, elevated-temperature seal ring, head, low temperature seal ring and locking nut, supporting mechanism comprises base and cabinet, collecting mechanism comprises condenser pipe, bottleneck card and receiving flask, the head inside of rotating mechanism is equipped with glass axle, head side is successively by glass axle, be enclosed within elevated-temperature seal ring on glass axle and put removing nut and be connected with revolving bottle, revolving bottle is by rotating hole with matching on protective cover in evaporation device, body is placed in the high-temperature water oil bath pan of evaporation device, head is by being arranged in the electric rotating machine of supporting mechanism, rotate in high-temperature water oil bath pan when revolving bottle is heated, increase heating surface area, Reaction time shorten.
Description
Technical field
The utility model relates to chemical apparatuses field, particularly relates to a kind of distilling apparatus.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, and be widely used in the fields such as oil refining, chemical industry, light industry, its principle is to be separated bi-component mixed liquor.Feed liquid heating is made its components vaporize, volatile components obtains enrichment in steam, difficult volatile component also obtains enrichment in raffinate, this achieve to a certain extent two components separation it utilize each component boiling point in mixing material or liquid-solid system different, low boiling component is evaporated, condensation is to be separated the unit process of whole component again, is the associating of evaporation and condensation two kinds of unit operations.With other separation means, as extraction, filtering for crystallizing etc. are compared, its advantage is not need to use other solvent beyond system components, thus ensures to introduce new impurity.
Find through patent retrieval, have related art scheme about distilling apparatus open.As: Chinese Patent Application No.: 201320131809.9, the applying date: on 03 21st, 2013, invention and created name was: distillation apparatus, and this application case comprises cucurbit, condensing bulb, Backflow bottle; Also comprise the heater corresponding with cucurbit, the condenser system corresponding with condensing bulb, control device, housing; Described condensing bulb is provided with retort gas entrance, distillating liquid outlet, condensate inlet, condensate outlet; It is characterized in that: described cucurbit is provided with three bottlenecks, be designated as the first bottleneck, the second bottleneck, the 3rd bottleneck respectively; Cucurbit is connected with the retort gas entrance of described condensing bulb by described first bottleneck; Cucurbit is communicated with nitrogen blowing apparatus by described second bottleneck; Cucurbit is communicated with sample adding device and anti-suck feeder by described 3rd bottleneck.This distillation apparatus can not occur not easily to produce bumping in suck-back, heating process after stopping heating, can avoid producing oxidation in measured matter heating process.This application case can carry out distillation procedure, but its distillation efficiency is low, and also need support by foreign object between each mechanism, also needs further improvement.
Utility model content
1. the utility model technical problem that will solve
The purpose of this utility model is to overcome the shortcoming of vaporising device function difference in prior art, provides the vaporising device of a kind of rotary heating and easily collecting.
2. technical scheme
For achieving the above object, the technical scheme that the utility model provides is:
A kind of distilling apparatus of the present utility model, comprises evaporation device, rotating mechanism, supporting mechanism and collecting mechanism, it is characterized in that:
Described evaporation device comprises high-temperature water oil bath pan and protective cover, this high-temperature water oil bath pan comprises temperature charactron and radiation heating resistances, described protective cover comprises spray head and rotating hole, this spray head is positioned at the inwall top of protective cover, be provided with mozzle in above-mentioned protective cover the conduction oil in high-temperature water oil bath pan and the spray head in protective cover are connected, described high-temperature water oil bath pan arranged outside has pump, and above-mentioned temperature charactron, radiation heating resistances and pump are electrically connected by wire;
Described rotating mechanism comprises revolving bottle, glass axle, puts removing nut, elevated-temperature seal ring, head, low temperature seal ring and locking nut, described revolving bottle matches with the rotating hole in protective cover in evaporation device, described head inside is equipped with glass axle, described head side successively by glass axle, be enclosed within elevated-temperature seal ring on glass axle and put removing nut and be connected with revolving bottle, described head opposite side is connected with collecting mechanism with locking nut by glass axle, the low temperature seal ring be enclosed within glass axle successively;
Described supporting mechanism comprises base and cabinet, described base is provided with cabinet, be connected with the head in rotating mechanism in the middle part of above-mentioned cabinet, described cabinet inside is provided with the electric rotating machine for driving revolving bottle to rotate, and described electric rotating machine is connected with power electric;
Described collecting mechanism comprises condenser pipe, bottleneck card and receiving flask, and described condenser pipe is connected to rotating mechanism and collecting mechanism by locking nut, and described condenser pipe lower end outlet is linked by bottleneck and is connected to receiving flask.
As further improvement of the present invention, the condenser pipe of collecting mechanism is snakelike scroll-type condenser pipe, condenser pipe cools outer field upper end and is provided with thermometer, temperature alarm and priming valve, this condenser pipe cools outer field lower end and is provided with delivery port, the outer field outer setting of cooling of described condenser pipe has heat-insulation layer, and above-mentioned thermometer and temperature alarm are electrically connected by wire.
As further improvement of the present invention, described protective cover is the hemispherical dome structure of high-boron-silicon glass material, and this protective cover is also provided with peep hole.
3, beneficial effect
Adopt technical scheme provided by the invention, compared with existing known technology, there is following remarkable result:
(1) a kind of distilling apparatus of the present utility model, comprise evaporation device, rotating mechanism, supporting mechanism and collecting mechanism, the head inside of rotating mechanism is equipped with glass axle, head side is successively by glass axle, be enclosed within elevated-temperature seal ring on glass axle and put removing nut and be connected with revolving bottle, revolving bottle is by rotating hole with matching on protective cover in evaporation device, body is placed in the high-temperature water oil bath pan of evaporation device, head is by being arranged in the electric rotating machine of supporting mechanism, rotate in high-temperature water oil bath pan when revolving bottle is heated, increase heating surface area, Reaction time shorten.
(2) a kind of distilling apparatus of the present utility model, in evaporation device, the inside of protective cover is provided with spray head, be provided with mozzle in protective cover the conduction oil in high-temperature water oil bath pan and the spray head in protective cover are connected, high-temperature water oil bath pan arranged outside has pump, during heating, by pump by the heating oil pump in high-temperature water oil bath pan to the spray head place of protective cover, by spray head, heating oil is sprayed on revolving bottle, increase heating surface area, shorten the evaporation reaction time.
(3) a kind of distilling apparatus of the present utility model, the condenser pipe of collecting mechanism is snakelike scroll-type condenser pipe, condenser pipe cools outer field upper end and is provided with thermometer, temperature alarm and priming valve, this condenser pipe cools outer field lower end and is provided with delivery port, the outer field outer setting of cooling of described condenser pipe has heat-insulation layer, above-mentioned thermometer and temperature alarm are electrically connected by wire, and such structural design makes the efficiency when condensation increase, and accelerate test efficiency.
(4) a kind of distilling apparatus of the present utility model, protective cover is the hemispherical dome structure of high-boron-silicon glass material, and this protective cover is also provided with peep hole, is convenient to observing response state and situation, collects test effect and content in time.
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of distilling apparatus of the present utility model;
Fig. 2 is the decomposing state structural representation of a kind of distilling apparatus of the present utility model.
Label declaration in schematic diagram:
11, high-temperature water oil bath pan; 12, temperature charactron; 13, radiation heating resistances; 21, protective cover; 22, spray head; 23, rotating hole; 24, peep hole; 30, revolving bottle; 31, glass axle; 32, removing nut is put; 33, elevated-temperature seal ring; 34, head; 35, low temperature seal ring; 36, locking nut; 41, base; 42, cabinet; 51, condenser pipe; 52, priming valve; 53, bottleneck card; 54, receiving flask.
Detailed description of the invention
For understanding content of the present utility model further, in conjunction with the accompanying drawings and embodiments the utility model is described in detail.
Embodiment 1
Composition graphs 1 and Fig. 2, a kind of distilling apparatus of the present embodiment, comprise evaporation device, rotating mechanism, supporting mechanism and collecting mechanism, evaporation device comprises high-temperature water oil bath pan 11 and protective cover 21, this high-temperature water oil bath pan 11 comprises temperature charactron 12 and radiation heating resistances 13, above-mentioned protective cover 21 comprises spray head 22 and rotating hole 23, this spray head 22 is positioned at the inwall top of protective cover 21, protective cover 21 is the hemispherical dome structure of high-boron-silicon glass material, this protective cover 21 is also provided with peep hole 24, also be provided with mozzle in this protective cover 21 spray head 22 in the conduction oil in high-temperature water oil bath pan 11 and protective cover 21 is connected, high-temperature water oil bath pan 11 arranged outside has pump, above-mentioned temperature charactron 12, radiation heating resistances 13 and pump are electrically connected by wire, after energising, heating oil in high-temperature water oil bath pan 11 is passed through water conservancy diversion tube pump to the spray head 22 in protective cover 21 by pump, by spray head 22, heating oil is sprayed the vessel surface of extremely required heating, increase heating surface (area) (HS, improve reaction efficiency, described rotating mechanism comprises revolving bottle 30, glass axle 31, puts removing nut 32, elevated-temperature seal ring 33, head 34, low temperature seal ring 35 and locking nut 36, described revolving bottle 30 matches with the rotating hole 23 in protective cover in evaporation device 21, head 34 inside is equipped with glass axle 31, head side successively by glass axle 31, be enclosed within elevated-temperature seal ring 33 on glass axle 31 and put removing nut 32 and be connected with revolving bottle 30, this head opposite side is connected with collecting mechanism with locking nut 36 by glass axle 31, the low temperature seal ring 35 be enclosed within glass axle 31 successively,
Supporting mechanism comprises base 41 and cabinet 42, base 42 is provided with cabinet 42, be connected with the head 34 in rotating mechanism in the middle part of cabinet 42, cabinet 42 inside is provided with the electric rotating machine for driving revolving bottle 30 to rotate, and this electric rotating machine is connected with power electric, after energising, electric rotating machine drives head 34 to rotate, linkage rotation bottle 30 rotates, and makes liquid to be distilled in revolving bottle 30 increase response area, Reaction time shorten;
Collecting mechanism comprises condenser pipe 51, bottleneck card 53 and receiving flask 54, condenser pipe 51 is connected to rotating mechanism and collecting mechanism by locking nut 36, the outlet of condenser 51 lower end is connected with receiving flask 54 by bottleneck card 53, this condenser pipe 51 is snakelike scroll-type condenser pipe, condenser pipe 51 cools outer field upper end and is provided with thermometer, temperature alarm and priming valve 52, this condenser pipe 51 cools outer field lower end and is provided with delivery port, the outer field outer setting of cooling of condenser pipe 51 has heat-insulation layer, above-mentioned thermometer and temperature alarm are electrically connected by wire, observe thermometer and temperature alarm, the outer field cooling fluid of cooling is changed in real time by priming valve 52, improve cooling effectiveness, shorten cool time, make whole still-process quickness and high efficiency.
During use, first priming valve in collecting mechanism 52 is opened, cooling fluid is added in condenser pipe 51, the delivery port of condenser pipe 51 lower end is clogged with stopper, then pour liquid to be distilled into revolving bottle 30, after whole supporting mechanism and collecting mechanism assembling, revolving bottle 30 is put into high-temperature water oil bath pan 11, pour heating oil into, cover protective cover 21, when starting to react, first open the electric rotating machine in supporting mechanism, electric rotating machine drives head 34 to rotate, linkage rotation bottle 30 rotates, open the temperature charactron 12 on high-temperature water oil bath pan 11 again, radiation heating resistances 13 and pump, heating oil in high-temperature water oil bath pan 11 is passed through water conservancy diversion tube pump to the spray head 22 in protective cover 21 by pump, by spray head 22, heating oil is sprayed to revolving bottle 30 upper surface, now evaporation device is started working, by peep hole 24 Real Time Observation heating state, gas after evaporation is because density diminishes and moves upward, come in the condenser pipe 51 of collecting mechanism, after condenser pipe 51 cools the cooling of the condensate liquid in skin, the liquid of distillation is made finally to be in receiving flask 54 by condenser 51 lower end, by observing condenser pipe 51 and cool the degree meter of outer upper end and temperature alarm can changing the outer field cooling fluid of cooling in real time.
Schematically above be described the utility model and embodiment thereof, this description does not have restricted, and also just one of the embodiment of the present utility model shown in accompanying drawing, actual structure is not limited thereto.So, if those of ordinary skill in the art enlightens by it, when not departing from the utility model and creating aim, design the frame mode similar to this technical scheme and embodiment without creationary, protection domain of the present utility model all should be belonged to.
Claims (3)
1. a distilling apparatus, comprises evaporation device, rotating mechanism, supporting mechanism and collecting mechanism, it is characterized in that:
Described evaporation device comprises high-temperature water oil bath pan (11) and protective cover (21), this high-temperature water oil bath pan (11) comprises temperature charactron (12) and radiation heating resistances (13), described protective cover (21) comprises spray head (22) and rotating hole (23), this spray head (22) is positioned at the inwall top of protective cover (21), be provided with mozzle in above-mentioned protective cover (21) spray head (22) in the conduction oil in high-temperature water oil bath pan (11) and protective cover (21) is connected, described high-temperature water oil bath pan (11) arranged outside has pump, above-mentioned temperature charactron (12), radiation heating resistances (13) and pump are electrically connected by wire,
Described rotating mechanism comprises revolving bottle (30), glass axle (31), put removing nut (32), elevated-temperature seal ring (33), head (34), low temperature seal ring (35) and locking nut (36), described revolving bottle (30) matches with the rotating hole (23) in protective cover in evaporation device (21), described head (34) inside is equipped with glass axle (31), described head side is successively by glass axle (31), be enclosed within elevated-temperature seal ring (33) on glass axle (31) and put removing nut (32) and be connected with revolving bottle (30), described head opposite side is successively by glass axle (31), the low temperature seal ring (35) be enclosed within glass axle (31) is connected with collecting mechanism with locking nut (36),
Described supporting mechanism comprises base (41) and cabinet (42), described base (41) is provided with cabinet (42), above-mentioned cabinet (42) middle part is connected with the head (34) in rotating mechanism, described cabinet (42) inside is provided with the electric rotating machine for driving revolving bottle (30) to rotate, and described electric rotating machine is connected with power electric;
Described collecting mechanism comprises condenser pipe (51), bottleneck card (53) and receiving flask (54), described condenser pipe (51) is connected to rotating mechanism and collecting mechanism by locking nut (36), and described condenser pipe (51) lower end outlet is connected with receiving flask (54) by bottleneck card (53).
2. a kind of distilling apparatus according to claim 1, it is characterized in that: the condenser pipe (51) of collecting mechanism is snakelike scroll-type condenser pipe, condenser pipe (51) cools outer field upper end and is provided with thermometer, temperature alarm and priming valve (52), this condenser pipe (51) cools outer field lower end and is provided with delivery port, the outer field outer setting of cooling of described condenser pipe (51) has heat-insulation layer, and above-mentioned thermometer and temperature alarm are electrically connected by wire.
3. a kind of distilling apparatus according to claim 1 and 2, is characterized in that: the hemispherical dome structure that described protective cover (21) is high-boron-silicon glass material, this protective cover (21) is also provided with peep hole (24).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520009196.0U CN204364916U (en) | 2015-01-07 | 2015-01-07 | A kind of distilling apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520009196.0U CN204364916U (en) | 2015-01-07 | 2015-01-07 | A kind of distilling apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204364916U true CN204364916U (en) | 2015-06-03 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520009196.0U Expired - Fee Related CN204364916U (en) | 2015-01-07 | 2015-01-07 | A kind of distilling apparatus |
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| Country | Link |
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| CN (1) | CN204364916U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106621432A (en) * | 2016-11-14 | 2017-05-10 | 东海县凯凯石英制品有限公司 | Quartz-based rotary evaporator |
| CN109731362A (en) * | 2018-12-29 | 2019-05-10 | 重庆医药高等专科学校 | The evaporation drying device of Paclitaxel liposome |
| CN111632396B (en) * | 2019-12-11 | 2021-03-02 | 东南大学 | Rotary evaporator gas transmission device based on management and control of Internet of things |
-
2015
- 2015-01-07 CN CN201520009196.0U patent/CN204364916U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106621432A (en) * | 2016-11-14 | 2017-05-10 | 东海县凯凯石英制品有限公司 | Quartz-based rotary evaporator |
| CN109731362A (en) * | 2018-12-29 | 2019-05-10 | 重庆医药高等专科学校 | The evaporation drying device of Paclitaxel liposome |
| CN109731362B (en) * | 2018-12-29 | 2021-03-23 | 重庆医药高等专科学校 | Evaporation drying device for paclitaxel liposome |
| CN111632396B (en) * | 2019-12-11 | 2021-03-02 | 东南大学 | Rotary evaporator gas transmission device based on management and control of Internet of things |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150603 Termination date: 20160107 |