CN207307857U - A kind of pilot scale glass reaction kettle for room temperature synthesis high molecular material - Google Patents
A kind of pilot scale glass reaction kettle for room temperature synthesis high molecular material Download PDFInfo
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- CN207307857U CN207307857U CN201721259958.8U CN201721259958U CN207307857U CN 207307857 U CN207307857 U CN 207307857U CN 201721259958 U CN201721259958 U CN 201721259958U CN 207307857 U CN207307857 U CN 207307857U
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- reaction kettle
- glass reaction
- rabble
- double
- high molecular
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Abstract
The utility model discloses a kind of pilot scale glass reaction kettle for room temperature synthesis high molecular material, including supporting rack, variable-frequency motor and double-layer glass reaction kettle, variable-frequency motor is connected with rabble by universal joint in the vertical direction, rabble is stretched into double-layer glass reaction kettle, hollow double-layer glass reaction kettle is installed between upper press cover and lower cover, rabble is equipped with ribbon spiral shape blade, is connected between ribbon spiral shape blade and rabble by strut, rabble bottom is equipped with agitating paddle.The middle part of rabble sets ribbon spiral shape blade, bottom is equipped with agitating paddle, ribbon spiral shape blade can be such that reaction solution flows in vertical direction, coordinate with rabble, so that material mixing is evenly, the initiator being added dropwise can efficiently be disperseed, prevent that material local concentration is excessive, rabble and ribbon spiral shape blade, increase the dynamics of stirring and the space of stirring, for the high liquid material of concentration, it can accomplish that whole material upper strata and bottom all stir evenly.
Description
Technical field
It the utility model is related to chemical reaction kettle technical field, and in particular to a kind of to synthesize high molecular material for room temperature
Pilot scale glass reaction kettle.
Background technology
With the fast development of high molecular material industry, the requirement in experimentation to chemical reaction kettle is also higher and higher,
Need, by the structure design and parameter configuration to container, to realize the mixture of the heating of technological requirement, evaporation, cooling and low high speed
Function.Currently used high molecular material working condition is relatively general more harsh, if in polymerization process, monomer polymerization is endless
Entirely, environmentally friendly hidden danger is not only had, but also the performance of final products can be influenced.
In newest room temperature synthesis technique, since the excessive concentration of sintetics, viscosity are larger, the stirring of glass kettle upper strata
Dynamics is inadequate, and stirring is insufficient, and material mixing is uneven, and material, which is added dropwise, can only drop down on high concentration liquid upper strata, causes local anti-
Should be uneven, influence synthetic effect.
Utility model content
The purpose of this utility model is that to solve the above-mentioned problems and provides a kind of capacitor testing fixture, this practicality
It is new to be achieved through the following technical solutions above-mentioned purpose：
A kind of pilot scale glass reaction kettle for room temperature synthesis high molecular material, including supporting rack, variable-frequency motor and bilayer
Glass reaction kettle, the variable-frequency motor are connected with rabble by universal joint in the vertical direction, and the rabble stretches into described
In double-layer glass reaction kettle, the universal joint is connected with crossbearer in the horizontal direction, and described upper crossbearer one end is equipped with the first limit
Position stent, the other end are equipped with the second limiting bracket, and upper press cover is equipped with below the universal joint, is fixed with below the upper press cover
Middle crossbearer, wherein the middle cross frame lower section are equipped with lower cross frame, lower cover, the upper press cover and lower cover are fixed with the lower cross frame
Between hollow double-layer glass reaction kettle is installed, the rabble is equipped with ribbon spiral shape blade, the ribbon spiral shape
Connected between blade and the rabble by strut, the rabble bottom is equipped with agitating paddle, and support frame as described above is equipped with the
Three limiting brackets, are equipped with support quarter butt, control are fixed with the support quarter butt between the 3rd limiting bracket and middle crossbearer
Device processed.
Further, first limiting bracket is fixedly connected by geometrical clamp with condenser, and the condenser lower end is set
There is the condenser pipe stretched to inside the double-layer glass reaction kettle.
Further, it is fixed with constant pressure funnel on second limiting bracket.
Further, support frame as described above bottom is equipped with universal wheel.
Further, feed inlet is equipped with the top of the double-layer glass reaction kettle, bottom is equipped with outlet valve.
Further, the outlet valve includes being arranged at the sealing flap inside the double-layer glass reaction kettle and passing through out
The valve rod that material mouth is attached thereto, the valve rod both sides are equipped with isocon.
The beneficial effects of the utility model are：
The middle part of rabble sets ribbon spiral shape blade, and bottom is equipped with agitating paddle, and ribbon spiral shape blade can make instead
Answer liquid to flow in vertical direction, coordinate with rabble, so that material mixing is evenly, can efficiently disperse what is be added dropwise
Initiator, prevents that material local concentration is excessive, and causes side reaction, improves product quality, meets the use demand of enterprise.Stir
Bar and ribbon spiral shape blade are mixed, the dynamics of stirring and the space of stirring is increased, for the high liquid material of concentration, can do
All stirred evenly to whole material upper strata and bottom, synthetic effect is notable.In addition, the utility model is simple in structure, can reduce
Vibrations, so that ensure that reaction kettle works normally, the production efficiency greatly improved.
Brief description of the drawings
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, drawings in the following description are only
It is some embodiments of the utility model, for those of ordinary skill in the art, in the premise not made the creative labor
Under, other attached drawings can also be obtained according to these attached drawings.
Fig. 1 is the utility model structure diagram；
Fig. 2 is the structure diagram of the utility model outlet valve.
Embodiment
To make the purpose of this utility model, technical solution and advantage clearer, below by the technology of the utility model
Scheme is described in detail.Obviously, the described embodiments are only a part of the embodiments of the utility model, rather than all
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not before creative work is made
Obtained all other embodiment is put, belongs to the scope that the utility model is protected.
Referring to shown in Fig. 1-Fig. 2, the utility model provides a kind of pilot scale glass for room temperature synthesis high molecular material
Reaction kettle, including supporting rack 100, variable-frequency motor 200 and double-layer glass reaction kettle 300, the variable-frequency motor 200 pass through universal joint
201 in the vertical directions are connected with rabble 310, and the rabble 310 is stretched into the double-layer glass reaction kettle 300, described
Universal joint 201 is connected with crossbearer 120 in the horizontal direction, and described upper 120 one end of crossbearer is equipped with the first limiting bracket 211, separately
One end is equipped with the second limiting bracket 203, and the lower section of universal joint 201 is equipped with upper press cover 111, and the lower section of upper press cover 111 is fixed
Equipped with middle crossbearer 110, the lower section of wherein the middle cross frame 110 is equipped with lower cross frame 130, and lower cover is fixed with the lower cross frame 130
101, hollow double-layer glass reaction kettle 300 is installed, on the rabble 310 between the upper press cover 111 and lower cover 101
Equipped with ribbon spiral shape blade 320, connected between the ribbon spiral shape blade 320 and the rabble 310 by strut 303
Connecing, 310 bottom of rabble is equipped with agitating paddle 302, and support frame as described above 100 is equipped with the 3rd limiting bracket 133, and the described 3rd
Support quarter butt 112 is equipped between limiting bracket 133 and middle crossbearer 110, controller 132 is fixed with the support quarter butt 112.
First limiting bracket 211 is fixedly connected by geometrical clamp 212 with condenser 210, and 210 lower end of condenser, which is equipped with, to be stretched to
Condenser pipe 213 inside the double-layer glass reaction kettle 300.Constant pressure funnel is fixed with second limiting bracket 203
202.100 bottom of support frame as described above is equipped with universal wheel 131.The top of double-layer glass reaction kettle 300 is equipped with feed inlet 321, bottom
Portion is equipped with outlet valve 301.The outlet valve 301 includes being arranged at the sealing flap inside the double-layer glass reaction kettle 300
3011 and the valve rod 3013 that is attached thereto through discharge port 3010,3013 both sides of valve rod are equipped with isocon 3012.
It should be noted that the utility model is a kind of pilot scale glass reaction kettle that high molecular material is synthesized for room temperature,
During work, raw material is added in double-layer glass reaction kettle 300 by feed inlet 321, then to double-layer glass reaction kettle 300
Hot water is passed through in interlayer and carries out circulating-heating, reaches and initiator, rabble 310 is added dropwise by constant pressure funnel 202 after assigned temperature
Middle part ribbon spiral shape blade 320 is set, bottom is equipped with agitating paddle 302, and ribbon spiral shape blade 320 can make reaction solution exist
Vertical Square flows up, and coordinates with rabble 310, so that material mixing is evenly, can efficiently disperse to be added dropwise draws
Agent is sent out, prevents that material local concentration is excessive, and causes side reaction, improves product quality, meets the use demand of enterprise, is triggered
When insulation 4-6 is small after agent is added dropwise, treat that temperature is reduced to 50 DEG C or so dischargings.
The above, is only specific embodiment of the present utility model, but the scope of protection of the utility model is not limited to
In this, any one skilled in the art can readily occur in change in the technical scope that the utility model discloses
Or replace, it should be covered within the scope of the utility model.Therefore, the scope of protection of the utility model should be with the power
Subject to the protection domain that profit requires.
Claims (6)
- A kind of 1. pilot scale glass reaction kettle for room temperature synthesis high molecular material, it is characterised in that：Including supporting rack（100）、 Variable-frequency motor（200）And double-layer glass reaction kettle（300）, the variable-frequency motor（200）Pass through universal joint（201）In vertical direction On be connected with rabble（310）, the rabble（310）Stretch into the double-layer glass reaction kettle（300）It is interior, the universal joint （201）Crossbearer is connected with the horizontal direction（120）, the upper crossbearer（120）One end is equipped with the first limiting bracket（211）, The other end is equipped with the second limiting bracket（203）, the universal joint（201）Lower section is equipped with upper press cover（111）, the upper press cover （111）Lower section is fixed with middle crossbearer（110）, wherein the middle cross frame（110）Lower section is equipped with lower cross frame（130）, the lower cross frame （130）On be fixed with lower cover（101）, the upper press cover（111）And lower cover（101）Between hollow double-deck glass is installed Glass reaction kettle（300）, the rabble（310）It is equipped with ribbon spiral shape blade（320）, the ribbon spiral shape blade （320）With the rabble（310）Between pass through strut（303）Connection, the rabble（310）Bottom is equipped with agitating paddle （302）, support frame as described above（100）It is equipped with the 3rd limiting bracket（133）, the 3rd limiting bracket（133）With middle crossbearer （110）Between be equipped with support quarter butt（112）, the support quarter butt（112）On be fixed with controller（132）.
- A kind of 2. pilot scale glass reaction kettle for room temperature synthesis high molecular material according to claim 1, it is characterised in that： First limiting bracket（211）Pass through geometrical clamp（212）And condenser（210）It is fixedly connected, the condenser（210）Lower end Equipped with stretching to the double-layer glass reaction kettle（300）Internal condenser pipe（213）.
- A kind of 3. pilot scale glass reaction kettle for room temperature synthesis high molecular material according to claim 1, it is characterised in that： Second limiting bracket（203）On be fixed with constant pressure funnel（202）.
- A kind of 4. pilot scale glass reaction kettle for room temperature synthesis high molecular material according to claim 1, it is characterised in that： Support frame as described above（100）Bottom is equipped with universal wheel（131）.
- A kind of 5. pilot scale glass reaction kettle for room temperature synthesis high molecular material according to claim 1, it is characterised in that： The double-layer glass reaction kettle（300）Top is equipped with feed inlet（321）, bottom is equipped with outlet valve（301）.
- A kind of 6. pilot scale glass reaction kettle for room temperature synthesis high molecular material according to claim 5, it is characterised in that： The outlet valve（301）Including being arranged at the double-layer glass reaction kettle（300）Internal sealing flap（3011）With through going out Material mouth（3010）The valve rod being attached thereto（3013）, the valve rod（3013）Both sides are equipped with isocon（3012）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721259958.8U CN207307857U (en) | 2017-09-28 | 2017-09-28 | A kind of pilot scale glass reaction kettle for room temperature synthesis high molecular material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721259958.8U CN207307857U (en) | 2017-09-28 | 2017-09-28 | A kind of pilot scale glass reaction kettle for room temperature synthesis high molecular material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207307857U true CN207307857U (en) | 2018-05-04 |
Family
ID=62428130
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721259958.8U Active CN207307857U (en) | 2017-09-28 | 2017-09-28 | A kind of pilot scale glass reaction kettle for room temperature synthesis high molecular material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207307857U (en) |
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2017
- 2017-09-28 CN CN201721259958.8U patent/CN207307857U/en active Active
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