CN207342694U - A kind of double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer - Google Patents
A kind of double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer Download PDFInfo
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- CN207342694U CN207342694U CN201721260977.2U CN201721260977U CN207342694U CN 207342694 U CN207342694 U CN 207342694U CN 201721260977 U CN201721260977 U CN 201721260977U CN 207342694 U CN207342694 U CN 207342694U
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- reaction kettle
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- glass reaction
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Abstract
A kind of double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer, including supporting rack, variable-frequency motor and double-layer glass reaction kettle, variable-frequency motor is connected with rabble by universal joint in the vertical direction, double-layer glass reaction kettle is installed between upper press cover and lower cover, material separating disc is fixed with the top of rabble, upper agitating vane is equipped with below material separating disc, middle agitating vane is equipped with below upper agitating vane, rabble bottom is equipped with lower stirring paddle, supporting rack is equipped with stent, support quarter butt is equipped between stent and middle crossbearer, supports and is fixed with controller on quarter butt.Multilayer rabble and agitating paddle, increase the dynamics of stirring and the space of stirring, for the high liquid material of concentration, can accomplish that whole material upper strata and bottom all stir evenly, synthetic effect is notable.Work light is equipped with the top of controller, its middle part is equipped with temperature adjustment knob and rotational speed regulation knob, and its underpart is equipped with temperature display, can be very good to understand and controls the parameters in reaction process.
Description
Technical field
It the utility model is related to chemical reaction kettle technical field, and in particular to a kind of double-deck glass for synthesizing polycarboxylate water-reducer
Glass reaction kettle.
Background technology
With the fast development of water-reducing agent industry, the requirement in experimentation to chemical reaction kettle it is also higher and higher, it is necessary to
By the structure design and parameter configuration to container, the mixture work(of the heating of technological requirement, evaporation, cooling and low high speed is realized
Energy.Polycarboxylate water-reducer is currently used high-performance water reducing agent, and the high efficiency water reducing agent that its working condition is more general is more severe
Carve, if in polymerization process, monomer polymerization is incomplete, not only have environmentally friendly hidden danger, but also the performance of concrete can be influenced.In
During examination, due to the glass reaction kettle of 20L, autoclave body depth more than 50cm, agitating paddle set it is on the lower side, for excessive concentration,
The big polycarboxylate water-reducer of viscosity, upper strata stirring dynamics is inadequate, and stirring is insufficient, and material mixing is uneven, and material is added dropwise can only
Drop down on high concentration liquid upper strata, cause local reaction uneven, influence synthetic effect.
Utility model content
The purpose of this utility model is that to solve the above-mentioned problems and provides a kind of capacitor testing fixture, this practicality
It is new to be achieved through the following technical solutions above-mentioned purpose:
A kind of double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer, including supporting rack, variable-frequency motor and double glazing are anti-
Kettle is answered, the variable-frequency motor is connected with rabble by universal joint in the vertical direction, and the rabble stretches into the double-deck glass
In glass reaction kettle, the universal joint is connected with crossbearer in the horizontal direction, and described upper crossbearer one end is equipped with limiting bracket, described
Upper press cover is equipped with below universal joint, middle crossbearer is fixed with below the upper press cover, lower cross frame, institute are equipped with below wherein the middle cross frame
State and lower cover is fixed with lower cross frame, double-layer glass reaction kettle, the stirring are installed between the upper press cover and lower cover
Material separating disc is fixed with the top of bar, upper agitating vane is equipped with below the material separating disc, is stirred in being equipped with below the upper agitating vane
Blade is mixed, the rabble bottom is equipped with lower stirring paddle, and support frame as described above is equipped with stent, is set between the stent and middle crossbearer
There is support quarter butt, be fixed with controller on the support quarter butt, feed inlet, bottom are equipped with the top of the double-layer glass reaction kettle
Equipped with outlet valve, the side of the feed inlet is equipped with steady thermometer, and the top of the double-layer glass reaction kettle is equipped with oil inlet, bottom
Portion is equipped with oil outlet.
Further, work light is equipped with the top of the controller, its middle part is equipped with temperature adjustment knob and rotating speed tune
Knob is saved, its underpart is equipped with temperature display.
Further, it is fixed with constant pressure funnel on the limiting bracket.
Further, support frame as described above bottom is equipped with fixed seat.
Further, the material separating disc is umbrella, be which is provided with equipped with sub-material mouth.
Further, the outlet valve includes being arranged at the sealing flap inside the double-layer glass reaction kettle and passing through out
The valve rod that material mouth is attached thereto, the valve rod both sides are equipped with isocon.
The beneficial effects of the utility model are:
Rabble is equipped with upper agitating vane, middle agitating vane and lower stirring paddle successively from top to bottom, is set at the top of rabble
There is umbrella material separating disc, so that the material mixing added is evenly, can efficiently disperse the initiator being added dropwise, prevent material
Local concentration is excessive, and causes side reaction, improves product quality, meets the use demand of enterprise, multilayer rabble and stirring
Paddle, increases the dynamics of stirring and the space of stirring, for the high liquid material of concentration, can accomplish whole material upper strata and bottom
Portion all stirs evenly, and synthetic effect is notable.Work light is equipped with the top of controller, its middle part is equipped with temperature adjustment knob and turns
Fast adjusting knob, its underpart are equipped with temperature display, can be very good to understand and control the parameters in reaction process, separately
Outside, the utility model is simple in structure, can reduce vibrations, so that ensure that reaction kettle works normally, the production efficiency greatly improved.
Brief description of the drawings
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, drawings in the following description are only
It is some embodiments of the utility model, for those of ordinary skill in the art, in the premise not made the creative labor
Under, other attached drawings can also be obtained according to these attached drawings.
Fig. 1 is the utility model structure diagram;
Fig. 2 is the structure diagram of the utility model outlet valve;
Fig. 3 is the utility model controller architecture schematic diagram;
Fig. 4 is the utility model material separating disc structure diagram.
Embodiment
To make the purpose of this utility model, technical solution and advantage clearer, below by the technology of the utility model
Scheme is described in detail.Obviously, the described embodiments are only a part of the embodiments of the utility model, rather than all
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not before creative work is made
Obtained all other embodiment is put, belongs to the scope that the utility model is protected.
Referring to shown in Fig. 1-Fig. 4, the utility model provides a kind of double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer,
Including supporting rack 100, variable-frequency motor 200 and double-layer glass reaction kettle 300, the variable-frequency motor 200 is by universal joint 201 perpendicular
Nogata has connected up rabble 310, and the rabble 310 is stretched into the double-layer glass reaction kettle 300, the universal joint
201 are connected with crossbearer 120 in the horizontal direction, and described upper 120 one end of crossbearer is equipped with limiting bracket 203, the universal joint 201
Lower section is equipped with upper press cover 111, and the lower section of upper press cover 111 is fixed with middle crossbearer 110, and the lower section of wherein the middle cross frame 110 is equipped with down
Crossbearer 130, is fixed with lower cover 101 on the lower cross frame 130, is provided between the upper press cover 111 and lower cover 101 double
Layer glass reaction kettle 300, the top of rabble 310 are fixed with material separating disc 320, and the lower section of material separating disc 320, which is equipped with, above to be stirred
Blade 313 is mixed, the upper lower section of agitating vane 313 is equipped with middle agitating vane 303, and 310 bottom of rabble is equipped with lower stirring
Paddle 302, support frame as described above 100 are equipped with stent 133, and support quarter butt 112, institute are equipped between the stent 133 and middle crossbearer 110
State and controller 132 is fixed with support quarter butt 112, the top of double-layer glass reaction kettle 300 is equipped with feed inlet 321, bottom
Equipped with outlet valve 301, the side of the feed inlet 321 is equipped with steady thermometer 213, the top of the double-layer glass reaction kettle 300
Equipped with oil inlet 223, bottom is equipped with oil outlet 220.
The top of controller 132 is equipped with work light 1322, its middle part is equipped with temperature adjustment knob 1323 and rotating speed
Adjusting knob 1321, its underpart are equipped with temperature display 1320.Constant pressure funnel 202 is fixed with the limiting bracket 203.Institute
State 100 bottom of supporting rack and be equipped with fixed seat 131.The material separating disc 320 is umbrella, be which is provided with equipped with sub-material mouth 3201.It is described
Outlet valve 301 include being arranged at sealing flap 3011 double-layer glass reaction kettle 300 inside and through discharge port 3010 and
Connection valve rod 3013,3013 both sides of valve rod are equipped with isocon 3012.
It should be noted that the utility model is a kind of double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer, during work,
Raw material is added in double-layer glass reaction kettle 300 by feed inlet 321, then by oil inlet 223 and oil outlet 220 to double
Deep fat is passed through in the interlayer of layer glass reaction kettle 300 and carries out circulating-heating, is added dropwise after reaching assigned temperature by constant pressure funnel 202
Initiator, rabble 310 are equipped with upper agitating vane 313, middle agitating vane 303 and lower stirring paddle 302, stir successively from top to bottom
Mix the top of bar 310 and be equipped with umbrella material separating disc 320, so that the material mixing added is evenly, can efficiently disperse to be added dropwise
Initiator, prevent that material local concentration is excessive, and cause side reaction, improve product quality, meet the use demand of enterprise,
The top of controller 132 is equipped with work light 1322, its middle part is equipped with temperature adjustment knob 1323 and rotational speed regulation knob 1321,
Its underpart is equipped with temperature display 1320, can be very good to understand and controls the parameters in reaction process, and initiator is added dropwise
After keep the temperature 4-6 it is small when, treat that temperature is reduced to 50 DEG C or so and adds 50%KOH solution and be neutralized to pH=7-8 and can pass through discharging
Valve 301 releases the finished product that synthesis finishes.
The above, is only specific embodiment of the present utility model, but the scope of protection of the utility model is not limited to
In this, any one skilled in the art can readily occur in change in the technical scope that the utility model discloses
Or replace, it should be covered within the scope of the utility model.Therefore, the scope of protection of the utility model should be with the power
Subject to the protection domain that profit requires.
Claims (6)
- A kind of 1. double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer, it is characterised in that:Including supporting rack(100), variable-frequency electric Machine(200)And double-layer glass reaction kettle(300), the variable-frequency motor(200)Pass through universal joint(201)In the vertical direction connects There is rabble(310), the rabble(310)Stretch into the double-layer glass reaction kettle(300)It is interior, the universal joint(201) Crossbearer is connected with horizontal direction(120), the upper crossbearer(120)One end is equipped with limiting bracket(203), the universal joint (201)Lower section is equipped with upper press cover(111), the upper press cover(111)Lower section is fixed with middle crossbearer(110), wherein the middle cross frame (110)Lower section is equipped with lower cross frame(130), the lower cross frame(130)On be fixed with lower cover(101), the upper press cover(111) And lower cover(101)Between double-layer glass reaction kettle is installed(300), the rabble(310)Top is fixed with material separating disc (320), the material separating disc(320)Lower section is equipped with upper agitating vane(313), the upper agitating vane(313)Lower section is stirred in being equipped with Mix blade(303), the rabble(310)Bottom is equipped with lower stirring paddle(302), support frame as described above(100)It is equipped with stent (133), the stent(133)With middle crossbearer(110)Between be equipped with support quarter butt(112), the support quarter butt(112)Upper fixation Equipped with controller(132), the double-layer glass reaction kettle(300)Top is equipped with feed inlet(321), bottom is equipped with outlet valve (301), the feed inlet(321)Side be equipped with steady thermometer(213), the double-layer glass reaction kettle(300)Top set There is oil inlet(223), bottom is equipped with oil outlet(220).
- A kind of 2. double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer according to claim 1, it is characterised in that:The control Device processed(132)Top is equipped with work light(1322), its middle part is equipped with temperature adjustment knob(1323)With rotational speed regulation knob (1321), its underpart is equipped with temperature display(1320).
- A kind of 3. double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer according to claim 1, it is characterised in that:The limit Position stent(203)On be fixed with constant pressure funnel(202).
- A kind of 4. double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer according to claim 1, it is characterised in that:The branch Support(100)Bottom is equipped with fixed seat(131).
- A kind of 5. double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer according to claim 1, it is characterised in that:Described point Charging tray(320)For umbrella, which is provided with equipped with sub-material mouth(3201).
- A kind of 6. double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer according to claim 1, it is characterised in that:It is described go out Expect valve(301)Including being arranged at the double-layer glass reaction kettle(300)Internal sealing flap(3011)With through discharge port (3010)The valve rod being attached thereto(3013), the valve rod(3013)Both sides are equipped with isocon(3012).
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CN201721260977.2U CN207342694U (en) | 2017-09-28 | 2017-09-28 | A kind of double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer |
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CN201721260977.2U CN207342694U (en) | 2017-09-28 | 2017-09-28 | A kind of double-layer glass reaction kettle for synthesizing polycarboxylate water-reducer |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112896251A (en) * | 2021-01-18 | 2021-06-04 | 岳丹 | Hot pitch transports strorage device for municipal administration highway construction |
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2017
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112896251A (en) * | 2021-01-18 | 2021-06-04 | 岳丹 | Hot pitch transports strorage device for municipal administration highway construction |
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