CN205684036U - A kind of without stirring horizontal reacting still - Google Patents

A kind of without stirring horizontal reacting still Download PDF

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Publication number
CN205684036U
CN205684036U CN201620535472.1U CN201620535472U CN205684036U CN 205684036 U CN205684036 U CN 205684036U CN 201620535472 U CN201620535472 U CN 201620535472U CN 205684036 U CN205684036 U CN 205684036U
Authority
CN
China
Prior art keywords
kettle
drain
support
horizontal reacting
driving motor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620535472.1U
Other languages
Chinese (zh)
Inventor
赵勇
杨旭林
罗男
罗一男
吴斌
刘钢
刘琦
张利
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chengdu Dymatic Jingying Chemicals Co., Ltd.
Original Assignee
Shunde Gao Naite Novel Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shunde Gao Naite Novel Material Co Ltd filed Critical Shunde Gao Naite Novel Material Co Ltd
Priority to CN201620535472.1U priority Critical patent/CN205684036U/en
Application granted granted Critical
Publication of CN205684036U publication Critical patent/CN205684036U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of without stirring horizontal reacting still.Including kettle, driving motor and support support, kettle is olive shape or the rhombus hollow vessel that two ends diameter is less than mid diameter, kettle both ends horizontal is supported on support, one end rotates with driving motor and couples, the other end is provided with the refluxing opening with kettle external connection and drain, is provided with drain hole in the middle part of kettle on a sidewall;Refluxing opening and drain are horizontally fixed on support and realize sealing by two-sided mechanical seal;Kettle outer wall is heated or cooled chuck;Drain is connected with emptying head by pipeline, and emptying head has isolating strainer and is arranged at kettle lateral middle, longitudinally upper region.This utility model, without internal stirrers, makes reactant can be fully contacted, without dead angle with reactor inwall each point, apparatus structure is simple, the cleaning of reactor of being more convenient for and thorough blowing, it is ensured that and improve product quality, improve product yield, reduce device fabrication cost.

Description

A kind of without stirring horizontal reacting still
Technical field
This utility model relates to a kind of chemical synthesizer, relates to a kind of Special Resin synthesizer, specifically a kind of nothing Stirring horizontal reacting still.
Background technology
The synthesizer of existing Special Resin uses vertical blade stirred tank, adds reaction mass from top, and bottom is put Go out synthetic product resin.
Use vertical blade stirred tank to make there is fraction material during blowing due to the existence of blade, particularly close The catalyst of resin sinks to the bottom, and partial reaction thing can be sticky on stirring paddle so that product yield reduces, and product quality declines, Criticize difference relatively big, add burden also to the cleaning of reactor.And owing to reaction temperature is higher, there is raw material before starting the reaction Distillation also forms crystallization on reactor top, makes reactant ratio unbalance, causes product quality to decline the most qualified.
Existing horizontal reacting still generally also uses agitating device, and is vented unreasonable structure.Due to conventional Horizontal counter The rotation answering still to be dependent on internal shaft carrys out mixed material, thus there is catalyst sedimentation problem, raw and auxiliary material is sublimate into instead Answer the crystallization of still top to make reaction ratio unbalance, there is also liquid level in course of reaction and enclose waving due to solvent by still wall one Send out very fast, cause this region reactant molecule amount unbalanced problem of the excessive reaction even cross-linked, cause molecular weight distribution to become Width affects end product quality.
Summary of the invention
This utility model discloses a kind of without stirring horizontal reacting still according to the deficiencies in the prior art.This utility model to solve Problem certainly is to provide one and is capable of each abundant reaction of reaction nothing, without washing the nothing stirring of still difficulty and reactant unbalance Horizontal reacting still.
This utility model is achieved through the following technical solutions:
Without stirring horizontal reacting still, including kettle, driving motor and support support, it is characterised in that: described kettle is two End diameter is less than olive shape or the rhombus hollow vessel of mid diameter, and kettle both ends horizontal is supported on support, one end and transmission Electric machine rotation couples, and the other end is provided with the refluxing opening with kettle external connection and drain, olive shape or Pedicellus et Pericarpium Trapae in the middle part of kettle It is provided with drain hole on one sidewall of shape tank body.
Described refluxing opening and drain are horizontally fixed on support and realize sealing by two-sided mechanical seal.
Described kettle outer wall has the chuck for reactor is heated or cooled.
Described drain by pipeline with emptying head be connected, be vented head have isolating strainer and be arranged at kettle lateral middle, Longitudinally upper region.
This utility model uses horizontal reacting still structure, and driving motor directly drives kettle to rotate, and this rotation instead of The stirring paddle of vertical response still, by this rotation, reactant is constantly fully contacted with still inwall, the material of distillation the most constantly quilt Bring reaction system into, make raw and auxiliary material more fully complete reaction, be effectively improved productivity.
When feeding intake, tapping hole is upward, puts into raw material from top.During blowing, tapping hole is downward, releases thing from dispensing valve Material.
This utility model helpfulness: this utility model changes traditional vertical response still, removes internal stirrers, makes anti- Answer thing can be fully contacted, without dead angle with reactor inwall each point.Apparatus structure is simple, the cleaning of reactor of being more convenient for and thoroughly putting Material, it is ensured that and improve product quality, improve product yield, reduce device fabrication cost.
Accompanying drawing explanation
Fig. 1 is this utility model reactor structural representation.
In figure, 1 is kettle, and 2 is chuck, and 3 is manhole and solid dog-house, and 4 is drain hole, and 5 is driving motor, and 6 is to put Eating dishes without rice or wine, 7 is refluxing opening, and 8 is support, and 9 is emptying head.
Detailed description of the invention
Further illustrating this utility model below in conjunction with detailed description of the invention, detailed description of the invention is to this utility model Further illustrating of principle, limits this utility model never in any form, and technology same or like with this utility model does not all have Scope beyond this utility model protection.
In conjunction with accompanying drawing 1.
Without stirring horizontal reacting still, including kettle 1, driving motor 5 and support support 8, described kettle 1 is that two ends diameter is little In olive shape or the rhombus hollow vessel of mid diameter, kettle 1 both ends horizontal is supported on support 8, one end and driving motor 5 turns Dynamic connection, the other end is provided with the refluxing opening 7 with kettle 1 external connection and drain 6, olive shape or rhombus in the middle part of kettle 1 It is provided with drain hole 4 on one sidewall of tank body.
Refluxing opening 7 and drain 6 are horizontally fixed on support 8 and realize sealing by two-sided mechanical seal.Kettle 1 outer wall There is the chuck 2 for reactor is heated or cooled.
Drain 6 is connected with emptying 9 by pipeline, be vented 9 have isolating strainer and be arranged at kettle 1 lateral middle, Longitudinally upper region.
Kettle 1 accumbency is arranged on support 8 or platform, and raw material puts into from manhole and solid dog-house 3.After having fed intake Locking manhole and solid dog-house 3, need to regulate driving motor 5 rotating speed according to technique.Manhole and solid is adjusted at the end of reaction Dog-house 3 down, releases product from drain hole 4.Only need to add a small amount of solvent when washing still, just can be reached by the rotation of kettle 1 Cleaning performance.
This utility model is a kind of improvement to conventional synthesis still, synthesis reactor accumbency is installed, by the rotation generation of kettle 1 For the effect of stirring paddle, save equipment making expense.And, kettle 1 is internal without dead angle, material can touch inwall each Corner, it is to avoid the reactant that traditional reactor causes due to material distillation crystallization is unbalance.Make reaction more abundant, product yield It is greatly improved.Blowing is more thorough, further increases product yield.Wash still more convenient, it is not necessary to steamed by solvent Vapour just can wash the clout at kettle 1 top off, and only a small amount of solvent of need just can be reactor by the rotation of kettle 1 in suitable temperature Clean up, reduce energy consumption, saved cost.
This utility model refluxing opening 7, drain 6 are horizontally mounted and are fixed on support 1 and are realized by two-sided mechanical seal Sealing, in reactor rotates, refluxing opening 7, drain 6 opposite brackets 1 are static, realize material by the rotation of kettle 1 Mixing.Emptying 9 is positioned at kettle 1 top, does not results in blocking in kettle 1 revolving reaction process.

Claims (4)

1. without a stirring horizontal reacting still, including kettle (1), driving motor (5) and support support (8), it is characterised in that: institute Stating kettle (1) is olive shape or the rhombus hollow vessel that two ends diameter is less than mid diameter, and kettle (1) both ends horizontal is supported on On frame (8), one end and driving motor (5) rotate and couple, the other end be provided with and the refluxing opening (7) of kettle (1) external connection and Drain (6), is provided with drain hole (4) on a sidewall of kettle (1) middle part olive shape or rhombus tank body.
It is the most according to claim 1 without stirring horizontal reacting still, it is characterised in that: described refluxing opening (7) and drain (6) It is horizontally fixed on support (8) above and to realize sealing by two-sided mechanical seal.
The most according to claim 1 and 2 without stirring horizontal reacting still, it is characterised in that: described kettle (1) outer wall have for The chuck (2) of reactor is heated or cooled.
The most according to claim 3 without stirring horizontal reacting still, it is characterised in that: described drain (6) by pipeline with Emptying head (9) connects, and emptying head (9) has isolating strainer and is arranged at kettle (1) lateral middle, longitudinally upper region.
CN201620535472.1U 2016-06-01 2016-06-01 A kind of without stirring horizontal reacting still Expired - Fee Related CN205684036U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620535472.1U CN205684036U (en) 2016-06-01 2016-06-01 A kind of without stirring horizontal reacting still

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620535472.1U CN205684036U (en) 2016-06-01 2016-06-01 A kind of without stirring horizontal reacting still

Publications (1)

Publication Number Publication Date
CN205684036U true CN205684036U (en) 2016-11-16

Family

ID=57260686

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620535472.1U Expired - Fee Related CN205684036U (en) 2016-06-01 2016-06-01 A kind of without stirring horizontal reacting still

Country Status (1)

Country Link
CN (1) CN205684036U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107096488A (en) * 2017-06-25 2017-08-29 盐城利民农化有限公司 A kind of synthesizer of olefin conversion
CN107159073A (en) * 2017-06-25 2017-09-15 盐城利民农化有限公司 A kind of synthesizer of paclobutrazol product

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107096488A (en) * 2017-06-25 2017-08-29 盐城利民农化有限公司 A kind of synthesizer of olefin conversion
CN107159073A (en) * 2017-06-25 2017-09-15 盐城利民农化有限公司 A kind of synthesizer of paclobutrazol product

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20170915

Address after: Xinjin County of Chengdu City, Sichuan province 611436 Deng Shuang Zhen Fine Chemical Industrial Park

Patentee after: Chengdu Dymatic Jingying Chemicals Co., Ltd.

Address before: 528306, Guangdong Province, Shunde District, Foshan Ronggui Li neighborhood committee building Feng Road, No. 7, Room Seven

Patentee before: Shunde Gao Naite novel material company limited

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161116

Termination date: 20200601

CF01 Termination of patent right due to non-payment of annual fee