A kind of without stirring horizontal reacting still
Technical field
This utility model relates to a kind of chemical synthesizer, relates to a kind of Special Resin synthesizer, specifically a kind of nothing
Stirring horizontal reacting still.
Background technology
The synthesizer of existing Special Resin uses vertical blade stirred tank, adds reaction mass from top, and bottom is put
Go out synthetic product resin.
Use vertical blade stirred tank to make there is fraction material during blowing due to the existence of blade, particularly close
The catalyst of resin sinks to the bottom, and partial reaction thing can be sticky on stirring paddle so that product yield reduces, and product quality declines,
Criticize difference relatively big, add burden also to the cleaning of reactor.And owing to reaction temperature is higher, there is raw material before starting the reaction
Distillation also forms crystallization on reactor top, makes reactant ratio unbalance, causes product quality to decline the most qualified.
Existing horizontal reacting still generally also uses agitating device, and is vented unreasonable structure.Due to conventional Horizontal counter
The rotation answering still to be dependent on internal shaft carrys out mixed material, thus there is catalyst sedimentation problem, raw and auxiliary material is sublimate into instead
Answer the crystallization of still top to make reaction ratio unbalance, there is also liquid level in course of reaction and enclose waving due to solvent by still wall one
Send out very fast, cause this region reactant molecule amount unbalanced problem of the excessive reaction even cross-linked, cause molecular weight distribution to become
Width affects end product quality.
Summary of the invention
This utility model discloses a kind of without stirring horizontal reacting still according to the deficiencies in the prior art.This utility model to solve
Problem certainly is to provide one and is capable of each abundant reaction of reaction nothing, without washing the nothing stirring of still difficulty and reactant unbalance
Horizontal reacting still.
This utility model is achieved through the following technical solutions:
Without stirring horizontal reacting still, including kettle, driving motor and support support, it is characterised in that: described kettle is two
End diameter is less than olive shape or the rhombus hollow vessel of mid diameter, and kettle both ends horizontal is supported on support, one end and transmission
Electric machine rotation couples, and the other end is provided with the refluxing opening with kettle external connection and drain, olive shape or Pedicellus et Pericarpium Trapae in the middle part of kettle
It is provided with drain hole on one sidewall of shape tank body.
Described refluxing opening and drain are horizontally fixed on support and realize sealing by two-sided mechanical seal.
Described kettle outer wall has the chuck for reactor is heated or cooled.
Described drain by pipeline with emptying head be connected, be vented head have isolating strainer and be arranged at kettle lateral middle,
Longitudinally upper region.
This utility model uses horizontal reacting still structure, and driving motor directly drives kettle to rotate, and this rotation instead of
The stirring paddle of vertical response still, by this rotation, reactant is constantly fully contacted with still inwall, the material of distillation the most constantly quilt
Bring reaction system into, make raw and auxiliary material more fully complete reaction, be effectively improved productivity.
When feeding intake, tapping hole is upward, puts into raw material from top.During blowing, tapping hole is downward, releases thing from dispensing valve
Material.
This utility model helpfulness: this utility model changes traditional vertical response still, removes internal stirrers, makes anti-
Answer thing can be fully contacted, without dead angle with reactor inwall each point.Apparatus structure is simple, the cleaning of reactor of being more convenient for and thoroughly putting
Material, it is ensured that and improve product quality, improve product yield, reduce device fabrication cost.
Accompanying drawing explanation
Fig. 1 is this utility model reactor structural representation.
In figure, 1 is kettle, and 2 is chuck, and 3 is manhole and solid dog-house, and 4 is drain hole, and 5 is driving motor, and 6 is to put
Eating dishes without rice or wine, 7 is refluxing opening, and 8 is support, and 9 is emptying head.
Detailed description of the invention
Further illustrating this utility model below in conjunction with detailed description of the invention, detailed description of the invention is to this utility model
Further illustrating of principle, limits this utility model never in any form, and technology same or like with this utility model does not all have
Scope beyond this utility model protection.
In conjunction with accompanying drawing 1.
Without stirring horizontal reacting still, including kettle 1, driving motor 5 and support support 8, described kettle 1 is that two ends diameter is little
In olive shape or the rhombus hollow vessel of mid diameter, kettle 1 both ends horizontal is supported on support 8, one end and driving motor 5 turns
Dynamic connection, the other end is provided with the refluxing opening 7 with kettle 1 external connection and drain 6, olive shape or rhombus in the middle part of kettle 1
It is provided with drain hole 4 on one sidewall of tank body.
Refluxing opening 7 and drain 6 are horizontally fixed on support 8 and realize sealing by two-sided mechanical seal.Kettle 1 outer wall
There is the chuck 2 for reactor is heated or cooled.
Drain 6 is connected with emptying 9 by pipeline, be vented 9 have isolating strainer and be arranged at kettle 1 lateral middle,
Longitudinally upper region.
Kettle 1 accumbency is arranged on support 8 or platform, and raw material puts into from manhole and solid dog-house 3.After having fed intake
Locking manhole and solid dog-house 3, need to regulate driving motor 5 rotating speed according to technique.Manhole and solid is adjusted at the end of reaction
Dog-house 3 down, releases product from drain hole 4.Only need to add a small amount of solvent when washing still, just can be reached by the rotation of kettle 1
Cleaning performance.
This utility model is a kind of improvement to conventional synthesis still, synthesis reactor accumbency is installed, by the rotation generation of kettle 1
For the effect of stirring paddle, save equipment making expense.And, kettle 1 is internal without dead angle, material can touch inwall each
Corner, it is to avoid the reactant that traditional reactor causes due to material distillation crystallization is unbalance.Make reaction more abundant, product yield
It is greatly improved.Blowing is more thorough, further increases product yield.Wash still more convenient, it is not necessary to steamed by solvent
Vapour just can wash the clout at kettle 1 top off, and only a small amount of solvent of need just can be reactor by the rotation of kettle 1 in suitable temperature
Clean up, reduce energy consumption, saved cost.
This utility model refluxing opening 7, drain 6 are horizontally mounted and are fixed on support 1 and are realized by two-sided mechanical seal
Sealing, in reactor rotates, refluxing opening 7, drain 6 opposite brackets 1 are static, realize material by the rotation of kettle 1
Mixing.Emptying 9 is positioned at kettle 1 top, does not results in blocking in kettle 1 revolving reaction process.