CN207187135U - A kind of parallel rotating evaporates combined instrument - Google Patents
A kind of parallel rotating evaporates combined instrument Download PDFInfo
- Publication number
- CN207187135U CN207187135U CN201721040945.1U CN201721040945U CN207187135U CN 207187135 U CN207187135 U CN 207187135U CN 201721040945 U CN201721040945 U CN 201721040945U CN 207187135 U CN207187135 U CN 207187135U
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- China
- Prior art keywords
- parallel
- port valve
- combined instrument
- main frame
- parallel rotating
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model is applied to evaporimeter equipment technical field, there is provided a kind of parallel rotating evaporates combined instrument, including rotary evaporating device, regulating collecting device and parallel vaporising device；The rotary evaporating device includes revolving bottle, evaporating dish, the first port valve and rotation main frame；The revolving bottle is attached with the rotation main frame；The regulating collecting device includes threeway glass tube, receiving flask, condenser, the second port valve and vacuum tube；The threeway glass tube is attached respectively with receiving flask, condenser and vacuum tube；The parallel vaporising device includes vacuum cover, adapter, transfer plate, crystal frame and sample cell；First port valve is arranged on the revolving bottle and the rotation main frame junction；Second port valve is arranged on the threeway glass tube and the vacuum tube junction, and whereby, the utility model effectively shortens the operating time, improves conventional efficient, saves expense.
Description
Technical field
It the utility model is related to evaporimeter equipment technical field, more particularly to a kind of parallel rotating evaporation combined instrument.
Background technology
Rotary Evaporators be called rotary evaporator it mainly by：The part such as motor, cucurbit, heating kettle, condenser pipe group
Into laboratory common equipment, available for it is quick, leniently most samples are distilled, caused by the rotation of sample
Active force effectively suppresses the boiling of sample, but is once only capable of handling a sample simultaneously, less efficient.
Parallel evaporator can simultaneously the multiple samples of rapid evaporation, high boiling solvent sample can be handled.Plurality of specifications can be matched
Rack for test tube (4~96), single sample volume range is 0.5~500ml.Each test tube is independently connected on vacuum cover, no
Cross-contamination issue be present, but can not individually control, and evaporation efficiency is not high
Common Rotary Evaporators are only capable of handling a sample every time, and when handling batch samples, efficiency is low；It is parallel
Evaporimeter can handle multiple samples simultaneously, but can not individually control and evaporation efficiency is not high, handle multiple different concentration conditions
Sample when it is relatively inefficient.Two kinds of instruments have advantage and disadvantage.
In summary, prior art there will naturally be inconvenience and defect in actual use, and it is therefore necessary to improved.
Utility model content
For it is above-mentioned the defects of, the purpose of this utility model is to provide a kind of parallel rotating evaporation combined instrument, and it can be with
Saving expense, effectively shorten the operating time, improve conventional efficient.
To achieve these goals, the utility model provides a kind of parallel rotating evaporation combined instrument, including rotary evaporation dress
Put, regulating collecting device and parallel vaporising device；The rotary evaporating device includes revolving bottle, evaporating dish, the first port valve and rotation
Turn main frame；The revolving bottle is attached with the rotation main frame；The regulating collecting device includes threeway glass tube, collected
Bottle, condenser, the second port valve and vacuum tube；The threeway glass tube is attached respectively with receiving flask, condenser and vacuum tube；
The parallel vaporising device includes vacuum cover, adapter, transfer plate, crystal frame and sample cell.
According to parallel rotating of the present utility model evaporate combined instrument, first port valve be arranged on the revolving bottle with it is described
Rotate main frame junction.
Combined instrument is evaporated according to parallel rotating of the present utility model, the revolving bottle is located at the top of evaporating dish.
According to parallel rotating of the present utility model evaporate combined instrument, second port valve be arranged on the threeway glass tube with
The vacuum tube junction.
Combined instrument is evaporated according to parallel rotating of the present utility model, the condenser connects the rotation main frame.
Combined instrument is evaporated according to parallel rotating of the present utility model, the vacuum cover is located above the adapter.
Combined instrument is evaporated according to parallel rotating of the present utility model, the adapter connects the sample cell.
Combined instrument is evaporated according to parallel rotating of the present utility model, the sample cell is placed on the crystal frame.
The utility model provides a kind of parallel rotating evaporation combined instrument, including rotary evaporating device, regulating collecting device
With parallel vaporising device；The rotary evaporating device includes revolving bottle, evaporating dish, the first port valve and rotation main frame；The rotation
Bottle is attached with the rotation main frame；First port valve is arranged on the revolving bottle and the rotation main frame junction；Institute
State rotation main frame to be attached with condenser, just the rotary evaporating device and regulating collecting device are connected；The tune
Section collection device includes threeway glass tube, receiving flask, condenser, the second port valve and vacuum tube；The threeway glass tube is with collecting
Bottle, condenser and vacuum tube are attached respectively；The parallel vaporising device includes vacuum cover, adapter, transfer plate, crystal frame
And sample cell；The cooperation of the vacuum tube and vacuum cover connects regulating collecting device with parallel vaporising device.When independent
During using rotary evaporating device, the second port valve is closed, the first port valve is opened；When parallel vaporising device is used alone, by
One port valve is closed, and the second port valve is opened；During simultaneously using rotary evaporating device with parallel vaporising device, by the first port valve and second
Port valve is all opened.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Fig. 2 is the utility model partial structural diagram；
In figure, 1- rotary evaporating devices, 2- regulating collecting devices, the parallel vaporising devices of 3-, 11- evaporating dishes, 12- rotations
Rolling bottle, 13- rotation main frames, the port valves of 14- first, 21- threeway glass tubes, the port valves of 22- second, 23- condensers, 24- vacuum tubes,
25- receiving flasks, 31- vacuum covers, 32- adapters, 33- transfer plates, 34- crystal frames, 35- sample cells.
Embodiment
In order that the purpose of this utility model, technical scheme and advantage are more clearly understood, below in conjunction with accompanying drawing and implementation
Example, the utility model is further elaborated, it will be appreciated that specific embodiment described herein is only explaining
The utility model, it is not used to limit the utility model.
Referring to Fig. 1, the utility model provides a kind of parallel rotating evaporation combined instrument, including rotary evaporating device 1, tune
Save collection device 2 and parallel vaporising device 3；The rotary evaporating device includes revolving bottle 12, evaporating dish 11, the and of the first port valve 14
Rotate main frame 13；The revolving bottle 12 is attached with the rotation main frame 13；The regulating collecting device 2 includes threeway glass
Pipe 21, receiving flask 25, condenser 23, the second port valve 22 and vacuum tube 24；The threeway glass tube 21 and receiving flask 25, condensation
Device 23 and vacuum tube 24 are attached respectively；The parallel vaporising device includes vacuum cover 31, adapter 32, transfer plate 32, water
Mask pattern 34 and sample cell 35.First port valve 14 is arranged on the revolving bottle 12 and rotation main frame 13 junction, condenser 23
Rotation main frame 13 is connected to, the upper end of threeway glass tube 21 is connected with condenser 23, and lower end is connected with receiving flask 25.Vacuum tube one
End connection threeway glass tube 21, other end connection vacuum cover 31.When rotary evaporating device is used alone, the second port valve 22 is closed,
The first port valve 14 is opened, condensation cycle water is opened, fills water in evaporating dish 11 and be heated to required temperature.Parallel steaming is used alone
During transmitting apparatus, the first port valve 14 is closed, opens the second port valve 22, opens condensation cycle water, it is a certain amount of by being poured into crystal frame 34
Pure water, heated by required temperature.Sample pours into sample cell 35, and adapter 32 is screwed on sample cell 35；By sample cell
35 are put on transfer plate 35, it is ensured that it is in place；Ensure that transfer plate each position is all occupied by sample cell 35；Shut vacuum cover 31
And tighten.Adjust required rotating speed.During both combinations, the first port valve 14 and the second port valve 22 are opened, while use rotary evaporation
Device 1 and parallel vaporising device 3.
Preferably, parallel rotating evaporation combined instrument of the present utility model, first port valve 14 are arranged on the rotation
Bottle 12 and rotation main frame 13 junction.The revolving bottle 12 is located at the top of evaporating dish 11, and sample is evaporated.
In addition, parallel-Rotary Evaporators of the present utility model, second port valve 22 is arranged on the threeway glass tube 21
With the junction of vacuum tube 24.The condenser 23 connects the rotation main frame 13, enters condensation for the sample after evaporation
Device.
Preferably, parallel-Rotary Evaporators of the present utility model, the vacuum cover 31 are located at the top of adapter 32,
The adapter 32 connects the sample cell 35 and the vacuum cover 31, the species for control operation sample.
Further, parallel rotating evaporation combined instrument of the present utility model, the sample cell 35 are placed in the crystal frame 34
On, for fixing the position of sample cell.
Referring to Fig. 2, the threeway glass tube 21 of parallel rotating evaporation combined instrument of the present utility model is used for condenser 23, very
Blank pipe 24, the connection of receiving flask 25 so that parallel vaporising device 3 and rotary evaporating device 1 can be fitted close work.
In summary, the utility model provides a kind of parallel rotating evaporation combined instrument, including rotary evaporating device, regulation
Collection device and parallel vaporising device；The rotary evaporating device includes revolving bottle, evaporating dish, the first port valve and rotation main frame；
The revolving bottle is attached with the rotation main frame；First port valve is arranged on the revolving bottle and connected with the rotation main frame
Meet place；The rotation main frame is attached with condenser, and just the rotary evaporating device and regulating collecting device are connected；
The regulating collecting device includes threeway glass tube, receiving flask, condenser, the second port valve and vacuum tube；The threeway glass tube
It is attached respectively with receiving flask, condenser and vacuum tube；The parallel vaporising device include vacuum cover, adapter, transfer plate,
Crystal frame and sample cell；The cooperation of the vacuum tube and vacuum cover connects regulating collecting device with parallel vaporising device.
When rotary evaporating device is used alone, the second port valve is closed, the first port valve is opened；When the parallel vaporising device of exclusive use
When, the first port valve is closed, the second port valve is opened；During simultaneously using rotary evaporating device with parallel vaporising device, first is led to
Valve and the second port valve are all opened.
Certainly, the utility model can also have other various embodiments, without departing substantially from the utility model spirit and its essence
In the case of, those skilled in the art work as can make various corresponding changes and deformation according to the utility model, but these
Corresponding change and deformation should all belong to the scope of the claims appended by the utility model.
Claims (8)
1. a kind of parallel rotating evaporates combined instrument, it is characterised in that including rotary evaporating device, regulating collecting device and parallel steaming
Transmitting apparatus；
The rotary evaporating device includes revolving bottle, evaporating dish, the first port valve and rotation main frame；
The revolving bottle is attached with the rotation main frame；
The regulating collecting device includes threeway glass tube, receiving flask, condenser, the second port valve and vacuum tube；
The threeway glass tube is attached respectively with receiving flask, condenser and vacuum tube；
The parallel vaporising device includes vacuum cover, adapter, transfer plate, crystal frame and sample cell.
2. parallel rotating according to claim 1 evaporates combined instrument, it is characterised in that first port valve is arranged on described
Revolving bottle and the rotation main frame junction.
3. parallel rotating according to claim 1 evaporates combined instrument, it is characterised in that the revolving bottle is located at evaporating dish
Top.
4. parallel rotating according to claim 1 evaporates combined instrument, it is characterised in that second port valve is arranged on described
Threeway glass tube and the vacuum tube junction.
5. parallel rotating according to claim 1 evaporates combined instrument, it is characterised in that the condenser connects the rotation
Main frame.
6. parallel rotating according to claim 1 evaporates combined instrument, it is characterised in that the vacuum cover is located at the adaptation
Above device.
7. parallel rotating according to claim 1 evaporates combined instrument, it is characterised in that the adapter connects the sample
Pipe and the vacuum cover.
8. parallel rotating according to claim 1 evaporates combined instrument, it is characterised in that the sample cell is placed in the crystal
On frame.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721040945.1U CN207187135U (en) | 2017-08-19 | 2017-08-19 | A kind of parallel rotating evaporates combined instrument |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721040945.1U CN207187135U (en) | 2017-08-19 | 2017-08-19 | A kind of parallel rotating evaporates combined instrument |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207187135U true CN207187135U (en) | 2018-04-06 |
Family
ID=61794395
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721040945.1U Expired - Fee Related CN207187135U (en) | 2017-08-19 | 2017-08-19 | A kind of parallel rotating evaporates combined instrument |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207187135U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110548304A (en) * | 2019-09-07 | 2019-12-10 | 天津药明康德新药开发有限公司 | centrifugal concentrator for removing boiling point solvent |
-
2017
- 2017-08-19 CN CN201721040945.1U patent/CN207187135U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110548304A (en) * | 2019-09-07 | 2019-12-10 | 天津药明康德新药开发有限公司 | centrifugal concentrator for removing boiling point solvent |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180406 Termination date: 20200819 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |