CN206955646U - The retracting device of gaseous sulfur in carbon disulphide production - Google Patents
The retracting device of gaseous sulfur in carbon disulphide production Download PDFInfo
- Publication number
- CN206955646U CN206955646U CN201720541083.4U CN201720541083U CN206955646U CN 206955646 U CN206955646 U CN 206955646U CN 201720541083 U CN201720541083 U CN 201720541083U CN 206955646 U CN206955646 U CN 206955646U
- Authority
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- China
- Prior art keywords
- tank body
- sulphur
- tank
- inner chamber
- gaseous sulfur
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 95
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 title claims abstract description 77
- 229910052717 sulfur Inorganic materials 0.000 title claims abstract description 29
- 239000011593 sulfur Substances 0.000 title claims abstract description 29
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 23
- 239000005864 Sulphur Substances 0.000 claims abstract description 66
- 238000011084 recovery Methods 0.000 claims abstract description 6
- 239000002826 coolant Substances 0.000 claims description 18
- 238000001816 cooling Methods 0.000 claims description 18
- 239000010410 layer Substances 0.000 claims description 18
- 239000000110 cooling liquid Substances 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 13
- 230000003993 interaction Effects 0.000 claims description 6
- 239000011229 interlayer Substances 0.000 claims description 6
- 238000006477 desulfuration reaction Methods 0.000 claims description 2
- 230000023556 desulfurization Effects 0.000 claims description 2
- 230000002035 prolonged effect Effects 0.000 claims 3
- 238000010276 construction Methods 0.000 abstract description 4
- 238000012423 maintenance Methods 0.000 abstract description 4
- 235000001508 sulfur Nutrition 0.000 description 11
- 238000000034 method Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241000405070 Percophidae Species 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 244000144985 peep Species 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/02—Preparation of sulfur; Purification
- C01B17/027—Recovery of sulfur from material containing elemental sulfur, e.g. luxmasses or sulfur containing ores; Purification of the recovered sulfur
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
It the utility model is related to a kind of retracting device of gaseous sulfur in carbon disulphide production, including catching sulphur tank (1) and digester (5), catch sulphur tank (1) and be provided with overflow pipe (2), the overflow pipe (2) is reached in digester (5) from sulphur tank (1) bottom shape that is inclined upwardly is caught, sulphur tank (1) will be caught with digester (5) to be connected, the digester (5) is the cavity of a closing, the bottom of cavity is provided with back sulphur pipe (9), the top of cavity is provided with gaseous sulfur recovery tube (4), simultaneously, digester (5) is provided with heater (8).Compared with prior art, the utility model is simple in construction, is suitable for maintenance, can high efficiente callback gaseous sulfur or carbon disulfide gas, effectively prevent gaseous sulfur and part carbon disulfide gas uncontrollable discharge in carbon disulphide production.
Description
Technical field
The utility model belongs to carbon disulphide production technical field, specifically in a kind of carbon disulphide production gaseous sulfur or
The device of a small amount of carbon disulfide gas recovery.
Background technology
Semicoke formula carbon disulphide production method is a kind of highly developed production technology, and technique is simple, aboundresources, raw material
Source is wide, and cost is low, but seriously polluted, in molten sulphur, adds sulphur, whole open type operations in sweetening process, in the molten sulphur of high temperature and defeated
A large amount of gaseous sulfurs and part carbon disulfide gas uncontrollable discharge are caused during sending, pollute air, to operating personnel's body
Damage, be primary pollution source in semicoke method.
Therefore, it is a kind of it is simple in construction, easy to operate, be suitable for the high efficiente callback gaseous sulfur of maintenance or the dress of carbon disulfide gas
Put and arise at the historic moment.
The content of the invention
The purpose of this utility model is to provide a kind of high efficiente callback gaseous sulfur simple in construction, easy to operate, being suitable for maintenance
With the retracting device of gaseous sulfur in the carbon disulphide production of carbon disulfide gas.
The utility model includes catching sulphur tank (1) and digester (5), catches sulphur tank (1) and is provided with overflow pipe (2), the overflow pipe (2)
Reached from sulphur tank (1) bottom shape that is inclined upwardly is caught in digester (5), sulphur tank (1) will be caught and be connected with digester (5), it is described
Digester (5) is the cavity of a closing, and the bottom of cavity is provided with back sulphur pipe (9), and the top of cavity is provided with gaseous sulfur recovery tube
(4), meanwhile, digester (5) is provided with heater (8).
Further, the heater (8) of above-mentioned digester (5) is preferably sandwich-type dielectric heater, in encirclement shape
The interlayer of digester (5) periphery is arranged at, heat-conducting medium is provided with interlayer, such as steam or conduction oil, can make to enter digester
(5) sulphur or carbon disulfide keep certain temperature.
Yet further, above-mentioned overflow pipe (2) is exported, i.e., overflow pipe (2) outlet in digester (5) is preferably set
There is duck-beak type cover plate (7), the duck-beak type cover plate (7) is obliquely connected on overflow pipe (2) mouth of pipe, and duck-beak type cover plate
(7) upper end is be hinged with overflow pipe (2), on the one hand can prevent sulphur or the carbon disulfide refluence entered in digester (5), also
Water conservancy diversion can be carried out to the sulphur entered in digester (5).
Yet further, the above-mentioned overflow pipe (2) being in digester (5) is preferably telescoping tube (3), can adjust and catch sulphur
The liquid level of tank (1).
Yet further, above-mentioned sulphur tank (1) of catching includes tank body (12), air inlet (11) and gas outlet (15), tank body
(12) it is provided with inner chamber and catches sulphur plate (17) and heater (13), caught sulphur plate (17) and be provided with polylith, catches one end connection of sulphur plate (17)
In on tank body (12) inwall, the other end, which tilts down, to be extended in the middle part of tank body (12) inner chamber and is arranged in interaction shape, and described overflows
Flow tube (2) is provided with material receiving port (10), and material receiving port (10) is extend into tank body (12) from tank body (12) bottom, described tank
Body (12) is the cooling sandwith layer for having coolant, and cooling sandwith layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and shape
Into coolant circulation system.
Yet further, above-mentioned sulphur tank (1) of catching is preferably provided with automaton, includes master controller CPU and temperature
Detector Q, the coolant circulation system of cooling sandwith layer are provided with circulating pump M, and master controller CPU obtains tank by hygrosensor Q
The temperature information of body (12) inner chamber simultaneously at least controls circulating pump M, heater (13) according to the temperature information of tank body (12) inner chamber
Work.
Compared with prior art, the utility model is simple in construction, is suitable for maintenance, being capable of high efficiente callback gaseous sulfur or curing
Carbon gas, effectively prevent gaseous sulfur and part carbon disulfide gas uncontrollable discharge in carbon disulphide production.
Brief description of the drawings
Fig. 1 is the structural representation of the utility model embodiment 1.
Fig. 2 is the structural representation that Fig. 1 right sides regard.
Fig. 3 is the structural representation of the utility model embodiment 2.
Shown in figure:1 is catches sulphur tank, and 2 be overflow pipe, and 3 be telescoping tube, and 4 be gaseous sulfur recovery tube, and 5 be digester, and 6 are
Peep hole, 7 be duck-beak type cover plate, and 8 be heater, and 9 are back sulphur pipe, and 10 be material receiving port, and 11 be air inlet, and 12 be tank body, 13
It is cooling liquid inlet for heater, 14,15 be gas outlet, and 16 be air-introduced machine, and 17 is catch sulphur plate, and 18 be slag notch, and 19 be cooling
Liquid exports.
Embodiment
The following detailed description of preferred embodiment of the present utility model.
Embodiment 1:Reference picture 1-2, is the structural representation of the utility model embodiment 1, including catches sulphur tank 1 and digester
5, catch sulphur tank 1 and be provided with overflow pipe 2, the overflow pipe 2 is reached in digester 5 from the bottom of sulphur tank 1 shape that is inclined upwardly is caught, and will catch sulphur tank
1 is connected with digester 5, and the digester 5 is the cavity of a closing, and the bottom of cavity is provided with go back to sulphur pipe (9), the top of cavity
Provided with gaseous sulfur recovery tube (4), meanwhile, digester 5 is provided with heater 8, and the heater 8 of the digester 5 is sandwich-type
Dielectric heater, to be arranged at the interlayer of the lower periphery of digester 5 in surrounding shape, heat-conducting medium is provided with interlayer, such as steam or
Conduction oil, it can make to enter the sulphur of digester 5 or carbon disulfide keeps certain temperature, described overflow pipe 2 exports, i.e., in desulfurization
The outlet of overflow pipe 2 in tank 5 is provided with duck-beak type cover plate 7, and the duck-beak type cover plate 7 is obliquely connected on the mouth of pipe of overflow pipe 2, and
And the upper end of duck-beak type cover plate 7 is be hinged with overflow pipe 2, bottom is in duckbill, on the one hand can prevent from entering in digester 5
Sulphur or carbon disulfide flow backwards, can also to enter digester 5 in sulphur carry out water conservancy diversion, it is described be in digester 5 in overflow pipe 2
For telescoping tube 3, the liquid level for catching sulphur tank 1 can be adjusted.
Embodiment 2:Reference picture 3, it is the structural representation of the embodiment of the present invention 2, compared with Example 1, the present embodiment
The main distinction is:Described sulphur tank 1 of catching includes tank body 12, air inlet 11 and gas outlet 15, is provided with the inner chamber of tank body 12 and catches sulphur
Plate 17, slag notch 18 and heater 13, gas outlet 15 are provided with air-introduced machine 16, and the sulphur plate 17 of catching is provided with polylith, catches sulphur plate 17
One end is connected on the inwall of tank body 12, and the other end, which tilts down, to be extended in the middle part of the inner chamber of tank body 12 and arranged in interaction shape, described
Overflow pipe 2 be provided with material receiving port 10, and material receiving port 10 is extend into tank body 12 from the bottom of tank body 12, and described tank body 12 is
There is the cooling sandwith layer of coolant, cooling sandwith layer is at least provided with cooling liquid inlet 14 and cooling liquid outlet 19 and forms coolant circulation
System, and automaton is provided with, include master controller CPU and hygrosensor Q, the coolant circulation system of cooling sandwith layer
Provided with circulating pump M, master controller CPU obtains the temperature information of the inner chamber of tank body 12 and according in tank body 12 by hygrosensor Q
The temperature information of chamber at least controls circulating pump M, heater 13 work.Catching sulphur tank 1 and can make to catch all the time by the present embodiment
Temperature in sulphur tank 1 is held constant within the scope of one, is greatly promoted and is caught sulphur effect.
Above-described is only preferred embodiment of the present utility model, it is noted that for the ordinary skill of this area
For personnel, without departing from the concept of the premise of the invention, some changes and improvements can also be made, these belong to this
The protection domain of utility model.
Claims (13)
1. the retracting device of gaseous sulfur in a kind of carbon disulphide production, including catch sulphur tank (1) and digester (5), it is characterised in that:
To catch sulphur tank (1) and be provided with overflow pipe (2), the overflow pipe (2) is reached in digester (5) from sulphur tank (1) bottom shape that is inclined upwardly is caught,
Sulphur tank (1) will be caught with digester (5) to be connected, the digester (5) is the cavity of a closing, and the bottom of cavity is provided with back sulphur pipe
(9), the top of cavity is provided with gaseous sulfur recovery tube (4), meanwhile, digester (5) is provided with heater (8).
2. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 1, it is characterised in that the digester
(5) heater (8) is sandwich-type dielectric heater, in the interlayer for surrounding shape and being arranged at digester (5) periphery, in interlayer
Provided with heat-conducting medium.
3. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 1 or 2, it is characterised in that described overflows
Flow tube (2) exports, i.e., overflow pipe (2) outlet in digester (5) is provided with duck-beak type cover plate (7), the duck-beak type cover plate (7)
Obliquely it is connected on overflow pipe (2) mouth of pipe, and duck-beak type cover plate (7) upper end and overflow pipe (2) are be hinged.
4. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 1 or 2, it is characterised in that described to be in
Overflow pipe (2) in digester (5) is telescoping tube (3).
5. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 3, it is characterised in that described to be in desulfurization
Overflow pipe (2) in tank (5) is telescoping tube (3).
6. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 1 or 2, it is characterised in that described catches
Sulphur tank (1) includes tank body (12), air inlet (11) and gas outlet (15), is provided with tank body (12) inner chamber and catches sulphur plate (17) and heat
Device (13), catch sulphur plate (17) and be provided with polylith, the one end for catching sulphur plate (17) is connected on tank body (12) inwall, and the other end tilts down
Extend in the middle part of tank body (12) inner chamber and arranged in interaction shape, described overflow pipe (2) is provided with material receiving port (10), and material receiving port
(10) it is extend into from tank body (12) bottom in tank body (12), described tank body (12) is the cooling sandwith layer for having coolant, and cooling is pressed from both sides
Layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and forms coolant circulation system.
7. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 3, it is characterised in that described catches sulphur tank
(1) comprising tank body (12), air inlet (11) and gas outlet (15), provided with catching sulphur plate (17) and heater in tank body (12) inner chamber
(13), catch sulphur plate (17) and be provided with polylith, the one end for catching sulphur plate (17) is connected on tank body (12) inwall, and the other end, which tilts down, to be prolonged
Reach in the middle part of tank body (12) inner chamber and arranged in interaction shape, described overflow pipe (2) is provided with material receiving port (10), and material receiving port
(10) it is extend into from tank body (12) bottom in tank body (12), described tank body (12) is the cooling sandwith layer for having coolant, and cooling is pressed from both sides
Layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and forms coolant circulation system.
8. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 4, it is characterised in that described catches sulphur tank
(1) comprising tank body (12), air inlet (11) and gas outlet (15), provided with catching sulphur plate (17) and heater in tank body (12) inner chamber
(13), catch sulphur plate (17) and be provided with polylith, the one end for catching sulphur plate (17) is connected on tank body (12) inwall, and the other end, which tilts down, to be prolonged
Reach in the middle part of tank body (12) inner chamber and arranged in interaction shape, described overflow pipe (2) is provided with material receiving port (10), and material receiving port
(10) it is extend into from tank body (12) bottom in tank body (12), described tank body (12) is the cooling sandwith layer for having coolant, and cooling is pressed from both sides
Layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and forms coolant circulation system.
9. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 5, it is characterised in that described catches sulphur tank
(1) comprising tank body (12), air inlet (11) and gas outlet (15), provided with catching sulphur plate (17) and heater in tank body (12) inner chamber
(13), catch sulphur plate (17) and be provided with polylith, the one end for catching sulphur plate (17) is connected on tank body (12) inwall, and the other end, which tilts down, to be prolonged
Reach in the middle part of tank body (12) inner chamber and arranged in interaction shape, described overflow pipe (2) is provided with material receiving port (10), and material receiving port
(10) it is extend into from tank body (12) bottom in tank body (12), described tank body (12) is the cooling sandwith layer for having coolant, and cooling is pressed from both sides
Layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and forms coolant circulation system.
10. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 6, it is characterised in that described catches sulphur
Tank (1) is provided with automaton, and comprising master controller CPU and hygrosensor Q, the coolant circulation system of cooling sandwith layer is set
There are circulating pump M, master controller CPU to obtain the temperature information of tank body (12) inner chamber and according to tank body (12) by hygrosensor Q
The temperature information of inner chamber at least controls circulating pump M, heater (13) work.
11. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 7, it is characterised in that described catches sulphur
Tank (1) is provided with automaton, and comprising master controller CPU and hygrosensor Q, the coolant circulation system of cooling sandwith layer is set
There are circulating pump M, master controller CPU to obtain the temperature information of tank body (12) inner chamber and according to tank body (12) by hygrosensor Q
The temperature information of inner chamber at least controls circulating pump M, heater (13) work.
12. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 8, it is characterised in that described catches sulphur
Tank (1) is provided with automaton, and comprising master controller CPU and hygrosensor Q, the coolant circulation system of cooling sandwith layer is set
There are circulating pump M, master controller CPU to obtain the temperature information of tank body (12) inner chamber and according to tank body (12) by hygrosensor Q
The temperature information of inner chamber at least controls circulating pump M, heater (13) work.
13. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 9, it is characterised in that described catches sulphur
Tank (1) is provided with automaton, and comprising master controller CPU and hygrosensor Q, the coolant circulation system of cooling sandwith layer is set
There are circulating pump M, master controller CPU to obtain the temperature information of tank body (12) inner chamber and according to tank body (12) by hygrosensor Q
The temperature information of inner chamber at least controls circulating pump M, heater (13) work.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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CN201621328397 | 2016-12-06 | ||
CN2016213283978 | 2016-12-06 |
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CN206955646U true CN206955646U (en) | 2018-02-02 |
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ID=59727785
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CN201710343917.5A Pending CN107117615A (en) | 2016-12-06 | 2017-05-16 | The retracting device of gaseous sulfur in carbon disulphide production |
CN201720541083.4U Active CN206955646U (en) | 2016-12-06 | 2017-05-16 | The retracting device of gaseous sulfur in carbon disulphide production |
Family Applications Before (1)
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CN201710343917.5A Pending CN107117615A (en) | 2016-12-06 | 2017-05-16 | The retracting device of gaseous sulfur in carbon disulphide production |
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CN (2) | CN107117615A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107117615A (en) * | 2016-12-06 | 2017-09-01 | 张贯彪 | The retracting device of gaseous sulfur in carbon disulphide production |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN2330640Y (en) * | 1997-12-27 | 1999-07-28 | 李清水 | Vapor-free desulfurizing reaction furnace for producing carbon bisulfide |
CN202880878U (en) * | 2012-10-16 | 2013-04-17 | 嵩县开拓者钼业有限公司 | Equipment for preparing sulfur from sulfur steam |
CN202962262U (en) * | 2012-11-30 | 2013-06-05 | 北京三聚创洁科技发展有限公司 | Desulfurization device |
CN104016344B (en) * | 2013-03-01 | 2016-02-10 | 辽宁瑞兴化工集团有限公司 | The method of hydrogen sulfide hydrate is avoided the formation of in a kind of carbon disulphide production process |
CN203959829U (en) * | 2014-06-16 | 2014-11-26 | 成都丽雅纤维股份有限公司 | Separating tank for process for preparation of CS 2 molten sulfur |
CN105293493B (en) * | 2015-11-20 | 2017-10-17 | 张贯彪 | Sulphur device is caught used in carbon disulphide production |
CN107117615A (en) * | 2016-12-06 | 2017-09-01 | 张贯彪 | The retracting device of gaseous sulfur in carbon disulphide production |
-
2017
- 2017-05-16 CN CN201710343917.5A patent/CN107117615A/en active Pending
- 2017-05-16 CN CN201720541083.4U patent/CN206955646U/en active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107117615A (en) * | 2016-12-06 | 2017-09-01 | 张贯彪 | The retracting device of gaseous sulfur in carbon disulphide production |
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Effective date of registration: 20181107 Address after: 457000 Puxian Industrial Park, fan County Industrial Agglomeration Area, Puyang, Henan Patentee after: Puyang Tianhong Industry Co., Ltd. Address before: 833400 Quxinhua Transfer of Office Building of Tianshan Street No.8 Party and Government Service Center, Alashankou City, Bortala Mongolian Autonomous Prefecture, Xinjiang Uygur Autonomous Region Patentee before: Zhang Guanbiao |
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