CN107117615A - The retracting device of gaseous sulfur in carbon disulphide production - Google Patents
The retracting device of gaseous sulfur in carbon disulphide production Download PDFInfo
- Publication number
- CN107117615A CN107117615A CN201710343917.5A CN201710343917A CN107117615A CN 107117615 A CN107117615 A CN 107117615A CN 201710343917 A CN201710343917 A CN 201710343917A CN 107117615 A CN107117615 A CN 107117615A
- Authority
- CN
- China
- Prior art keywords
- tank body
- sulphur
- tank
- digester
- gaseous sulfur
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 89
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 title claims abstract description 71
- 229910052717 sulfur Inorganic materials 0.000 title claims abstract description 26
- 239000011593 sulfur Substances 0.000 title claims abstract description 26
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 20
- 239000005864 Sulphur Substances 0.000 claims abstract description 63
- 238000011084 recovery Methods 0.000 claims abstract description 5
- 239000002826 coolant Substances 0.000 claims description 15
- 238000001816 cooling Methods 0.000 claims description 15
- 239000010410 layer Substances 0.000 claims description 15
- 239000000110 cooling liquid Substances 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 13
- 230000003993 interaction Effects 0.000 claims description 6
- 239000011229 interlayer Substances 0.000 claims description 6
- 238000006477 desulfuration reaction Methods 0.000 claims description 2
- 230000023556 desulfurization Effects 0.000 claims description 2
- 230000002035 prolonged effect Effects 0.000 claims 3
- 238000010276 construction Methods 0.000 abstract description 4
- 238000012423 maintenance Methods 0.000 abstract description 4
- 235000001508 sulfur Nutrition 0.000 description 11
- 238000000034 method Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000405070 Percophidae Species 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 244000144985 peep Species 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/02—Preparation of sulfur; Purification
- C01B17/027—Recovery of sulfur from material containing elemental sulfur, e.g. luxmasses or sulfur containing ores; Purification of the recovered sulfur
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
The present invention relates to a kind of retracting device of gaseous sulfur in carbon disulphide production, including catching sulphur tank (1) and digester (5), sulphur tank (1) is caught provided with overflow pipe (2), the overflow pipe (2) is reached in digester (5) from sulphur tank (1) bottom shape that is inclined upwardly is caught, sulphur tank (1) will be caught with digester (5) to be connected, the digester (5) is the cavity of a closing, the bottom of cavity is provided with back sulphur pipe (9), the top of cavity is provided with gaseous sulfur recovery tube (4), simultaneously, digester (5) is provided with heater (8).Compared with prior art, the present invention it is simple in construction, be suitable for maintenance, can high efficiente callback gaseous sulfur or carbon disulfide gas, effectively prevent gaseous sulfur and part carbon disulfide gas uncontrollable discharge in carbon disulphide production.
Description
Technical field
The invention belongs to carbon disulphide production technical field, a kind of specifically gaseous sulfur or a small amount of in carbon disulphide production
The device that carbon disulfide gas is reclaimed.
Background technology
Semicoke formula carbon disulphide production method is a kind of highly developed production technology, and technique is simple, aboundresources, raw material
Source is wide, and cost is low, but seriously polluted, whole open type operations in molten sulphur, plus sulphur, sweetening process, in the molten sulphur of high temperature and defeated
A large amount of gaseous sulfurs and part carbon disulfide gas uncontrollable discharge are caused during sending, air is polluted, to operating personnel's body
Damage, be primary pollution source in semicoke method.
Therefore, it is a kind of it is simple in construction, easy to operate, be suitable for the high efficiente callback gaseous sulfur of maintenance or the dress of carbon disulfide gas
Put and arise at the historic moment.
The content of the invention
It is an object of the invention to provide a kind of high efficiente callback gaseous sulfur and two simple in construction, easy to operate, being suitable for maintenance
The retracting device of gaseous sulfur in the carbon disulphide production of nitric sulfid gas.
The present invention includes catching sulphur tank (1) and digester (5), catches sulphur tank (1) and is provided with overflow pipe (2), the overflow pipe (2) is from catching
Sulphur tank (1) bottom shape that is inclined upwardly is reached in digester (5), will be caught sulphur tank (1) and is connected with digester (5), the desulfurization
Tank (5) is the cavity of a closing, and the bottom of cavity is provided with back sulphur pipe (9), and the top of cavity is provided with gaseous sulfur recovery tube (4), together
When, digester (5) is provided with heater (8).
Further, the heater (8) of above-mentioned digester (5) is preferably sandwich-type dielectric heater, in encirclement shape
It is arranged in the interlayer of digester (5) periphery, interlayer and is provided with heat-conducting medium, such as steam or conduction oil can makes to enter digester
(5) sulphur or carbon disulfide keep certain temperature.
Yet further, above-mentioned overflow pipe (2) is exported, i.e., overflow pipe (2) outlet in digester (5) is preferably set
There is duck-beak type cover plate (7), the duck-beak type cover plate (7) is obliquely connected on overflow pipe (2) mouth of pipe, and duck-beak type cover plate
(7) upper end is hinged with overflow pipe (2), on the one hand can be prevented the sulphur or carbon disulfide that enter in digester (5) from flowing backwards, may be used also
Water conservancy diversion is carried out to the sulphur entered in digester (5).
Yet further, the above-mentioned overflow pipe (2) being in digester (5) is preferably telescoping tube (3), can adjust and catch
The liquid level of sulphur tank (1).
Yet further, above-mentioned sulphur tank (1) of catching includes tank body (12), air inlet (11) and gas outlet (15), tank body
(12) provided with sulphur plate (17) and heater (13) is caught in inner chamber, sulphur plate (17) is caught provided with polylith, one end connection of sulphur plate (17) is caught
In on tank body (12) inwall, the other end, which is tilted down, to be extended in the middle part of tank body (12) inner chamber and in interaction shape arrangement, and described overflows
Flow tube (2) is provided with material receiving port (10), and material receiving port (10) is extend into tank body (12) from tank body (12) bottom, described tank body
(12) to there is the cooling sandwith layer of coolant, cooling sandwith layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and is formed
Coolant circulation system.
Yet further, above-mentioned sulphur tank (1) of catching is preferably provided with automaton, includes master controller CPU and temperature
Detector Q, the coolant circulation system of cooling sandwith layer is provided with circulating pump M, and master controller CPU obtains tank by hygrosensor Q
The temperature information of body (12) inner chamber simultaneously at least controls circulating pump M, heater (13) according to the temperature information of tank body (12) inner chamber
Work.
Compared with prior art, the present invention is simple in construction, be suitable for maintenance, being capable of high efficiente callback gaseous sulfur or carbon disulfide gas
Body, effectively prevents gaseous sulfur and part carbon disulfide gas uncontrollable discharge in carbon disulphide production.
Brief description of the drawings
Fig. 1 is the structural representation of the embodiment of the present invention 1.
Fig. 2 is the structural representation that Fig. 1 right sides are regarded.
Fig. 3 is the structural representation of the embodiment of the present invention 2.
Shown in figure：1 is catches sulphur tank, and 2 be overflow pipe, and 3 be telescoping tube, and 4 be gaseous sulfur recovery tube, and 5 be digester, and 6 are
Peep hole, 7 be duck-beak type cover plate, and 8 be heater, and 9 are back sulphur pipe, and 10 be material receiving port, and 11 be air inlet, and 12 be tank body, 13
It is cooling liquid inlet for heater, 14,15 be gas outlet, and 16 be air-introduced machine, and 17 is catch sulphur plate, and 18 be slag notch, and 19 be cooling
Liquid is exported.
Embodiment
The following detailed description of the preferred embodiment of the present invention.
Embodiment 1：Reference picture 1-2, is the structural representation of the embodiment of the present invention 1, including catches sulphur tank 1 and digester 5, catches
Sulphur tank 1 is provided with overflow pipe 2, and the overflow pipe 2 is reached in digester 5 from the bottom of sulphur tank 1 shape that is inclined upwardly is caught, will catch sulphur tank 1 with
Digester 5 is connected, and the digester 5 is the cavity of a closing, and the bottom of cavity is provided with back sulphur pipe (9), and the top of cavity is set
There is gaseous sulfur recovery tube (4), meanwhile, digester 5 is provided with heater 8, and the heater 8 of the digester 5 is situated between for sandwich-type
Matter heater, to be provided with heat-conducting medium in surrounding shape and be arranged in the interlayer of the lower periphery of digester 5, interlayer, such as steam or leads
Deep fat, can make to enter the sulphur of digester 5 or carbon disulfide keeps certain temperature, described overflow pipe 2 is exported, i.e., in digester
The outlet of overflow pipe 2 in 5 is provided with duck-beak type cover plate 7, and the duck-beak type cover plate 7 is obliquely connected on the mouth of pipe of overflow pipe 2, and
The upper end of duck-beak type cover plate 7 is hinged with overflow pipe 2, and bottom is in duckbill, on the one hand can prevent the sulphur entered in digester 5
Or carbon disulfide flows backwards, can also water conservancy diversion be carried out to the sulphur entered in digester 5, the overflow pipe 2 in digester 5 is
Telescoping tube 3, can adjust the liquid level for catching sulphur tank 1.
Embodiment 2：Reference picture 3, is the structural representation of the embodiment of the present invention 2, compared with Example 1, the present embodiment
The main distinction is：Described sulphur tank 1 of catching is included in tank body 12, air inlet 11 and gas outlet 15, the inner chamber of tank body 12 provided with catching sulphur
Plate 17, slag notch 18 and heater 13, gas outlet 15 are provided with air-introduced machine 16, and the sulphur plate 17 of catching catches sulphur plate 17 provided with polylith
One end is connected on the inwall of tank body 12, and the other end, which is tilted down, to be extended in the middle part of the inner chamber of tank body 12 and in interaction shape arrangement, described
Overflow pipe 2 be provided with material receiving port 10, and material receiving port 10 extend into tank body 12 from the bottom of tank body 12, and described tank body 12 is has
The cooling sandwith layer of coolant, cooling sandwith layer is at least provided with cooling liquid inlet 14 and cooling liquid outlet 19 and forms coolant cyclic system
System, and provided with automaton, comprising master controller CPU and hygrosensor Q, the coolant circulation system of cooling sandwith layer is set
There are circulating pump M, master controller CPU to obtain the temperature information of the inner chamber of tank body 12 and according to the inner chamber of tank body 12 by hygrosensor Q
Temperature information at least control circulating pump M, the work of heater 13.Catching sulphur tank 1 and can make to catch sulphur all the time by the present embodiment
Temperature in tank 1 is held constant within the scope of one, is greatly promoted and is caught sulphur effect.
Above-described is only the preferred embodiment of the present invention, it is noted that for one of ordinary skill in the art
For, without departing from the concept of the premise of the invention, some changes and improvements can also be made, these belong to the present invention
Protection domain.
Claims (10)
1. the retracting device of gaseous sulfur in a kind of carbon disulphide production, including catch sulphur tank (1) and digester (5), it is characterised in that：
Sulphur tank (1) is caught provided with overflow pipe (2), the overflow pipe (2) is reached in digester (5) from sulphur tank (1) bottom shape that is inclined upwardly is caught,
Sulphur tank (1) will be caught with digester (5) to be connected, the digester (5) is the cavity of a closing, and the bottom of cavity is provided with back sulphur pipe
(9), the top of cavity is provided with gaseous sulfur recovery tube (4), meanwhile, digester (5) is provided with heater (8).
2. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 1, it is characterised in that the digester
(5) heater (8) is sandwich-type dielectric heater, to be arranged in encirclement shape in the interlayer of digester (5) periphery, interlayer
Provided with heat-conducting medium.
3. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 1 or 2, it is characterised in that described overflows
Flow tube (2) is exported, i.e., overflow pipe (2) outlet in digester (5) is provided with duck-beak type cover plate (7), the duck-beak type cover plate (7)
Obliquely it is connected on overflow pipe (2) mouth of pipe, and duck-beak type cover plate (7) upper end is hinged with overflow pipe (2).
4. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 1 or 2, it is characterised in that described to be in
Overflow pipe (2) in digester (5) is telescoping tube (3).
5. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 3, it is characterised in that described to be in desulfurization
Overflow pipe (2) in tank (5) is telescoping tube (3).
6. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 1 or 2, it is characterised in that described catches
Sulphur tank (1) is included in tank body (12), air inlet (11) and gas outlet (15), tank body (12) inner chamber provided with catching sulphur plate (17) and heat
Device (13), catches sulphur plate (17) provided with polylith, the one end for catching sulphur plate (17) is connected on tank body (12) inwall, and the other end is tilted down
Extend in the middle part of tank body (12) inner chamber and in interaction shape arrangement, described overflow pipe (2) is provided with material receiving port (10), and material receiving port
(10) it is extend into from tank body (12) bottom in tank body (12), described tank body (12) is the cooling sandwith layer for having coolant, cooling folder
Layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and forms coolant circulation system.
7. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 3, it is characterised in that described catches sulphur tank
(1) comprising tank body (12), air inlet (11) and gas outlet (15), it is provided with tank body (12) inner chamber and catches sulphur plate (17) and heater
(13) sulphur plate (17), is caught provided with polylith, and the one end for catching sulphur plate (17) is connected on tank body (12) inwall, and the other end, which is tilted down, to be prolonged
Reach in the middle part of tank body (12) inner chamber and in interaction shape arrangement, described overflow pipe (2) is provided with material receiving port (10), and material receiving port
(10) it is extend into from tank body (12) bottom in tank body (12), described tank body (12) is the cooling sandwith layer for having coolant, cooling folder
Layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and forms coolant circulation system.
8. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 4, it is characterised in that described catches sulphur tank
(1) comprising tank body (12), air inlet (11) and gas outlet (15), it is provided with tank body (12) inner chamber and catches sulphur plate (17) and heater
(13) sulphur plate (17), is caught provided with polylith, and the one end for catching sulphur plate (17) is connected on tank body (12) inwall, and the other end, which is tilted down, to be prolonged
Reach in the middle part of tank body (12) inner chamber and in interaction shape arrangement, described overflow pipe (2) is provided with material receiving port (10), and material receiving port
(10) it is extend into from tank body (12) bottom in tank body (12), described tank body (12) is the cooling sandwith layer for having coolant, cooling folder
Layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and forms coolant circulation system.
9. the retracting device of gaseous sulfur in carbon disulphide production as claimed in claim 5, it is characterised in that described catches sulphur tank
(1) comprising tank body (12), air inlet (11) and gas outlet (15), it is provided with tank body (12) inner chamber and catches sulphur plate (17) and heater
(13) sulphur plate (17), is caught provided with polylith, and the one end for catching sulphur plate (17) is connected on tank body (12) inwall, and the other end, which is tilted down, to be prolonged
Reach in the middle part of tank body (12) inner chamber and in interaction shape arrangement, described overflow pipe (2) is provided with material receiving port (10), and material receiving port
(10) it is extend into from tank body (12) bottom in tank body (12), described tank body (12) is the cooling sandwith layer for having coolant, cooling folder
Layer is at least provided with cooling liquid inlet (14) and cooling liquid outlet (19) and forms coolant circulation system.
10. the retracting device of gaseous sulfur in the carbon disulphide production as described in claim any one of 6-9, it is characterised in that institute
That states catches sulphur tank (1) provided with automaton, and comprising master controller CPU and hygrosensor Q, the coolant of cooling sandwith layer is followed
Loop system is provided with circulating pump M, and master controller CPU obtains the temperature information and basis of tank body (12) inner chamber by hygrosensor Q
The temperature information of tank body (12) inner chamber at least controls circulating pump M, the work of heater (13).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621328397 | 2016-12-06 | ||
| CN2016213283978 | 2016-12-06 |
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| Publication Number | Publication Date |
|---|---|
| CN107117615A true CN107117615A (en) | 2017-09-01 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720541083.4U Active CN206955646U (en) | 2016-12-06 | 2017-05-16 | The retracting device of gaseous sulfur in carbon disulphide production |
| CN201710343917.5A Pending CN107117615A (en) | 2016-12-06 | 2017-05-16 | The retracting device of gaseous sulfur in carbon disulphide production |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720541083.4U Active CN206955646U (en) | 2016-12-06 | 2017-05-16 | The retracting device of gaseous sulfur in carbon disulphide production |
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| Country | Link |
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| CN (2) | CN206955646U (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN206955646U (en) * | 2016-12-06 | 2018-02-02 | 张贯彪 | The retracting device of gaseous sulfur in carbon disulphide production |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2330640Y (en) * | 1997-12-27 | 1999-07-28 | 李清水 | Vapor-free desulfurizing reaction furnace for producing carbon bisulfide |
| CN202880878U (en) * | 2012-10-16 | 2013-04-17 | 嵩县开拓者钼业有限公司 | Equipment for preparing sulfur from sulfur steam |
| CN202962262U (en) * | 2012-11-30 | 2013-06-05 | 北京三聚创洁科技发展有限公司 | Desulfurization device |
| CN104016344A (en) * | 2013-03-01 | 2014-09-03 | 辽宁瑞兴化工集团有限公司 | Method for avoiding forming hydrogen sulfide hydrate in carbon bisulfide production process |
| CN203959829U (en) * | 2014-06-16 | 2014-11-26 | 成都丽雅纤维股份有限公司 | Separating tank for process for preparation of CS 2 molten sulfur |
| CN105293493A (en) * | 2015-11-20 | 2016-02-03 | 张贯彪 | Sulfur catcher used in carbon disulfide production |
| CN206955646U (en) * | 2016-12-06 | 2018-02-02 | 张贯彪 | The retracting device of gaseous sulfur in carbon disulphide production |
-
2017
- 2017-05-16 CN CN201720541083.4U patent/CN206955646U/en active Active
- 2017-05-16 CN CN201710343917.5A patent/CN107117615A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2330640Y (en) * | 1997-12-27 | 1999-07-28 | 李清水 | Vapor-free desulfurizing reaction furnace for producing carbon bisulfide |
| CN202880878U (en) * | 2012-10-16 | 2013-04-17 | 嵩县开拓者钼业有限公司 | Equipment for preparing sulfur from sulfur steam |
| CN202962262U (en) * | 2012-11-30 | 2013-06-05 | 北京三聚创洁科技发展有限公司 | Desulfurization device |
| CN104016344A (en) * | 2013-03-01 | 2014-09-03 | 辽宁瑞兴化工集团有限公司 | Method for avoiding forming hydrogen sulfide hydrate in carbon bisulfide production process |
| CN203959829U (en) * | 2014-06-16 | 2014-11-26 | 成都丽雅纤维股份有限公司 | Separating tank for process for preparation of CS 2 molten sulfur |
| CN105293493A (en) * | 2015-11-20 | 2016-02-03 | 张贯彪 | Sulfur catcher used in carbon disulfide production |
| CN206955646U (en) * | 2016-12-06 | 2018-02-02 | 张贯彪 | The retracting device of gaseous sulfur in carbon disulphide production |
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|---|---|
| CN206955646U (en) | 2018-02-02 |
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| TA01 | Transfer of patent application right |
Effective date of registration: 20181127 Address after: 457000 Puxian Industrial Park, fan County Industrial Agglomeration Area, Puyang, Henan Applicant after: PUYANG TIANHONG INDUSTRIAL Co.,Ltd. Address before: 833400 Quxinhua Transfer of Office Building of Tianshan Street No.8 Party and Government Service Center, Alashankou City, Bortala Mongolian Autonomous Prefecture, Xinjiang Uygur Autonomous Region Applicant before: Zhang Guanbiao |
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Application publication date: 20170901 |
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