CN206853659U - A kind of reactor of dichloromethane - Google Patents
A kind of reactor of dichloromethane Download PDFInfo
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- CN206853659U CN206853659U CN201720429369.3U CN201720429369U CN206853659U CN 206853659 U CN206853659 U CN 206853659U CN 201720429369 U CN201720429369 U CN 201720429369U CN 206853659 U CN206853659 U CN 206853659U
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- filter
- screen pack
- reactor
- reactor housing
- heating rod
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Abstract
The utility model discloses a kind of reactor of dichloromethane, a kind of controllability when aiming to provide heating is good, the reactor of good filtration effect and safety, its drip irrigation device be reactor housing be externally provided with heater and be arranged at into, filter in discharging opening, heater includes heating rod, for installing the mounting assembly of heating rod and the drive device for driving heating rod to work, filter include be respectively arranged at into, first filter and the second filter in discharging opening and the support component being arranged in first filter, the utility model is applied to reactor technical field.
Description
Technical field
A kind of reactor technical field is the utility model is related to, more specifically, it relates to a kind of reaction of dichloromethane
Kettle.
Background technology
Dichloromethane is mainly used in film production and field of medicaments in China.The consumption figure for being wherein used for film production accounts for always
The 50% of consumption figure, medicine aspect account for the 20% of aggregate consumption, and cleaning agent and chemical industry consumption figure account for the 20% of aggregate consumption, its
He accounts for 10% at aspect.Dichloromethane, which is also used in industrial refrigeration system, is used as refrigerating medium use.
At present, in the market be used for prepare the reactor of dichloromethane, it include reactor housing, charging aperture, discharging opening,
Agitator, the motor for driving agitator rotation and the fixed support for fixing motor.Traditional reactor is used
Heater be to be heated by steam pipe, the controllability of such mode of heating is poor, it is not easy to lasting holding one
Fixed temperature, and traditional reactor does not all take filtering when preparing dichloromethane in charging aperture and discharging opening, therefore
When being processed preparation, reaction speed on the one hand can be influenceed, on the other hand can influence to prepare degree of purity, by being included in discharging
Mouthful when do not filtered can also influence dichloromethane prepare degree of purity.
Utility model content
In view of the deficienciess of the prior art, controllability when the purpose of this utility model is to provide a kind of heating is good,
The reactor of good filtration effect and safety.
To achieve the above object, the utility model provides following technical scheme：A kind of reactor of dichloromethane, including
Reactor housing, charging aperture, discharging opening, agitator, for drive agitator rotate motor and for fixing consolidating for motor
Fixed rack, the charging aperture are arranged on reactor housing upper, and discharging opening is arranged on the bottom of reactor housing, agitator one end
Stretch into reactor housing, other end stretch out reactor housing and and motor connection, it is characterized in that：Outside the reactor housing
Provided with heater and the intraoral filter of charging and discharging is arranged at, heater includes heating rod, for installing heating rod
Mounting assembly and the drive device for driving heating rod to work, filter include that to be respectively arranged at charging and discharging intraoral
First filter and the second filter and the support component that is arranged in first filter.
By using above-mentioned technical proposal, reactor housing is externally provided with heater and to be arranged at charging and discharging intraoral
Filter, include heating rod, the mounting assembly for installing heating rod and for driving heating rod work by setting
The heater of drive device, using heating rod as main heating source, and fixed by mounting assembly, so with driving
Device is controlled temperature, the heater set using said structure, ensure that the controllability to heating source, filter bag
Include the support group for being respectively arranged at the intraoral first filter of charging and discharging and the second filter and being arranged in first filter
Part, and by the first filter set respectively into and out of material mouth and the second filter, adding filter effect, during feed liquor
When can ensure the speed of reaction, and go out liquid, the degree of purity of preparation can be increased, and the support set in first filter
Component, then it can increase the support effect to the first screen pack and the second screen pack, to the first screen pack during so as to reduce feed liquor
Impact, so that it is guaranteed that good filter effect.
The utility model is further arranged to：The mounting assembly includes the connection side wall being connected with each other with reactor housing
And for connecting heating rod and connecting being connected by heat conducting pipe for side wall, connect shape between side wall and the outer wall of reactor housing
Into there is oil storage chamber, oil storage chamber includes fuel feed hole and drain oil, has conduction oil, the first filter bag in shoe cream room room
The first screen pack and the second screen pack for being respectively arranged at first filter both ends are included, support component includes being arranged at the first filtering
Support column between net and the second screen pack, glue on support column and be provided with activated carbon.
By using above-mentioned technical proposal, mounting assembly includes the connection side wall and use being connected with each other with reactor housing
In connection heating rod and being connected by heat conducting pipe for side wall is connected, by the mounting assembly of such as above-mentioned structure setting, and because
Heating rod is attached by heat conducting pipe, and is connected between side wall and the outer wall of reactor housing formed with shoe cream room
Room, oil storage chamber include fuel feed hole and drain oil, and shoe cream room has conduction oil in room, the conduction oil that has in oil storage chamber and
The setting of heat conducting pipe, increase Modulatory character of the heating rod to reactor housing, so as to accurately be adjusted to the temperature needed,
The first screen pack and the second screen pack further set at the both ends of first filter, was improved by the screen pack at both ends
Effect is filtered, and support component includes being arranged at support column between the first screen pack and the second screen pack, and support column can be
Support is provided between first screen pack and the second screen pack, is prevented because flow velocity is too fast, causes to rest on the first screen pack and the
The time of two screen packs is shorter, further glues on the support columns and is provided with activated carbon, by the activated carbon of setting, adds to miscellaneous
The adsorption effect of matter, so as to further ensure good reaction, and add the degree of purity for preparing dichloromethane.
The utility model is further arranged to：Be additionally provided with thermal insulation layer on the outer wall of the oil storage chamber, the first screen pack and
Second screen pack is made of resistant material.
By using above-mentioned technical proposal, thermal insulation layer is additionally provided with the outer wall of oil storage chamber, by the outer of oil storage chamber
The thermal insulation layer set on wall, it ensure that and in process operation, avoid, because the temperature of oil storage chamber is too high, causing not personnel
Necessary damage, security during operation is ensure that, first and second screen pack is made by resistant material, by by first and second
Screen pack is made of anticorrosion material, because preparation solution has existing corrosivity, therefore is made of anticorrosion material
Screen pack, on the one hand, add the intensity of screen pack, on the other hand also can guarantee that good filter effect.
Brief description of the drawings
Fig. 1 is a kind of structural representation of the reactor embodiment of dichloromethane of the utility model.
Fig. 2 is a kind of first filter cross section structure diagram of the reactor embodiment of dichloromethane of the utility model.
Reference in figure, 1- reactor housings, 10- charging apertures, 101- first filters, the screen packs of 1010- first,
The screen packs of 1011- second, 1012- support columns, 11- discharging openings, 12- agitators, 13- heating rods, 140- connection side walls, 141- storages
Oil-in chamber, 142- fuel feed holes, 143- drain oils, 144- heat conducting pipes, 15- drive devices, 2- motors, 21- fixed supports.
Embodiment
A kind of reactor embodiment of dichloromethane of the utility model is described further referring to figs. 1 to Fig. 2.
A kind of reactor of dichloromethane, including reactor housing 1, charging aperture 10, discharging opening 11, agitator 12, be used for
The motor 2 that agitator 12 rotates and the fixed support 21 for fixing motor 2, charging aperture 10 is driven to be arranged on reactor housing
1 top, discharging opening 11 are arranged on the bottom of reactor housing 1, and the one end of agitator 12 is stretched into reactor housing 1, other end
Stretch out reactor housing 1 to be simultaneously connected with motor 2, reactor housing 1 is externally provided with heater and to be arranged at charging and discharging intraoral
Filter, include heating rod 13, the mounting assembly for installing heating rod 13 and for driving heating rod 13 by setting
The heater of the drive device 15 of work, with heating rod 13 for main heating source, and fixed by mounting assembly,
And then temperature is controlled with drive device, the heater set using said structure, the controllability to heating source is ensure that,
Filter includes being respectively arranged at the intraoral filter 110 of first filter 101 and second of charging and discharging and is arranged at first
Support component in filter 101, and by the filter of first filter 101 and second set respectively into and out of material mouth
110, add filter effect, when can ensure the speed of reaction during feed liquor, and go out liquid, the degree of purity of preparation can be increased, and
And the support component set in first filter 101, then it can increase to the first screen pack 1010 and the second screen pack 1011
Support effect, impact during so as to reduce feed liquor to the first screen pack 1010, so that it is guaranteed that good filter effect.
The utility model is further arranged to, and mounting assembly includes the connection side wall 140 being connected with each other with reactor housing 1
And for connecting heating rod 13 and connecting being connected by heat conducting pipe 13 for side wall 140, pass through the installation of such as above-mentioned structure setting
Component, and since heating rod 13 is attached by heat conducting pipe 144, and connect side wall 140 and reactor housing 1
Include fuel feed hole 142 and drain oil 143, the internal memory of oil storage chamber 141 formed with oil storage chamber 141, oil storage chamber 141 between outer wall
There is conduction oil, the setting of the conduction oil and heat conducting pipe 144 that have in oil storage chamber 141, increase heating rod 13 is to reacting still shell
The Modulatory character of body 1, so as to accurately be adjusted to the temperature needed, further set at the both ends of first filter 101
The first screen pack 1010 and the second screen pack 1011, filter effect, and support component are improved by the screen pack at both ends
Including the support column 1012 being arranged between the first screen pack 1010 and the second screen pack 1011, support column 1012 can be first
Support is provided between the screen pack 1011 of screen pack 1010 and second, prevents from, because flow velocity is too fast, causing to rest on the first screen pack
1010 and second screen pack 1011 time it is shorter, further on support column 1012 glue be provided with activated carbon, pass through setting
Activated carbon, the adsorption effect to impurity is added, so as to further ensure good reaction, and add and prepare dichloromethane
The degree of purity of alkane.
The utility model is further arranged to, and thermal insulation layer is additionally provided with the outer wall of oil storage chamber 141, by oil storage chamber
The thermal insulation layer set on 141 outer wall, it ensure that and in process operation, avoid because the temperature of oil storage chamber 141 is too high, it is right
Personnel cause unnecessary damage, ensure that security during operation, and first and second screen pack is made by resistant material, lead to
Cross and first and second screen pack is made of anticorrosion material, because preparation solution has existing corrosivity, therefore use anti-corrosion
Screen pack made of corrosion material, on the one hand, add the intensity of screen pack, on the other hand also can guarantee that good filter effect.
Preferred embodiment of the present utility model is the foregoing is only, not limiting the utility model, the skill of this area
Art personnel carry out common variations and alternatives in the range of technical solutions of the utility model should all be included in guarantor of the present utility model
In the range of shield.
Claims (3)
1. a kind of reactor of dichloromethane, including reactor housing, charging aperture, discharging opening, agitator, for driving agitator
The motor of rotation and the fixed support for fixing motor, the charging aperture are arranged on reactor housing upper, and discharging opening is set
Put and stretched into the bottom of reactor housing, agitator one end in reactor housing, other end stretch out reactor housing and with electricity
Machine connects, it is characterized in that：The reactor housing is externally provided with heater and is arranged at the intraoral filter of charging and discharging,
Heater includes heating rod, the mounting assembly for installing heating rod and the drive device for driving heating rod to work,
Filter includes being respectively arranged at the intraoral first filter of charging and discharging and the second filter and being arranged at first filter
Interior support component.
2. a kind of reactor of dichloromethane according to claim 1, it is characterized in that：The mounting assembly includes and reaction
Connection side wall that still shell body phase connects and for connecting heating rod and connecting being connected by heat conducting pipe for side wall, connects side wall
Include fuel feed hole and drain oil formed with oil storage chamber, oil storage chamber between the outer wall of reactor housing, shoe cream room is deposited in room
There is conduction oil, the first filter includes being respectively arranged at first screen pack and the second screen pack at first filter both ends,
Support component includes the support column being arranged between the first screen pack and the second screen pack, is glued on support column and is provided with activated carbon.
3. a kind of reactor of dichloromethane according to claim 2, it is characterized in that：On the outer wall of the oil storage chamber also
Provided with thermal insulation layer, the first screen pack and the second screen pack are made of resistant material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720429369.3U CN206853659U (en) | 2017-04-22 | 2017-04-22 | A kind of reactor of dichloromethane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720429369.3U CN206853659U (en) | 2017-04-22 | 2017-04-22 | A kind of reactor of dichloromethane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206853659U true CN206853659U (en) | 2018-01-09 |
Family
ID=60816408
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720429369.3U Active CN206853659U (en) | 2017-04-22 | 2017-04-22 | A kind of reactor of dichloromethane |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206853659U (en) |
-
2017
- 2017-04-22 CN CN201720429369.3U patent/CN206853659U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 317000 Taizhou City, Zhejiang Province, chemical raw material base Lin Hai Park Patentee after: Zhejiang Taizhou Lianchuang Environmental Protection Technology Co., Ltd. Address before: 317000 Taizhou City, Zhejiang Province, Zhejiang province chemical raw material base Lin Hai Park Patentee before: Zhejiang Taizhou LIAN Environmental Protection Technology Co., Ltd. |
|
| CP03 | Change of name, title or address |