CN206848111U - Normal temperature and pressure gas solubility determines device - Google Patents

Normal temperature and pressure gas solubility determines device Download PDF

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Publication number
CN206848111U
CN206848111U CN201720791918.1U CN201720791918U CN206848111U CN 206848111 U CN206848111 U CN 206848111U CN 201720791918 U CN201720791918 U CN 201720791918U CN 206848111 U CN206848111 U CN 206848111U
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CN
China
Prior art keywords
valve
cylinder
pipeline
balance cylinder
pipe
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Expired - Fee Related
Application number
CN201720791918.1U
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Chinese (zh)
Inventor
程庆超
童富果
刘刚
钟佳思
刘创
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China Three Gorges University CTGU
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China Three Gorges University CTGU
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Priority to CN201720791918.1U priority Critical patent/CN206848111U/en
Application granted granted Critical
Publication of CN206848111U publication Critical patent/CN206848111U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

Normal temperature and pressure gas solubility determines device, including balance cylinder, balance cylinder upper end is connected by the first pipeline with vavuum pump, first valve is installed on the first pipeline, top cover is installed in balance cylinder's opening, pressure gauge is installed in top cap central, balance cylinder bottom is connected by second pipe with cylinder, second valve and the 3rd valve are installed on second pipe, the 3rd pipeline is communicated with second pipe between the second valve and the 3rd valve, the 4th valve is installed on the 3rd pipeline, support is fixedly connected with cylinder outer wall, displacement monitors are installed in support, displacement monitors thimble is resisted against on cylinder piston rod.

Description

Normal temperature and pressure gas solubility determines device
Technical field
It the utility model is related to normal temperature and pressure gas solubility measure device.
Background technology
The field that the solubility of gas in a liquid is related to is very extensive, such as:Chemical process design, Environmental Chemistry, biology Medical technology, biophysics, geochemistry etc., it is industrial very important basic data.The solubility of gas is most It is by vascular unloading technique experimental test, due to the solubility very little of general gas flow in a liquid, is brought to experiment very big Difficulty, result of the test are not easy to measure accurately.Existing test device includes complicated solvent purification device and excessive switching Head and valve, not only device airtight test is numerous and diverse, and pipeline cleaning is difficult.
The content of the invention
It is to be solved in the utility model to be to provide normal temperature and pressure gas solubility measure device, to realize at normal temperatures and pressures The test of gas solubility, solve existing instrument test precision not enough and sealing technical problem.
In order to solve the above-mentioned technical problem, the technical solution of the utility model is:Normal temperature and pressure gas solubility measure dress Put, including balance cylinder, balance cylinder upper end are connected by the first pipeline with vavuum pump, and the first valve is provided with the first pipeline, Top cover is installed in balance cylinder's opening, pressure gauge is installed in top cap central, balance cylinder bottom passes through second pipe and cylinder Connection, is provided with the second valve and the 3rd valve, the second pipe between the second valve and the 3rd valve on second pipe On be communicated with the 3rd pipeline, the 4th valve is installed on the 3rd pipeline, support is fixedly connected with cylinder outer wall, in support Displacement monitors are installed, displacement monitors thimble is resisted against on cylinder piston rod.
The beneficial effects of the utility model are:The utility model can take out the mode of pressure first by remaining in solution using vacuum Gas evolution, then entered by gas from solution bottom, fully gas is dissolved in solution;On the other hand, this practicality is new Type only can need to change gas in piston container into pure gas (such as O to different type gas test2、CO2Deng), it is operated Mode is simple and efficient;On the other hand, the utility model can read pressure and piston by digital display manometer and displacement monitors Change in displacement, improve the precision of monitoring.
Brief description of the drawings
The utility model is described further below in conjunction with the accompanying drawings:
Fig. 1 is structural representation of the present utility model.
In figure:Balance cylinder 1, the first valve 2, vavuum pump 3, the pipeline 5 of top cover 4 first, pressure gauge 6, cylinder 7, support 8, position Move monitor 9, the second valve 10, the 3rd valve 11, the 3rd pipeline 12, have the 4th valve 13, second pipe 14.
Embodiment
As shown in figure 1, normal temperature and pressure gas solubility determines device, including balance cylinder 1, the upper end of balance cylinder 1 pass through first Pipeline 5 is connected with vavuum pump 3, and the first valve 2 is provided with the first pipeline 5, and top cover 4 is provided with the opening of balance cylinder 1, The center of top cover 4 is provided with pressure gauge 6, and the bottom of balance cylinder 1 is connected with cylinder 7 by second pipe 14, pacified on second pipe 14 Equipped with the second valve 10 and the 3rd valve 11, is communicated with the second pipe 14 between the second valve 10 and the 3rd valve 11 Three pipelines 12, the 4th valve 13 is provided with the 3rd pipeline 12, support 8 is fixedly connected with the outer wall of cylinder 7, in support 8 Displacement monitors 9 are installed, the thimble of displacement monitors 9 is resisted against on the piston rod of cylinder 7.
Normal temperature and pressure gas solubility determines the application method of device, comprises the following steps:
A, gas is injected, is first shut off the second valve 10, the 3rd valve 11 is opened and the 4th valve 13, pusher cylinder 7 is lived Stopper rod is descending, is then filled under test gas in cylinder 7 by the 3rd pipeline 12, after under test gas is filled with, closes the Three valves 11 and the 4th valve 13;
B, liquor capacity V is determined, the quality m by measuring solution calculates the volume V of balance cylinder 1 shared by solution, then will Solution is poured into balance cylinder 1, and control liquor capacity accounts for the ratio of the volume of balance cylinder 1 2/3 or so, finally seals top cover 4 It is installed in the opening of balance cylinder 1;
C, pressure gas is taken out, the first valve 2 is opened, balance cylinder 1 is evacuated using vavuum pump 3, treats that pressure gauge 6 drops to -90kpa In the range of to -100kpa, the first valve 2 is closed, treats the value stabilization of pressure gauge 6, records pressure value P1
D, gas solubility determines, and be zeroed displacement monitors 9, and opens the 3rd valve 11 and the second valve 10 successively, sees The movement of push rod in piston container is examined, after push rod movement is stable, the record value of displacement monitors 9 is L1, pressure value P2
E, the amount solubility s of substance for calculation:
In formula:PaRepresent standard atmospheric pressure 1.013 × 105Pa;P1、P2It is negative value to represent relatively large air pressure;R represents preferable Gas constant 8.314J/molk;T represents absolute temperature, T=Celsius temperatures+273.15;V1Represent the volume of balance cylinder 1;
Unit:K, normal temperature state takes T=20+273.15=293.15k in the utility model;M represents gas molar quality, Unit:g/mol.

Claims (1)

1. normal temperature and pressure gas solubility determines device, it is characterised in that:Including balance cylinder(1), balance cylinder(1)Upper end passes through One pipeline(5)With vavuum pump(3)Connection, in the first pipeline(5)On the first valve is installed(2), in balance cylinder(1)Pacify in opening Equipped with top cover(4), in top cover(4)Center is provided with pressure gauge(6), balance cylinder(1)Bottom passes through second pipe(14)With cylinder (7)Connection, in second pipe(14)On the second valve is installed(10)With the 3rd valve(11), in the second valve(10)With the 3rd Valve(11)Between second pipe(14)On be communicated with the 3rd pipeline(12), in the 3rd pipeline(12)On the 4th valve is installed (13), in cylinder(7)Support is fixedly connected with outer wall(8), in support(8)Displacement monitors are installed(9), displacement monitors (9)Thimble is resisted against cylinder(7)On piston rod.
CN201720791918.1U 2017-07-03 2017-07-03 Normal temperature and pressure gas solubility determines device Expired - Fee Related CN206848111U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720791918.1U CN206848111U (en) 2017-07-03 2017-07-03 Normal temperature and pressure gas solubility determines device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720791918.1U CN206848111U (en) 2017-07-03 2017-07-03 Normal temperature and pressure gas solubility determines device

Publications (1)

Publication Number Publication Date
CN206848111U true CN206848111U (en) 2018-01-05

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Family Applications (1)

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CN201720791918.1U Expired - Fee Related CN206848111U (en) 2017-07-03 2017-07-03 Normal temperature and pressure gas solubility determines device

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CN (1) CN206848111U (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109738328A (en) * 2019-01-28 2019-05-10 中粮粮油工业(巢湖)有限公司 Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure
CN110523178A (en) * 2019-09-16 2019-12-03 温州捷朴环保科技有限公司 A kind of smog pollution purification device based on hypergravity
CN112782035A (en) * 2021-01-25 2021-05-11 安徽省宣城市华纳新材料科技有限公司 Kiln gas carbon dioxide concentration measuring instrument
CN113008728A (en) * 2021-02-23 2021-06-22 河南工程学院 Device and method for measuring water solubility of methane

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109738328A (en) * 2019-01-28 2019-05-10 中粮粮油工业(巢湖)有限公司 Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure
CN110523178A (en) * 2019-09-16 2019-12-03 温州捷朴环保科技有限公司 A kind of smog pollution purification device based on hypergravity
CN110523178B (en) * 2019-09-16 2020-12-04 固安县朔程燃气有限公司 Smoke pollution purifier based on hypergravity
CN112782035A (en) * 2021-01-25 2021-05-11 安徽省宣城市华纳新材料科技有限公司 Kiln gas carbon dioxide concentration measuring instrument
CN113008728A (en) * 2021-02-23 2021-06-22 河南工程学院 Device and method for measuring water solubility of methane
CN113008728B (en) * 2021-02-23 2021-12-17 河南工程学院 Device and method for measuring water solubility of methane

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CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20180105

Termination date: 20180703