CN109738328A - Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure - Google Patents

Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure Download PDF

Info

Publication number
CN109738328A
CN109738328A CN201910080772.3A CN201910080772A CN109738328A CN 109738328 A CN109738328 A CN 109738328A CN 201910080772 A CN201910080772 A CN 201910080772A CN 109738328 A CN109738328 A CN 109738328A
Authority
CN
China
Prior art keywords
vegetable oil
inspiratory capacity
detection method
normal temperature
water column
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910080772.3A
Other languages
Chinese (zh)
Inventor
王佐才
韩志国
孟祥永
李万平
宋玉义
陈吉江
赵仕峰
黄一华
朱永奇
罗建华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cofco Food Marketing Co Ltd
Cofco Grain And Oil Industry (chaohu) Co Ltd
Original Assignee
Cofco Food Marketing Co Ltd
Cofco Grain And Oil Industry (chaohu) Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cofco Food Marketing Co Ltd, Cofco Grain And Oil Industry (chaohu) Co Ltd filed Critical Cofco Food Marketing Co Ltd
Priority to CN201910080772.3A priority Critical patent/CN109738328A/en
Publication of CN109738328A publication Critical patent/CN109738328A/en
Pending legal-status Critical Current

Links

Landscapes

  • Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)

Abstract

The invention discloses vegetable oil inspiratory capacity rapid detection methods under a kind of normal temperature and pressure, it is to mark water column initial position, start magnetic stirring apparatus, adjusting blender stirring rotor speed makes tested vegetable oil generation vortex reach maximum, water column moves in transparent tracheae simultaneously, and mobile distance is multiplied by being vegetable oil to be measured inspiratory capacity at normal temperatures and pressures after the calculating of transparent tracheae inner hole sectional area.The present invention provides one kind directly to detect vegetable oil air-breathing quantity measuring method to be filled, rapid examination and tested vegetable oil inspiratory capacity can be calculated by water column movement, the adjustment filling production nitrogen charging technique of different batches vegetable oil in time saves nitrogen charging cost, improves production and detection efficiency;Client plant oil bottle is avoided to generate depression wrinkle mark phenomenon;The method is simple, quick, easy to operate and testing cost is cheap.

Description

Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure
Technical field:
Vegetable oil inspiratory capacity is quickly detected using magnetic stirring apparatus the present invention relates to a kind of, more particularly to PET is avoided to pack Plant oil bottle generates the rapid detection method that negative pressure causes depression.
Background technique:
The refining vegetable oil that vegetable oil especially newly refines out has oxidation and air-breathing unstability;Food-grade packing timber Expect PET, that is, polyethylene terephthalate, currently on the market the Packaging Bottle filling for beverage or vegetable oil.
After PET Packaging Bottle filling and capping, oil bottle becomes a sealing system, influences bottle empty in addition to vegetable oil oil temperature changes Outside shape, the pressure in the bottle is influenced there is also overhead gas in vegetable oil inhaler itself or oxidation reaction and is changed, the deformation of generation bottle body, It rises phenomena such as flat, thus strong influence terminal market product quality.In the industry mainly using nitrogen-charging fresh-keeping mode ensure oil product and Bottle-type presentation quality;Currently, a kind of not yet quickly detect nitrogen-charging fresh-keeping effect method, it would therefore be highly desirable to develop a kind of scientific, letter Just PET packs vegetable oil air-breathing quantity measuring method.
Summary of the invention:
Place that purpose of the invention is to overcome the shortcomings in the prior art, is to provide a kind of normal temperature and pressure vegetable oil Inspiratory capacity rapid detection method cannot really reflect nitrogen charging effect in bottle after avoiding packaging vegetable oil nitrogen charging, to influence to produce Product physical and chemical index and image appearance.
The following technical solution is employed for the technical problems to be solved by the invention to realize:
Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure, comprises the steps of:
(1) the vegetable oil to be measured injection test bottle five/everywhere that room temperature is mutually synthermal, and it is put into stirrer, use is close Lidstock, sealing cover are equipped with 2 holes;
(2) in thermometer insertion one hole of sealing cover, test is put on magnetic stirring apparatus with bottle;
(3) Duan Shuizhu being injected into using pasteur pipet in transparent tracheae one end again, the other end is inserted on another hole of sealing cover, Keep transparent tracheae, thermometer, bottleneck and seal cap sealing state;
(4) water column initial position is marked, magnetic stirring apparatus is started, adjusting blender stirring rotor speed produces tested vegetable oil Raw vortex reaches maximum;Water column moves in transparent tracheae simultaneously;
(5) after the mobile stopping of water column in transparent tracheae, water column moving distance and vegetable oil oil temperature are recorded;
It (6) is vegetable oil to be measured air-breathing at normal temperatures and pressures after mobile distance is calculated multiplied by tracheae inner hole sectional area Amount.
Specifically: moving distance L, using transparent tracheae inside radius R, according to formula V=π R2L calculates vegetable oil to be measured Inspiratory capacity at normal temperatures and pressures.
Further technology: the transparent tracheae is hose, is supported in bending part using plastic circle ring fastener, rounding off.
Further technology: one end for being marked with water column of transparent tracheae is horizontally arranged.
Further technology: one end for being marked with water column of transparent tracheae is placed on the floating plate of the water surface.
Further technology: keep the water surface tranquil.
Further technology: transparent tracheae, thermometer, bottleneck and seal cap sealing state are kept.
Further technology: thermometer is inserted 3 times, and bottom, middle layer and the surface layer of vegetable oil are located at, and is all reached to temperature at 3 Start magnetic stirring apparatus after to room temperature.
Further technology: in the bottle of the other end insertion test bottle of the transparent tracheae at top 1/5th, and thoroughly The bright tracheae other end is not contacted with vegetable oil to be measured.
It is of the invention to be advantageous in that:
1, the present invention provides one kind directly to detect vegetable oil air-breathing quantity measuring method to be filled, passes through water column moving distance It can simply observe and calculate tested vegetable oil inspiratory capacity;
2, filling production nitrogen charging technique is adjusted in time, saves nitrogen charging cost, improves production and detection efficiency;
3, client plant oil bottle is avoided to generate depression wrinkle mark phenomenon;
4, the method is simple, easy to operate and testing cost is cheap.
Detailed description of the invention:
To describe the technical solutions in the embodiments of the present invention more clearly, make required in being described below to embodiment Attached drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for For those of ordinary skill in the art, without creative efforts, it can also be obtained according to these attached drawings other Attached drawing;
Fig. 1 is vegetable oil air-breathing quantity measuring method device figure under a kind of normal temperature and pressure;
Wherein drawing reference numeral: 1, magnetic stirring apparatus;2, stirrer;3, bottle is used in test;4, sealing cover;5, thermometer;6, thoroughly Bright tracheae;7, vegetable oil;8, water column;10, meter ruler.
Specific embodiment:
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention, Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making Every other embodiment obtained, shall fall within the protection scope of the present invention under the premise of creative work.
Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure, used tool includes magnetic stirring apparatus;Stirrer; Bottle is used in test;Thermometer;Sealing cover;Transparent tracheae;Vegetable oil;Small water column;Pasteur pipet;Meter ruler.
By the mutually synthermal vegetable oil to be measured injection test bottle five/everywhere of room temperature, test is specially 250ml with bottle Glass reagent bottle, vegetable oil 200ml to be measured, and be put into stirrer, stirrer length 49.5mm diameter 10mm are close with sealing cover Envelope, sealing cover use mobile phase diplopore lid;
For the effect for guaranteeing sealing, sealing ring is added with bottle bottleneck contact position in mobile phase diplopore lid and test;
Thermometer is inserted into one hole of mobile phase diplopore lid, and test bottle is put on magnetic stirring apparatus;
Thermometer is observed, after vegetable oil room temperature to be measured, opens further work;
Meanwhile to guarantee that temperature detection precise degrees, thermometer are inserted 3 times, it is located at bottom, middle layer and the table of vegetable oil Layer, opens further work after temperature at 3 all reaches room temperature;
A Duan Shuizhu, water column length 20mm, other end insertion stream phase are injected into using pasteur pipet in transparent tracheae one end again On another hole of diplopore lid, the transparent tracheae is hose, is supported in bending part using plastic circle ring fastener, rounding off;
Keep transparent tracheae, thermometer, bottleneck and stream phase diplopore lid sealing state;Sealing still adds sealing ring herein, Enhance sealing effect;Suction pipe uses transparent tracheae PU-6 × 4mm length 1500mm;
After injecting water column, test bottle is inserted into transparent tracheae one end, wherein the other end of transparent tracheae is horizontal positioned, Guarantee again without other external worlds under the influence of, water column remains static;
20 millimeters away from top in the bottle of the other end insertion test bottle of transparent tracheae.
In order to preferably more accurately detect, the other end of transparent tracheae is placed on the floating plate of the water surface, keeps water Face is tranquil;
After the completion of the above preparation, in the initial position of transparent tracheae outer wall mark water droplet, starts magnetic stirring apparatus, adjust Section blender stirring rotor speed makes tested vegetable oil generate vortex and reaches maximum;Water column moves in transparent tracheae simultaneously;
For recording the mobile distance of water column after the mobile stopping of water column in transparent tracheae;
In order to place a meter ruler at the transparent tracheae of horizontal segment with clear viewing distance;
Mobile distance L is multiplied by pasteur pipet inner hole section product π R2It is oil to be measured air-breathing at normal temperatures and pressures after calculating Amount.
Specifically: moving distance L, using transparent tracheae inside radius R, according to formula V=π R2L calculates vegetable oil to be measured Inspiratory capacity at normal temperatures and pressures.
There is provided a kind of equipment for cooperating the detection method simultaneously, such as Fig. 1, vegetable oil inspiratory capacity is quick under a kind of normal temperature and pressure Detection device, including
Test bottle 3, the test bottle include glass bottle body and sealing cover, and sealing cover is equipped with hole;
Rabbling mechanism, the rabbling mechanism is for the vegetable oil 7 in mixing test bottle;
Transparent tracheae 6, described transparent tracheae one end are inserted into vial, and water column is equipped in the other end;
Wherein, the rabbling mechanism stirrer blender jar implants oil, vegetable oil air content can change or generate oxygen Change reaction, bottle top gas volume will increase or reduce, to push water column mobile.
Further include temperature-detecting device, be set in vial, for detecting the temperature of the vegetable oil in vial.
The temperature-detecting device uses thermometer 5, and sealing cover 4 is equipped with 2 holes, and one of hole is transparent for being inserted into Tracheae 6, thermometer 5 are inserted in another hole.
The transparent tracheae 6, thermometer 5, the bottleneck of test bottle 3 and sealing cover 4 are in sealing state.
The rabbling mechanism includes magnetic stirring apparatus 1 and stirrer 2, and magnetic stirring apparatus 1 is located at test 3 lower section of bottle, uses In support test bottle 3, and drives and be located at stirrer 2 rotation of the test in bottle 3.
Test bottle is inserted into transparent tracheae one end, wherein the other end of transparent tracheae is horizontal positioned.
It is described in order to place a meter ruler 10 at the transparent tracheae of horizontal segment with clear viewing distance.
Start magnetic stirring apparatus 1, adjusting 1 stirrer of magnetic stirring apparatus, 2 revolving speed reaches tested vegetable oil generation vortex most Greatly, while the inner water column 8 of transparent tracheae 6 moves, mobile distance multiplied by transparent 6 inner hole section of tracheae product calculate after be plant The inspiratory capacity at normal temperatures and pressures of object oil 7.
In description of the invention, it should be noted that the orientation of the instructions such as term "vertical", "upper", "lower", "horizontal" or Person's positional relationship is orientation based on the figure or positional relationship, is merely for convenience of description of the present invention and simplification of the description, Rather than the device or element of instruction or hint meaning must have a particular orientation, and are constructed and grasped with specific orientation Make, therefore is not considered as limiting the invention.In addition, " first ", " second ", " third ", " the 4th " are only used for description mesh , and should not be understood as indicating or implying relative importance.
In description of the invention, it is also necessary to explanation, unless otherwise specific regulation and limitation, term " setting ", " peace Dress ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integrally Connection, can be mechanical connection, is also possible to be electrically connected, can be and be directly connected to, and be also possible to be connected by intermediary, can To be the connection inside two elements.For the ordinary skill in the art, can understand as the case may be above-mentioned The concrete meaning of term in the present invention.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (8)

1. vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure, it is characterised in that: comprise the steps of:
(1) the vegetable oil to be measured injection test bottle five/everywhere that room temperature is mutually synthermal, and it is put into stirrer, use sealing cover Sealing, sealing cover are equipped with 2 holes;
(2) in thermometer insertion one hole of sealing cover, test is put on magnetic stirring apparatus with bottle;
(3) Duan Shuizhu is injected into using pasteur pipet in transparent tracheae one end again, the other end is inserted on another hole of sealing cover;
(4) water column initial position is marked, magnetic stirring apparatus is started, blender is adjusted and stirs rotor speed, generates tested vegetable oil Vortex reaches maximum, while water column moves in transparent tracheae;
(5) after the mobile stopping of water column in transparent tracheae, water column moving distance and vegetable oil oil temperature are recorded;
It (6) is vegetable oil to be measured inspiratory capacity at normal temperatures and pressures after mobile distance is calculated multiplied by tracheae inner hole sectional area.
2. vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure according to claim 1, it is characterised in that: The transparent tracheae is hose, is supported in bending part using plastic circle ring fastener, rounding off.
3. vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure according to claim 1, it is characterised in that: One end for being marked with water column of transparent tracheae is horizontally arranged.
4. vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure according to claim 3, it is characterised in that: One end for being marked with water column of transparent tracheae is placed on the floating plate of the water surface.
5. vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure according to claim 4, it is characterised in that: Keep the water surface tranquil.
6. vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure according to claim 1, it is characterised in that: Keep transparent tracheae, thermometer, bottleneck and seal cap sealing state.
7. vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure according to claim 1, it is characterised in that: Thermometer is inserted 3 times, is located at bottom, middle layer and the surface layer of vegetable oil, is started magnetic agitation after temperature at 3 all reaches room temperature Device.
8. vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure according to claim 1, it is characterised in that: In the other end insertion test bottle of the transparent tracheae, apart from 20 millimeters of bottle top.
CN201910080772.3A 2019-01-28 2019-01-28 Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure Pending CN109738328A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910080772.3A CN109738328A (en) 2019-01-28 2019-01-28 Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910080772.3A CN109738328A (en) 2019-01-28 2019-01-28 Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure

Publications (1)

Publication Number Publication Date
CN109738328A true CN109738328A (en) 2019-05-10

Family

ID=66366448

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910080772.3A Pending CN109738328A (en) 2019-01-28 2019-01-28 Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure

Country Status (1)

Country Link
CN (1) CN109738328A (en)

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1995966A (en) * 2006-09-30 2007-07-11 梁嘉臻 Method for detecting oxygen absorption capacity of deoxidizer
CN201025473Y (en) * 2006-12-05 2008-02-20 刘昂峰 Portable sorbent and inspiration measurement instrument
CN102235959A (en) * 2010-12-22 2011-11-09 保定天威集团有限公司 Method for determining air content in transformer oil through mechanical oscillation method
CN202362222U (en) * 2011-11-21 2012-08-01 张金川 Whole-course visualized gas content tester
CN102645525A (en) * 2012-04-09 2012-08-22 中国科学院深圳先进技术研究院 Device and method for measuring solubility of refrigerant in refrigerator oil and application thereof
CN103743647A (en) * 2014-01-07 2014-04-23 湖南巴陵油脂有限公司 Device and method for rapidly determining content of nitrogen in edible vegetable oil
CN103808628A (en) * 2014-03-03 2014-05-21 重庆医科大学 Blood-culture carbon dioxide trace-gas detection system and detection method thereof
CN204882293U (en) * 2015-08-22 2015-12-16 杨景宇 Measure device of gas production volume
CN105675434A (en) * 2016-03-16 2016-06-15 中国地质大学(北京) System and method for measuring gas content
CN205353070U (en) * 2015-12-19 2016-06-29 大连大孤山污水处理有限公司 New dissolved oxygen determination device
CN106404593A (en) * 2016-12-15 2017-02-15 珠江水利委员会珠江水利科学研究院 Plant leaf scale transpiration measurement device and measurement method thereof
CN206848111U (en) * 2017-07-03 2018-01-05 三峡大学 Normal temperature and pressure gas solubility determines device

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1995966A (en) * 2006-09-30 2007-07-11 梁嘉臻 Method for detecting oxygen absorption capacity of deoxidizer
CN201025473Y (en) * 2006-12-05 2008-02-20 刘昂峰 Portable sorbent and inspiration measurement instrument
CN102235959A (en) * 2010-12-22 2011-11-09 保定天威集团有限公司 Method for determining air content in transformer oil through mechanical oscillation method
CN202362222U (en) * 2011-11-21 2012-08-01 张金川 Whole-course visualized gas content tester
CN102645525A (en) * 2012-04-09 2012-08-22 中国科学院深圳先进技术研究院 Device and method for measuring solubility of refrigerant in refrigerator oil and application thereof
CN103743647A (en) * 2014-01-07 2014-04-23 湖南巴陵油脂有限公司 Device and method for rapidly determining content of nitrogen in edible vegetable oil
CN103808628A (en) * 2014-03-03 2014-05-21 重庆医科大学 Blood-culture carbon dioxide trace-gas detection system and detection method thereof
CN204882293U (en) * 2015-08-22 2015-12-16 杨景宇 Measure device of gas production volume
CN205353070U (en) * 2015-12-19 2016-06-29 大连大孤山污水处理有限公司 New dissolved oxygen determination device
CN105675434A (en) * 2016-03-16 2016-06-15 中国地质大学(北京) System and method for measuring gas content
CN106404593A (en) * 2016-12-15 2017-02-15 珠江水利委员会珠江水利科学研究院 Plant leaf scale transpiration measurement device and measurement method thereof
CN206848111U (en) * 2017-07-03 2018-01-05 三峡大学 Normal temperature and pressure gas solubility determines device

Similar Documents

Publication Publication Date Title
CN106018163B (en) A kind of system measuring the solubility parameter of gas in a liquid
JP2016136928A (en) Shaking-type culture apparatus, and culture method using the same
CN101830420B (en) Fully-automatic thermostatic magnetic stirring sterile liquid medicine preparing and packaging device
CN109738328A (en) Vegetable oil inspiratory capacity rapid detection method under a kind of normal temperature and pressure
CN208766072U (en) A kind of experimental provision measuring H2O2 decomposition reaction rate constant
CN109738327A (en) Vegetable oil inspiratory capacity device for fast detecting under a kind of normal temperature and pressure
CN203227313U (en) Rotary evaporator
CN108114652A (en) A kind of magnetic agitation Agitation Tank
CN203519504U (en) Static state evaluation device for scale inhibition performance of reverse-osmosis scale inhibitor
CN105644949A (en) Polypropylene vacuum metering tank
CN109021050A (en) A kind of biosynthesis instrument
CN208695037U (en) A kind of anti-spillage convenient test medication spoon
CN205786457U (en) Micro-moisture detection device
CN102551544A (en) Nutrient solution adding device for water dispenser
CN209673186U (en) Level monitoring device under a kind of agitator tank
CN200958999Y (en) Portable inspecting reagent microtube
CN209911370U (en) Simple and easy survey device of mud oxygen consumption rate
CN208187594U (en) Calorimetric reaction vessel for high-precision calorimeter
CN208699341U (en) A kind of metering device and liquid packaging bottle for vertical Dumpage type liquid packaging bottle
US4957707A (en) Thermal hazard evaluation
CN215312459U (en) Triangular flask capable of indicating temperature
CN109051201A (en) A kind of metering device and liquid packaging bottle for vertical Dumpage type liquid packaging bottle
CN204666461U (en) A kind of oxidized metal measuring appliance
CN213068809U (en) Dissolution testing device for dapoxetine hydrochloride tablets
US20210189311A1 (en) Device and method for culturing cells in a shaking operation

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20190510