CN206823221U - A kind of adjustment type fat diffuser - Google Patents
A kind of adjustment type fat diffuser Download PDFInfo
- Publication number
- CN206823221U CN206823221U CN201720603998.3U CN201720603998U CN206823221U CN 206823221 U CN206823221 U CN 206823221U CN 201720603998 U CN201720603998 U CN 201720603998U CN 206823221 U CN206823221 U CN 206823221U
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- Prior art keywords
- flask
- extraction
- diffuser
- adjustment type
- pipe
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes
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- Extraction Or Liquid Replacement (AREA)
Abstract
It the utility model is related to the technical field of plant and the extraction of vegetable oil material crude fat, disclose a kind of adjustment type fat diffuser, including extracting flask, extract cylinder and condenser, the extraction flask is immersed in water-bath, the extraction cylinder is connected by extracting flask described in the Bian Guanyu of side, the opposite side of the extraction cylinder is provided with the siphon pipe connected with the extraction flask, the upper end of the extraction cylinder connects with the lower port of the condenser, the extraction flask is the flask of preset capacity, the siphon pipe includes two flexible pipes and a U-tube, upper end of the U-tube respectively with two flexible pipes is connected, the lower end of wherein one flexible pipe connects with the bottom side of the extraction cylinder, the lower end of another flexible pipe connects with the extraction flask.Adjustment type fat diffuser provided by the utility model, enhances disposal ability, improves extracting efficiency.
Description
Technical field
The technical field of plant and the extraction of vegetable oil material crude fat is the utility model is related to, more particularly to a kind of adjustment type
Fat diffuser.
Background technology
Usual laboratory is using remaining method measure plant crude fat, dry weight and extraction with residue after petroleum ether extraction sample
Dry weight can calculates the content of plant crude fat before sample.
Experimental determination plant crude fat, by solvent evaporative condenser, sample is extracted and extracted, backflow, so circulated past
It is multiple, untill extracting completely.
This crude fat determines, and using extraction equipment for fat, takes liquid-solid extraction mode, is according to solvents upon solids mixture
Needed for composition solubility it is big, it is small to the solubility of impurity to reach the purpose of extraction separation.Utilize siphon principle and solvent
Automatic back flow, it is extracted product reflux and concentrates in flask.Because the boiling point of extract is higher than solvent, there was only solvent after being heated
Instilled after gaseous state evaporation, condensation in shuttle, make leaching process each time, be all dissolving of the neat solvent to extract, because
Solvent can be recycled, and solid matter is continuously extracted by neat solvent, make solvent load less, and extraction effect is preferable.
Normal fat digester is simple, handy, both saves solvent, and effect of extracting is again good.But also there is weak point：Due to leaching
It is smaller to carry a capacity, less than 10 samples can only be accommodated；Fat diffuser number will be increased when handling great amount of samples, simultaneously
Multiple auxiliary equipments are connected, it is also few even if the sample so handled；Multiple fat diffuser connections look in a mess, operate
Also bother.
Utility model content
(1) technical problems to be solved
The purpose of this utility model is to provide a kind of adjustment type fat diffuser, to solve existing fat diffuser capacity
It is small, the problem of trivial operations.
(2) technical scheme
In order to solve the above-mentioned technical problem, a kind of adjustment type fat diffuser of the utility model offer, including extraction flask,
Cylinder and condenser are extracted, the extraction flask is immersed in water-bath, and the extraction cylinder passes through extraction described in the Bian Guanyu of side
Flask connects, the opposite side of the extraction cylinder be provided with the siphon pipe that connect of extraction flask, the upper end of the extraction cylinder and
The lower port connection of the condenser, the extraction flask are the flask of preset capacity, the siphon pipe include two flexible pipes and
One U-tube, upper end of the U-tube respectively with two flexible pipes are connected, wherein the lower end of a flexible pipe and the leaching
The bottom side connection of cylinder is proposed, the lower end of another flexible pipe connects with the extraction flask.
Wherein, the bottom of a pan of the water-bath is provided with the flask support being adapted to the round-bottomed flask.
Wherein, the upper end of condenser is provided with cooling water outlet, and the condenser lower end is provided with cooling water intake.
Wherein, stay-warm case is provided with the upside of the water-bath, the stay-warm case is adapted to the flask.
Wherein, the lower end of the side pipe is located in the bottleneck of the flask, the upper end of the side pipe and the extraction cylinder
Upside connection.
Wherein, the outside of the side pipe is provided with insulation material.
Wherein, the bottom side of the extraction cylinder is provided with siphon pipe bypass outlet, the siphon pipe bypass outlet and wherein one
The lower end connection of the flexible pipe；The bottleneck of the flask is provided with siphon pipe backflow import, siphon pipe backflow import with it is another
The lower end connection of flexible pipe described in root.
Wherein, the material of the flexible pipe is organic silicon rubber.
Wherein, the height adjustable adjusting range of the U-tube is 10-28cm.
Wherein, the material of the U-tube is polytetrafluoroethylene (PTFE).
(3) beneficial effect
Adjustment type fat diffuser provided by the utility model, increases capacity, improves disposal ability, by using big
The flask of capacity, demand of the varying number sample to different solvents amount is met, solvent evaporation is stable, improves extracting efficiency；
Height Adjustable siphon pipe is set, meets the extraction to varying number sample, operation is simplified, improves extracting efficiency.
Brief description of the drawings
The structural representation of Fig. 1 the utility model embodiments.
In figure, 1：Extract flask；2：Siphon pipe；3：Extract cylinder；4：Condenser；5：Bian Guan；6：Water-bath；7：Stay-warm case；
8：Insulation material；9：Sample sack；10：Water inlet；11：Delivery port；12：Siphon pipe bypass outlet；13：Siphon pipe backflow import；
14：U-tube；15：Flexible pipe.
Embodiment
With reference to the accompanying drawings and examples, specific embodiment of the present utility model is described in further detail.Below
Example is used to illustrate the utility model, but is not limited to the scope of the utility model.
The utility model embodiment is small for existing fat diffuser capacity, the problem of trivial operations, there is provided one kind regulation
Type fat diffuser.
As shown in Figure 1, the utility model provides a kind of adjustment type fat diffuser, including extraction flask 1, extraction cylinder 3
With condenser 4, the extraction flask 1 is immersed in water-bath 6, and the extraction cylinder 3 is burnt by the side pipe 5 of side with the extraction
Bottle 1 connects, and the opposite side of the extraction cylinder 3 is provided with the siphon pipe 2 connected with the extraction flask 1, the upper end of the extraction cylinder 3
Connected with the lower port of the condenser 4, the lower end of the condenser 4 is provided with water inlet 10, and the upper end of the condenser 4 is provided with
Delivery port 11, is respectively communicated with cooling water pipe, to cool down solvent vapour, solvent vapour condensing reflux is entered in extraction cylinder 3；
Wherein, the extraction flask 1 is the round-bottomed flask of preset capacity, and preset capacity scope is 3-5L, in the present embodiment
Capacity is 4L round-bottomed flask, meets the demand of different solvents amount, improves the disposal ability and extracting efficiency of digester；It is described
Siphon pipe 2 includes two U-tubes 14 of flexible pipe 15 and one, and upper end of the U-tube 14 respectively with two flexible pipes 15 is connected, its
In the lower end of a flexible pipe 15 connect with the bottom side of the extraction cylinder 3, the lower end of another flexible pipe 15 and the leaching
Flask 1 is carried to connect.
Further, the bottom of a pan of the water-bath 6 is provided with the flask support being adapted to the round-bottomed flask, makes round-bottomed flask steady
Fixed heated, solvent evaporation is stable.
Wherein, the upside of water-bath 6 is provided with stay-warm case 7, and the stay-warm case 7 is adapted to the round-bottomed flask, improved
The heat insulation effect of water-bath 6, prevents heat to wander away.
Further, the lower end of the side pipe 5 is located in the bottleneck of the round-bottomed flask, the upper end of the side pipe 5 with
The upside connection of the extraction cylinder 3, when the solvent evaporation in round-bottomed flask, the upside of extraction cylinder 3 is passed through by side pipe 5, is entered
And enter in condenser 4.
Wherein, the outside of the side pipe 5 is provided with insulation material 8, prevents side pipe 5 from radiating, avoids the solvent vapour in side pipe 5
Residual titration is condensed, energy is saved, improves extracting efficiency.
Further, the bottom side of the extraction cylinder 3 is provided with siphon pipe bypass outlet 12, the siphon pipe bypass outlet 12 and
The lower end connection of wherein one flexible pipe 15；The bottleneck of the round-bottomed flask is provided with siphon pipe backflow import 13, the siphon
Pipe backflow import 13 is connected with the lower end of another flexible pipe 15.
Wherein, flexible pipe 15 and the connection of siphon pipe backflow import 13 can open, and after extraction terminates, open flexible pipe 15 and rainbow
The connection of suction pipe backflow import 13, recycling design.
Further, the material of the flexible pipe 15 is organic silicon rubber, and not soluble in water and any solvent is nonpoisonous and tasteless, is changed
It is stable to learn property, upper end of the U-tube 14 respectively with two flexible pipes 15 is connected, by adjust the height of U-tube 14 come
Regulation extraction cylinder 3 internal solvent backflow height；It is naturally curved downwards with subordinate's pressure U-tube 14, height reduction, two flexible pipes 15
Song, the height reduction of U-tube 14 is more, and the degree of crook of flexible pipe 15 is bigger, and the height adjustable adjusting range of the U-tube 14 is
10-28cm, the height of U-tube 14 is determined according to the quantity of sample in extraction cylinder 3, to reach optimum extraction effect.
Wherein, the material of the U-tube 14 is polytetrafluoroethylene (PTFE).
The concrete operations flow of the utility model embodiment is as follows：
Will after sample comminution load sample sack 9 in, by sample sack 9 be put into extraction cylinder 3 in etc. it is to be leached；
According to the quantity of sample adjust U-tube 14 height, make U-tube 14 height be beyond height of specimen 3-4cm, then
According to the quantity of sample, appropriate petroleum ether solvent is taken to add in round-bottomed flask；
Heated water bath pot 6, evaporate the petroleum ether in round-bottomed flask, oil ether fume enters condenser 4 by side pipe 5,
By the cooling of condensed water, oil ether fume condensing reflux, which enters in extraction cylinder 3, to be extracted；
When the petroleum ether liquid level in extraction cylinder 3 exceedes U-tube 14, the petroleum ether dissolved with extraction fat passes through rainbow
Suction pipe 2 flows back in round-bottomed flask, and oil ether fume is pure solvent vapour；
After sample extraction is complete, continue heated water bath pot 6, open flexible pipe 15 and the connection of siphon pipe backflow import 13, return
Solvent is received, collects sample residues.
The utility model embodiment also provides following experimental data
(1) regulating effect on siphon pipe height：
From upper table data, when the U-tube of siphon pipe is highly 28cm, only extraction 12 times in 8 hours, with U-tube height
The reduction of degree, extracting times gradually rise, and can reach 34 times during 11cm, surface, for the difference of required extraction sample size, adjust
The height of section U-tube can make sample extraction reach optimum efficiency.
(2) effect of side pipe increase insulation material
When U-tube is highly 25cm, side pipe does not use the return time of insulation material, and for 56 minutes, side pipe was using insulation
The return time of material is 52 minutes；It can be seen that.Opposite side pipe uses insulation material, can reduce by 7.7% time, play energy efficiency
Effect.
Adjustment type fat diffuser provided by the utility model, increases capacity, improves disposal ability, by using big
The flask of capacity, demand of the varying number sample to different solvents amount is met, solvent evaporation is stable, improves extracting efficiency；
Height Adjustable siphon pipe is set, meets the extraction to varying number sample, operation is simplified, improves extracting efficiency.
Preferred embodiment of the present utility model is the foregoing is only, it is all at this not to limit the utility model
Within the spirit and principle of utility model, any modification, equivalent substitution and improvements made etc., the utility model should be included in
Protection domain within.
Claims (10)
1. a kind of adjustment type fat diffuser, including extraction flask, extraction cylinder and condenser, the extraction flask is immersed in water-bath
Pot in, it is described extraction cylinder by described in the Bian Guanyu of side extract flask connect, it is described extraction cylinder opposite side be provided with it is described
The siphon pipe of flask connection is extracted, the upper end of the extraction cylinder connects with the lower port of the condenser, it is characterised in that described
Extract the flask that flask is preset capacity, the siphon pipe includes two flexible pipes and a U-tube, the U-tube respectively with two
The upper end connection of the flexible pipe, wherein the lower end of a flexible pipe connects with the bottom side of the extraction cylinder, another described soft
The lower end of pipe connects with the extraction flask.
2. adjustment type fat diffuser as claimed in claim 1, it is characterised in that the bottom of a pan of the water-bath be provided with it is described
The flask support of flask adaptation.
3. adjustment type fat diffuser as claimed in claim 1, it is characterised in that stay-warm case is provided with the upside of the water-bath,
The stay-warm case is adapted to the flask.
4. adjustment type fat diffuser as claimed in claim 1, it is characterised in that the upper end of condenser goes out provided with cooling water
The mouth of a river, the condenser lower end are provided with cooling water intake.
5. adjustment type fat diffuser as claimed in claim 1, it is characterised in that the lower end of the side pipe is located in the burning
In the bottleneck of bottle, the upper end of the side pipe connects with the upside of the extraction cylinder.
6. adjustment type fat diffuser as claimed in claim 1, it is characterised in that the outside of the side pipe is provided with thermal insulating material
Material.
7. adjustment type fat diffuser as claimed in claim 1, it is characterised in that the bottom side of the extraction cylinder is provided with siphon pipe
Bypass outlet, the siphon pipe bypass outlet are connected with the lower end of wherein one flexible pipe；The bottleneck of the flask is provided with rainbow
Suction pipe backflow import, the siphon pipe backflow import are connected with the lower end of another flexible pipe.
8. adjustment type fat diffuser as claimed in claim 1, it is characterised in that the material of the flexible pipe is organosilicon rubber
Glue.
9. adjustment type fat diffuser as claimed in claim 1, it is characterised in that the height adjustable adjusting range of the U-tube
For 10-28cm.
10. adjustment type fat diffuser as claimed in claim 1, it is characterised in that the material of the U-tube is polytetrafluoroethyl-ne
Alkene.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720603998.3U CN206823221U (en) | 2017-05-26 | 2017-05-26 | A kind of adjustment type fat diffuser |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720603998.3U CN206823221U (en) | 2017-05-26 | 2017-05-26 | A kind of adjustment type fat diffuser |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206823221U true CN206823221U (en) | 2018-01-02 |
Family
ID=60773808
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720603998.3U Expired - Fee Related CN206823221U (en) | 2017-05-26 | 2017-05-26 | A kind of adjustment type fat diffuser |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206823221U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108579123A (en) * | 2018-04-08 | 2018-09-28 | 太极集团四川南充制药有限公司 | The method for extracting liposoluble constituent with solvent recovery integrated apparatus using fat-soluble ingredient cycle extraction |
| CN113693457A (en) * | 2021-09-16 | 2021-11-26 | 杭州老板电器股份有限公司 | Steaming oven with oil refining function and refining control method of animal fat |
-
2017
- 2017-05-26 CN CN201720603998.3U patent/CN206823221U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108579123A (en) * | 2018-04-08 | 2018-09-28 | 太极集团四川南充制药有限公司 | The method for extracting liposoluble constituent with solvent recovery integrated apparatus using fat-soluble ingredient cycle extraction |
| CN113693457A (en) * | 2021-09-16 | 2021-11-26 | 杭州老板电器股份有限公司 | Steaming oven with oil refining function and refining control method of animal fat |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180102 Termination date: 20200526 |