CN206783802U

CN206783802U - Electric deposition device

Info

Publication number: CN206783802U
Application number: CN201720479384.9U
Authority: CN
Inventors: 刘涛; 姜姗姗; 王中慧
Original assignee: Luliang University
Current assignee: Luliang University
Priority date: 2017-05-03
Filing date: 2017-05-03
Publication date: 2017-12-22
Anticipated expiration: 2027-05-03

Abstract

The utility model discloses a kind of electrochemical reaction appts, more particularly to a kind of electric deposition device；It can adjust the balance of consersion unit, improve reaction rate and cleaning reaction chamber can be made to become more convenient；The utility model includes case lid, casing, four pack supports, power line, rectifier, negative electrode, anode, motor, agitating paddle, contiguous block, chain, driving wheel, driven pulley, lever, control-rod and cleaning plate, motor is located on the upside of case lid, agitating paddle is located in casing, motor output end bottom is connected through case lid with agitating paddle top, lever is vertically connected on driving wheel side, chain bottom is fixedly connected with control-rod top, by osculum with being communicated outside casing inside reaction chamber, the output end of drainpipe is provided with door, support includes top plate, threaded rod, screwed pipe, left spring, right spring, ball bearing and base, it is connected on the upside of top plate with bottom half.

Description

Electric deposition device

Technical field

The technical field of electrochemical reaction appts is the utility model is related to, more particularly to a kind of electric deposition device.

Background technology

It is well known that electric deposition device is the usual means that electrodeposit reaction is carried out in industrial production and scientific experiment, Electrolytic etching of metal is smelted and is used widely in laboratory, and the utility model is mainly for the electric deposition device for laboratory It is illustrated and illustrates, the significant difference of its electric deposition device with being used in electrolytic etching of metal field of smelting is its volume more It is small, it is necessary to complete workload it is also smaller, simply its can reach experiment purpose；Electric deposition device bag in existing laboratory Casing, case lid, power line, rectifier, anode and negative electrode are included, reaction chamber is provided with casing, charging aperture is provided with the top of reaction chamber, enters Material mouth is communicated with reaction chamber, and case lid is located at charging aperture, and rectifier is located on casing lateral wall, and the negative electrode and anode are respectively provided with On box inside wall, the negative electrode and anode electrically connect with rectifier and power line successively, in use, by electrolyte through charging Mouth is injected into reaction chamber, and power line external power supply makes negative electrode and anode strap direct current in the presence of rectifier, and charged particle exists Under electric field action, displacement occurs to male or female, so as to be enriched with material needed for precipitation；Find, placing in its use It is often uneven due to placing place during electric deposition device, there is electrodeposition apparatus imbalance, so as to influence electrolyte in reaction chamber In distribution, cause reaction effect poor, with the progress of reaction, the concentration of charged particle reduces, and causes reaction rate slack-off, After the completion of reaction, because reacted solution and sediment band are corrosive, unsuitable direct body contact, cause cleaning not side Just.

Utility model content

In order to solve the above technical problems, the utility model provides a kind of balance that can adjust consersion unit, improves reaction speed The electric deposition device of rate and easy cleaning.

Electrodeposition apparatus of the present utility model, including case lid, casing, power line, rectifier, negative electrode and anode, in casing Provided with reaction chamber, charging aperture is provided with the top of reaction chamber, charging aperture is communicated with reaction chamber, and case lid is located at charging aperture, rectifier peace On casing lateral wall, the negative electrode and anode are arranged on box inside wall, the negative electrode and anode successively with rectification Device and power line electrical connection, in addition to four pack supports, motor, agitating paddle, contiguous block, chain, driving wheel, driven pulley, lever, Connecting rod, control-rod and cleaning plate, the motor are located on the upside of case lid, and the agitating paddle is located in reaction chamber, the motor Bottom output end is connected through case lid with agitating paddle；Connect on the downside of the contiguous block with the front side wall top of casing and rear wall top Connect, and wall box is stretched out in contiguous block rear end, and chute, driving wheel and driven pulley the center difference are provided with inside the contiguous block The first rotary shaft and the second rotary shaft are provided with, the driven pulley is connected by the second rotary shaft with the front end of the chute, institute State driving wheel to be connected with the rear end of the chute by the first rotary shaft, and one end of first rotary shaft passes contiguous block The bottom of side wall and connecting rod connects, and the top of connecting rod and the lever vertical connection, the driving wheel lead to driven pulley Chain connection is crossed, the chain bottom is fixedly connected with control-rod top, and the control-rod bottom is connected with cleaning plate, and described Plate is cleared up perpendicular to horizontal plane, the left end and right-hand member of the cleaning plate contact with the left side wall and right side wall of casing respectively, described The right anterior angle of bottom half and right relief angle are equipped with drainpipe, and the drainpipe is communicated with reaction chamber, and the output end of drainpipe is provided with Door；Four pack support includes top plate, threaded rod, screwed pipe, left spring, right spring, left support bar, right support bar and bottom Seat, the base upside are provided with standing groove, ball bearing are provided with standing groove, the screwed pipe is inserted into ball bearing Interior, simultaneously spiral shell is filled to inside screwed pipe top for the threaded rod bottom insertion, and the threaded rod top is connected with the top plate lower end, The bottom of the left support bar and the bottom of right support bar are connected with the left side on the top of base and right side respectively, the left support The top of bar and the top of right support bar are connected with the bottom of left spring and the bottom of right spring respectively, the left spring and right bullet The top of spring is connected with the left side of top plate bottom and right side respectively, four groups of top plate tops respectively with casing bottom front left side, Forward right side, left rear side connect with right lateral side.

Electrodeposition apparatus of the present utility model, in addition to blast pipe, gas collection case, relief valve and three-way connection, it is described The input of blast pipe is connected with case lid, and the blast pipe communicates with reaction chamber, and the supervisor of gas collection case and three-way connection connects Connect, the output end and relief valve of the blast pipe are connected with two looped pipelines of three-way connection respectively.

Electrodeposition apparatus of the present utility model, in addition to chuck, the chuck are covered on the outside of casing, the chuck and case External side wall is provided with cooling chamber, and the chuck upper and lower part is respectively equipped with water injection pipe and outlet pipe, the water injection pipe and water outlet Guan Junyu cooling chambers communicate.

Electrodeposition apparatus of the present utility model, in addition to several helical coiled tubes, the helical coiled tube is positioned at cooling Intracavitary, and the input of the helical coiled tube and output end connect with the water injection pipe and outlet pipe respectively.

Electrodeposition apparatus of the present utility model, in addition to rotary nozzle and feed pipe, the rotary nozzle are arranged on casing Inside top, the feed pipe connect through casing with the rotary nozzle.

The beneficial effects of the utility model are compared with prior art：By above-mentioned setting, in use, by rotating screw thread Pipe, screwed pipe produce relative motion with threaded rod so that the total length of screwed pipe and threaded rod changes, adjustable support Just, so as to the balance of adjustment equipment；After equipment adjustment balance, according to being actually needed, it would be desirable to which the experiment product reacted is put In in reaction chamber, it is connected respectively with negative electrode and anode, reaction chamber is injected the electrolyte into by charging aperture, power line switches on power, Form electric field between negative electrode and anode, the charged particle in electrolyte is reacted in the presence of electric field, with entering for reaction OK, the concentration of electrolyte gradually reduces, and particle distribution is gradually uneven, and reaction speed slows down, and the rotation of motor driven agitating paddle can promote Enter the motion of particle, beneficial to the diffusion of particle, so as to improve reaction rate；After the completion of question response, drainpipe baffle plate is opened, will be anti- Electrolyte discharge after answering, takes out experiment product, rotating operation handle, and lever drives driving wheel rotation, the rotation drive of driving wheel Control-rod and cleaning plate on chain move forward and backward, and cleaning plate, which moves forward and backward, can promote deposit to aggregation at drainpipe, so that Realize the cleaning of reaction chamber.

Brief description of the drawings

Fig. 1 is structural representation of the present utility model；

Fig. 2 is right view of the present utility model；

Fig. 3 is the partial enlarged drawing in A portions in this Fig. 1；

Fig. 4 is the structural representation of driving wheel of the present utility model；

Fig. 5 is chuck internal structure schematic diagram of the present utility model.

Embodiment

With reference to the accompanying drawings and examples, specific embodiment of the present utility model is described in further detail.Below Embodiment is used to illustrate the utility model, but is not limited to the scope of the utility model.

As shown in Figures 1 to 5, electrodeposition apparatus of the present utility model, including case lid 1, casing 2, power line 4, rectifier, Negative electrode 6 and anode 7, casing 2 is interior to be provided with reaction chamber, is provided with charging aperture at the top of reaction chamber, charging aperture communicates with reaction chamber, case lid 1 It is located at charging aperture, rectifier is arranged on the lateral wall of casing 2, and negative electrode 6 and anode 7 are arranged on box inside wall, negative electrode 6 Electrically connected successively with rectifier and power line 4 with anode 7, in addition to four pack supports 3, motor 8, agitating paddle 9, contiguous block 10, chain Bar 11, driving wheel 12, driven pulley 13, lever 14, connecting rod 141, control-rod 15 and cleaning plate 16, motor 8 are located on case lid 1 Side, agitating paddle 9 are located in reaction chamber, and the bottom output end of motor 8 is connected through case lid 1 with agitating paddle 9；The downside of contiguous block 10 with The front side wall top of casing 2 connects with rear wall top, and the side wall of casing 2 is stretched out in the rear end of contiguous block 10, is set inside contiguous block 10 There is chute, driving wheel 12 and the center of driven pulley 13 are respectively arranged with the first rotary shaft and the second rotary shaft, and driven pulley 13 passes through The front end of two rotary shafts and chute is connected, and driving wheel 12 is connected by the rear end of the first rotary shaft and chute, and the first rotary shaft One end pass the side wall of contiguous block 14 and be connected with the bottom of connecting rod 14, the top of connecting rod 141 is vertical with lever 14 to be connected Connect, driving wheel 12 is connected with driven pulley 13 by chain 11, and the bottom of chain 11 is fixedly connected with the top of control-rod 15, control-rod 15 Bottom is connected with cleaning plate 16, and clears up plate 16 perpendicular to horizontal plane, clears up left end and the right-hand member left side with casing 2 respectively of plate 16 Side wall and right side wall contact, the bottom, right anterior angle of casing 2 and right relief angle are equipped with drainpipe 17, and drainpipe 17 communicates with reaction chamber, The output end of drainpipe 17 is provided with door；Four pack supports 3 include top plate 31, threaded rod 32, screwed pipe 33, left spring 34, the right side Spring 35, left support bar 37, right support bar 38 and base 39, the upside of base 39 are provided with standing groove, rolling are provided with standing groove Pearl bearing 36, screwed pipe 33 are inserted into ball bearing 36, and simultaneously spiral shell is filled to inside the top of screwed pipe 33 insertion of the bottom of threaded rod 32, The top of threaded rod 32 is connected with the lower end of top plate 31, the bottom of left support bar 37 and the bottom of right support bar 38 respectively with base 39 The left side on top connects with right side, the top of left support bar 37 and the top of right support bar 38 respectively with the bottom of left spring 34 and The top of the bottom connection of right spring 35, left spring 34 and right spring 35 is connected with the left side of the bottom of top plate 31 and right side respectively, Four groups of tops of top plate 31 are connected with the bottom front left side of casing 2, forward right side, left rear side and right lateral side respectively., can by above-mentioned setting To adjust the balance of consersion unit, improve reaction rate and easy cleaning reaction chamber.

Electric deposition device of the present utility model, in addition to blast pipe 18, gas collection case 19, relief valve 20 and three-way connection 21, the input of blast pipe 18 is connected with case lid 1, and blast pipe 18 communicates with reaction chamber, gas collection case 19 and three-way connection 21 Supervisor connection, the output end and relief valve 20 of blast pipe 18 are connected with two looped pipelines of three-way connection 21 respectively.Set by above-mentioned Put, can be by caused gas collection in reaction chamber into gas collection case, the setting of relief valve can avoid gas collection case In gas it is excessive and produce blast, improve the security of equipment.

Electrodeposition apparatus of the present utility model, in addition to chuck 22, chuck 22 are covered in the outside of casing 2, chuck 22 and case The lateral wall of body 2 is provided with cooling chamber, and the upper and lower part of chuck 22 is respectively equipped with water injection pipe 23 and outlet pipe 24, water injection pipe 23 and water outlet Pipe 24 communicates with cooling chamber.By above-mentioned setting, cold water can be injected into cooling chamber by water injection pipe, is produced in absorbing reaction Raw heat.

Electrodeposition apparatus of the present utility model, in addition to helical coiled tube 25, helical coiled tube 25 are located in cooling chamber, and The input and output end of helical coiled tube 25 connect with water injection pipe 23 and outlet pipe 24 respectively；By above-mentioned setting, can drop The flow velocity of cold water in low cooling chamber, extend the time of cold water survival in chuck, increase heat exchange area, improve the efficiency of heat absorption, Using water wisely.

Electrodeposition apparatus of the present utility model, in addition to rotary nozzle 26 and feed pipe 27, rotary nozzle 26 are arranged on case The inside top of body 2, feed pipe 27 connect through casing 2 with rotary nozzle 26；, after completion of the reaction, will be for by above-mentioned setting Water pipe accesses water source, is rinsed by rotary nozzle to reaction cavity wall water spray, meanwhile, it is used cooperatively, makes clear with cleaning plate Washing becomes more convenient.

In use, by the screwed pipe in swinging mounting, screwed pipe is set to produce relative motion with threaded rod so that screwed pipe Changed with the total length of threaded rod, so as to the balance of adjustment equipment；Cold water is injected into cooling chamber by water injection pipe, exchanged heat Cold water afterwards is discharged from outlet pipe, after equipment adjustment balance, case lid is opened, according to being actually needed, it would be desirable to the reality reacted The product of testing are placed in reaction chamber, are connected respectively with negative electrode and anode, are injected the electrolyte into reaction chamber by charging aperture, are switched on power, Charged particle in electrolyte is reacted in the presence of electric field, as the progress of reaction, the particle concentration of electrolyte are gradual Reduce, Particle diffusion slows, and causes reaction speed to slow down, and motor driven agitating paddle rotates the motion that can accelerate particle, profit In the diffusion of particle, so as to improve reaction rate, the cold water of chuck can be with caused heat in absorbing reaction, the baffle plate in chuck Residence time of the cold water in chuck can be extended, improves the efficiency of heat absorption, using water wisely, caused gas leads in reaction chamber Cross blast pipe to enter in gas collection case through three-way connection, when the gas in gas collection case is excessive, relief valve is in pressure In the presence of lose heart, the collective effect of exhaust outlet and gas collector can collect caused gas in reaction, relief valve Set and improve the security of equipment, after the completion of question response, open drainpipe baffle plate, reacted electrolyte is discharged, then Experiment product is taken out, feed pipe is accessed into water source, is rinsed by rotary nozzle to reaction cavity wall water spray, while rotating operation Handle, lever drive driving wheel to rotate by connecting rod, before and after the control-rod and cleaning plate on the rotation drive chain of driving wheel Motion, cleaning plate, which moves forward and backward, can promote deposit and water for cleaning to clear up plate and rotary nozzle to aggregation, discharge at drainpipe Collective effect, cleaning is become more convenient.

Described above is only preferred embodiment of the present utility model, it is noted that for the common skill of the art For art personnel, on the premise of the utility model technical principle is not departed from, some improvement and modification can also be made, these change Enter and also should be regarded as the scope of protection of the utility model with modification.

Claims

1. a kind of electric deposition device, including case lid（1）, casing（2）, power line（4）, rectifier, negative electrode（6）And anode（7）, case Body（2）It is interior to be provided with reaction chamber, charging aperture is provided with the top of reaction chamber, charging aperture communicates with reaction chamber, case lid（1）It is located at charging aperture Place, rectifier are arranged on casing（2）On lateral wall, the negative electrode（6）And anode（7）It is arranged on box inside wall, it is described Negative electrode（6）And anode（7）Successively with rectifier and power line（4）Electrical connection, it is characterised in that also including four pack supports（3）, electricity Machine（8）, agitating paddle（9）, contiguous block（10）, chain（11）, driving wheel（12）, driven pulley（13）, lever（14）, connecting rod （141）, control-rod（15）With cleaning plate（16）, the motor（8）Positioned at case lid（1）Upside, the agitating paddle（9）Positioned at reaction Intracavitary, the motor（8）Bottom output end pass through case lid（1）With agitating paddle（9）Connection；The contiguous block（10）Downside and case Body（2）Front side wall top connected with rear wall top, and contiguous block（10）Casing is stretched out in rear end（2）Side wall, the contiguous block （10）Inside is provided with chute, the driving wheel（12）And driven pulley（13）Center is respectively arranged with the first rotary shaft and second and rotated Axle, the driven pulley（13）It is connected by the second rotary shaft with the front end of the chute, the driving wheel（12）Pass through first turn Moving axis is connected with the rear end of the chute, and one end of first rotary shaft passes contiguous block（14）Side wall and connecting rod （14）Bottom connection, connecting rod（141）Top and the lever（14）Vertical connection, the driving wheel（12）With it is driven Wheel（13）Pass through chain（11）Connection, the chain（11）Bottom and control-rod（15）Top is fixedly connected, the control-rod （15）Bottom and cleaning plate（16）Connection, and the cleaning plate（16）Perpendicular to horizontal plane, the cleaning plate（16）Left end and Right-hand member respectively with casing（2）Left side wall and right side wall contact, the casing（2）Bottom, right anterior angle and right relief angle are equipped with draining Pipe（17）, the drainpipe（17）Communicated with reaction chamber, drainpipe（17）Output end be provided with door；Four pack support（3） Include top plate（31）, threaded rod（32）, screwed pipe（33）, left spring（34）, right spring（35）, left support bar（37）, right branch Strut（38）And base（39）, the base（39）Upside is provided with standing groove, and ball bearing is provided with standing groove（36）, institute State screwed pipe（33）It is inserted into ball bearing（36）It is interior, the threaded rod（32）Simultaneously spiral shell is filled to screwed pipe for bottom insertion（33）Top Inside, the threaded rod（32）Top and the top plate（31）Lower end connects, the left support bar（37）Bottom and right support Bar（38）Bottom respectively with base（39）The left side on top connected with right side, the left support bar（37）Top and right branch Strut（38）Top respectively with left spring（34）Bottom and right spring（35）Bottom connection, the left spring（34）And the right side Spring（35）Top respectively with top plate（31）The left side of bottom connects with right side, four groups of top plates（31）Top respectively with case Body（2）Bottom front left side, forward right side, left rear side connect with right lateral side.

2. electric deposition device as claimed in claim 1, it is characterised in that also including blast pipe（18）, gas collection case（19）、 Relief valve（20）And three-way connection（21）, the blast pipe（18）Input and case lid（1）Connection, the blast pipe（18）With Reaction chamber communicates, gas collection case（19）With three-way connection（21）Supervisor connection, the blast pipe（18）Output end and let out Pressure valve（20）Respectively with three-way connection（21）Two looped pipelines connection.

3. electric deposition device as claimed in claim 2, it is characterised in that also including chuck（22）, the chuck（22）Covering In casing（2）Outside, the chuck（22）With casing（2）Lateral wall is provided with cooling chamber, the chuck（22）Upper and lower part point She You not water injection pipe（23）And outlet pipe（24）, the water injection pipe（23）And outlet pipe（24）Communicated with cooling chamber.

4. electric deposition device as claimed in claim 3, it is characterised in that also including several helical coiled tubes（25）, it is described Helical coiled tube（25）In cooling chamber, and the helical coiled tube（25）Input and output end respectively with the water filling Pipe（23）And outlet pipe（24）Connection.

5. electric deposition device as claimed in claim 4, it is characterised in that also including rotary nozzle（26）And feed pipe（27）, The rotary nozzle（26）Installed in casing（2）Inside top, the feed pipe（27）Through casing（2）With the rotary nozzle （26）Connection.