CN206701272U - A kind of multistage purification devices of medicine intermediate - Google Patents

A kind of multistage purification devices of medicine intermediate Download PDF

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Publication number
CN206701272U
CN206701272U CN201720490749.8U CN201720490749U CN206701272U CN 206701272 U CN206701272 U CN 206701272U CN 201720490749 U CN201720490749 U CN 201720490749U CN 206701272 U CN206701272 U CN 206701272U
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CN
China
Prior art keywords
decoction
feed hopper
reative cell
purification devices
purifying room
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Expired - Fee Related
Application number
CN201720490749.8U
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Chinese (zh)
Inventor
张桂友
金育岐
修振宁
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LIANYUNGANG HENGFEI PHARMACEUTICAL Co Ltd
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LIANYUNGANG HENGFEI PHARMACEUTICAL Co Ltd
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Priority to CN201720490749.8U priority Critical patent/CN206701272U/en
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Publication of CN206701272U publication Critical patent/CN206701272U/en
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Abstract

The utility model discloses a kind of multistage purification devices of medicine intermediate, including feed hopper, reative cell and purifying room, it is connected at the top of the bottom of the feed hopper and reative cell, mixing arrangement is provided with the reative cell, the bottom of the reative cell is connected by efferent duct and purifying room, the end that the purifying room corresponds to efferent duct, which is provided with, rocks groove, the purifying interior is provided with adsorption plate, the inwall on the periphery of the adsorption plate and purifying room is fixedly mounted, the bottom of the purifying room is by adsorption plate formed with connecing liquid storehouse, the side top for connecing liquid storehouse is connected with discharge pipe, and catch box is connected with by discharge pipe.The medicine intermediate multistage purification devices, it is simple to operate, before to decoction purification process to decoction hybrid reaction after, purified after reaction, improve decoction purifying effect.

Description

A kind of multistage purification devices of medicine intermediate
Technical field
It the utility model is related to technical field of medical equipment, more particularly to a kind of multistage purification devices of medicine intermediate.
Background technology
Medicine intermediate is some for some industrial chemicals or chemical products in medicine synthesis process, thisization Chemical product, it is not necessary to the production licence of medicine, can be produced in common chemical plant, as long as reaching the rank of some, you can Synthesis for medicine.In medicine intermediate building-up process, it is often necessary to which the compound for synthesizing or extracting to obtain is divided From purification, single compound or a kind of compound with identical structure parent nucleus are obtained, medicine is pure to medicine in manufacturing process Degree requires high, it is necessary to be separated to the impurity in medicine material, and traditional separate mode is separated using filter screen more, Filtered using this method, it is necessary to carry out repeating screening to raw material, time-consuming, effect is poor, in view of stating defect, is necessary design one in fact Kind isolates and purifies device and is improved device.But device is isolated and purified at present, can not be thoroughly mixed by it before being separated to intermediate Separated after conjunction, causing inferior separating effect, and operating efficiency is relatively low.
Utility model content
The purpose of this utility model is and a kind of medicine intermediate proposed in order to solve shortcoming present in prior art Multistage purification devices.
To achieve these goals, the utility model employs following technical scheme:
A kind of multistage purification devices of medicine intermediate, including feed hopper, reative cell and purifying room, the bottom of the feed hopper It is connected at the top of portion and reative cell, mixing arrangement is provided with the reative cell, the bottom of the reative cell passes through output Pipe is connected with purifying room, and the end that the purifying room corresponds to efferent duct, which is provided with, rocks groove, and the purifying interior is provided with Adsorption plate, the inwall on the periphery and purifying room of the adsorption plate are fixedly mounted, and the bottom of the purifying room is formed by adsorption plate Liquid storehouse is connect, the side top for connecing liquid storehouse is connected with discharge pipe, and is connected with catch box by discharge pipe.
Preferably, sealing plate is provided with the top of the feed hopper, and feed liquor input pipe is provided with by sealing plate.Right When injection needs the intermediate decoction purified in feed hopper, medical liquid container is connected by feed liquor input pipe, improved at decoction purifying The wholesomeness of reason, ensure the quality of intermediate decoction.
Preferably, the output port that feed hopper is corresponded in the feed hopper is provided with multigroup back-up ring in gradually small shape.In medicine Liquid, which enters after feed hopper, is arranged decoction after the multiple obstruction of decoction by the bottom of feed hopper by the back-up ring in feed hopper side wall Enter in reative cell, decoction premixing is handled.
Preferably, the mixing arrangement includes rotation seat, rotary shaft and hybrid blade, and the hybrid blade corresponds to feed hopper Bottom be fixedly mounted on the rotating shaft, the both ends of the rotary shaft pass through the rotation seat inwall relative with reative cell and fix company Connect.After decoction in feed hopper enters reative cell, decoction falls on hybrid blade, and hybrid blade is turned by heave hand turn moving axis Dynamic, rotary shaft is rotated by rotation seat, so as to be sufficiently mixed reaction to the decoction in reative cell, is advantageous to decoction purification process.
Preferably, described rock corresponds to the end of efferent duct and is provided with back round in groove, described to rock opposite side pair in groove Round should be returned and be provided with outage, the internal diameter of the outage is more than back the internal diameter of round.Mixed decoction leads in reative cell Cross efferent duct and enter that purifying is indoor to rock in groove, due to decoction by efferent duct fall caused by impulsive force enter and rock Groove, discharged by the outage for rocking groove opposite side, the decoction at the place of row does not drain into purifying interior by returning round, improves intermediate Decoction hybrid reaction effect.
Preferably, the adsorption plate is at least provided with three groups, and is set between adsorption plate using gradually close shape layering.Hierarchical layered The contaminant filter in intermediate decoction is removed by the adsorption plate of different densities, improves the effect of decoction purifying.
Preferably, transparent scale line is provided with the catch box.After in purifying room, decoction after purification enters catch box, The capacity of catch box inner liquid medicine is checked by the transparent scale line on catch box, is measured as needed.
In the utility model, decoction is entered by feed liquor input pipe will by the back-up ring in feed hopper side wall after feed hopper Decoction after the multiple obstruction of decoction, after entering reative cell after being pre-mixed to decoction, decoction falls on hybrid blade, and hybrid blade is by weight Rotary shaft is driven to rotate, rotary shaft is rotated by rotation seat, and reaction is sufficiently mixed to the decoction in reative cell, is mixed in reative cell Decoction afterwards enters that purifying is indoor to rock in groove by efferent duct, due to decoction by efferent duct fall caused by impulsive force Into groove is rocked, discharged by the outage for rocking groove opposite side, the decoction at the place of row does not drain into purifying interior by returning round, leads to The adsorption plate hierarchical classification for crossing different densities removes to the contaminant filter in intermediate decoction, and decoction after purification enters purifying room Bottom Jie Ye storehouses in, and by connecing in discharge pipe dispatch to the catch box above the side of liquid storehouse.The medicine intermediate multistage is pure Makeup is put, simple to operate, before to decoction purification process to decoction hybrid reaction after, purified after reaction, improve decoction it is pure The effect of change.
Brief description of the drawings
Fig. 1 be the utility model proposes a kind of medicine intermediate multistage purification devices structural representation;
Fig. 2 be the utility model proposes a kind of medicine intermediate multistage purification devices feeding hopper structure schematic diagram;
Fig. 3 be the utility model proposes the multistage purification devices of medicine intermediate a kind of rock slot structure schematic diagram.
In figure:1 feed hopper;11 sealing plates;111 feed liquor input pipes;12 back-up rings;2 reative cells;21 mixing arrangements;211 rotate Seat;212 rotary shafts;213 hybrid blades;22 efferent ducts;3 purifying rooms;31 rock groove;311 times rounds;312 taps;32 absorption Plate;33 connect liquid storehouse;331 discharge pipes;332 catch boxs;333 transparent scale lines.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole Embodiment.
Reference picture 1-3, a kind of multistage purification devices of medicine intermediate, including feed hopper 1, reative cell 2 and purifying room 3, The top of the feed hopper 1 is provided with sealing plate 11, and sealing plate 11 is provided with feed liquor input pipe 111.To feed hopper 1 When interior injection needs the intermediate decoction purified, medical liquid container is connected by feed liquor input pipe 111, improves decoction purification process Wholesomeness, ensure the quality of intermediate decoction.Corresponded in the feed hopper 1 feed hopper 1 output port be provided with it is multigroup in gradually The back-up ring 12 of small shape.Decoction enter feed hopper 1 after by the back-up ring 12 in the side wall of feed hopper 1 by the multiple obstruction of decoction after medicine Liquid is discharged into reative cell 2 by the bottom of feed hopper 1, and decoction premixing is handled.The bottom of the feed hopper 1 and reative cell 2 Top be connected, be provided with mixing arrangement 21 in the reative cell 2, the mixing arrangement 21 includes rotation seat 211, rotated Axle 212 and hybrid blade 213, the bottom of the corresponding feed hopper 1 of the hybrid blade 213 is fixedly mounted in rotary shaft 212, described The both ends of rotary shaft 212 are fixedly connected by the inwall relative with reative cell 2 of rotation seat 211.Decoction in feed hopper 1 enters After reative cell 2, decoction falls on hybrid blade 213, and hybrid blade 213 is rotated by heave hand turn moving axis 212, and rotary shaft 212 is logical Cross rotation seat 211 to rotate, so as to be sufficiently mixed reaction to the decoction in reative cell 2, be advantageous to decoction purification process.The reaction The bottom of room 2 is connected by efferent duct 22 and purifying room 3, and the end of the corresponding efferent duct 22 in purifying room 3 is provided with rolling Dynamic groove 31, described rock corresponds to the end of efferent duct 22 and is provided with back round 311 in groove 31, described to rock opposite side pair in groove 31 Round 311 should be returned and be provided with outage 312, the internal diameter of the outage 312 is more than back the internal diameter of round 311.Mixed in reative cell 2 Decoction after conjunction enters rocking in groove 31 in purifying room 3 by efferent duct 22, due to being produced when decoction is fallen by efferent duct 22 Raw impulsive force, which enters, rocks groove 31, is discharged by the outage 312 for rocking the opposite side of groove 31, and the decoction for not arranging place passes through the row of going back to Hole 311 is drained into purifying room 3, improves intermediate decoction hybrid reaction effect.Adsorption plate 32, institute are provided with the purifying room 3 The inwall for stating the periphery of adsorption plate 32 and purifying room 3 is fixedly mounted, the adsorption plate 32 at least provided with three groups, and adsorption plate 32 it Between set using the layering of gradually close shape.Hierarchical layered is gone by the adsorption plate 32 of different densities to the contaminant filter in intermediate decoction Remove, improve the effect of decoction purifying.The bottom of the purifying room 3 by adsorption plate 32 formed with connecing liquid storehouse 33, it is described to connect liquid storehouse 33 side top is connected with discharge pipe 331, and is connected with catch box 332 by discharge pipe 331.Set on the catch box 332 It is equipped with transparent scale line 333.After in purifying room 3, decoction after purification enters catch box 332, by transparent on catch box 332 Graduation mark 333 checks the capacity of the inner liquid medicine of catch box 332, measures as needed.
In the utility model, decoction is entered after feed hopper 1 by the side wall of feed hopper 1 by feed liquor input pipe 111 Back-up ring 12 is by decoction after the multiple obstruction of decoction, and after entering reative cell 2 after being pre-mixed to decoction, decoction falls on hybrid blade 213, Hybrid blade 213 is rotated by heave hand turn moving axis 212, and rotary shaft 212 is rotated by rotation seat 211, to the decoction in reative cell 2 Reaction is sufficiently mixed, mixed decoction enters rocking in groove 31 in purifying room 3 by efferent duct 22 in reative cell 2, due to Decoction falls caused impulsive force into groove 31 is rocked by efferent duct 22, by the outage 312 for rocking the opposite side of groove 31 Discharge, the decoction at the place of row is not drained into purifying room 3 by returning round 312, passes through the hierarchical classification pair of adsorption plate 32 of different densities Contaminant filter in intermediate decoction removes, and decoction after purification enters in the bottom Jie Ye storehouses 33 of purifying room 3, and by connecing liquid In the dispatch of discharge pipe 331 to catch box 332 above the side of storehouse 33.
It is described above, the only preferable embodiment of the utility model, but the scope of protection of the utility model is not This is confined to, any one skilled in the art is in the technical scope that the utility model discloses, according to this practicality New technical scheme and its utility model design are subject to equivalent substitution or change, should all cover in protection model of the present utility model Within enclosing.

Claims (7)

1. a kind of multistage purification devices of medicine intermediate, including feed hopper (1), reative cell (2) and purifying room (3), its feature It is, the bottom of the feed hopper (1) is provided with mixing dress with being connected at the top of reative cell (2) in the reative cell (2) Put (21), the bottom of the reative cell (2) is connected by efferent duct (22) and purifying room (3), and purifying room (3) is corresponding The end of efferent duct (22), which is provided with, rocks groove (31), and adsorption plate (32), the adsorption plate are provided with purifying room (3) (32) periphery and the inwall of purifying room (3) are fixedly mounted, and the bottom of purifying room (3) is by adsorption plate (32) formed with connecing Liquid storehouse (33), the side top for connecing liquid storehouse (33) is connected with discharge pipe (331), and is connected with collection by discharge pipe (331) Liquid case (332).
A kind of 2. multistage purification devices of medicine intermediate according to claim 1, it is characterised in that the feed hopper (1) sealing plate (11) is provided with the top of, and feed liquor input pipe (111) is provided with by sealing plate (11).
A kind of 3. multistage purification devices of medicine intermediate according to claim 1, it is characterised in that the feed hopper (1) output port that feed hopper (1) is corresponded in is provided with multigroup back-up ring (12) in gradually small shape.
A kind of 4. multistage purification devices of medicine intermediate according to claim 1, it is characterised in that the mixing arrangement (21) rotation seat (211), rotary shaft (212) and hybrid blade (213), the corresponding feed hopper (1) of the hybrid blade (213) are included Bottom be fixedly mounted in rotary shaft (212), the both ends of the rotary shaft (212) pass through rotation seat (211) and reative cell (2) Relative inwall is fixedly connected.
5. the multistage purification devices of a kind of medicine intermediate according to claim 1, it is characterised in that described to rock groove () The end of interior corresponding efferent duct (22) is provided with back round (311), and described groove (31) the interior opposite side that rocks correspondingly returns round (311) Outage (312) is provided with, the internal diameter of the outage (312) is more than back the internal diameter of round (311).
A kind of 6. multistage purification devices of medicine intermediate according to claim 1, it is characterised in that the adsorption plate (32) at least provided with three groups, and set between adsorption plate (32) using gradually close shape layering.
A kind of 7. multistage purification devices of medicine intermediate according to claim 1, it is characterised in that the catch box (332) transparent scale line (333) is provided with.
CN201720490749.8U 2017-05-05 2017-05-05 A kind of multistage purification devices of medicine intermediate Expired - Fee Related CN206701272U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112552426A (en) * 2020-12-14 2021-03-26 江苏万力生物科技有限公司 Method and equipment for extracting heparin sodium in porcine small intestine mucosa
CN115007015A (en) * 2022-06-07 2022-09-06 大理原生农业科技有限公司 Preparation device and use method of nutrient solution for paris polyphylla

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112552426A (en) * 2020-12-14 2021-03-26 江苏万力生物科技有限公司 Method and equipment for extracting heparin sodium in porcine small intestine mucosa
CN112552426B (en) * 2020-12-14 2022-03-18 江苏万力生物科技有限公司 Method and equipment for extracting heparin sodium in porcine small intestine mucosa
CN115007015A (en) * 2022-06-07 2022-09-06 大理原生农业科技有限公司 Preparation device and use method of nutrient solution for paris polyphylla

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171205

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