CN206688290U - A kind of device for organic phase and aqueous phase Gravity Separation - Google Patents
A kind of device for organic phase and aqueous phase Gravity Separation Download PDFInfo
- Publication number
- CN206688290U CN206688290U CN201720289415.4U CN201720289415U CN206688290U CN 206688290 U CN206688290 U CN 206688290U CN 201720289415 U CN201720289415 U CN 201720289415U CN 206688290 U CN206688290 U CN 206688290U
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- valve
- tee
- ball valve
- reduced
- conductivity meter
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Abstract
A kind of device for organic phase and aqueous phase Gravity Separation, it is related to a kind of water separation device, described device is by reactor, electromagnetic flowmeter, tee ball valve, repid cut-off valve, reduced tee, reduced flange, conductivity meter and control system composition.Electromagnetic flowmeter, T-shaped tee ball valve, reducer tee are sequentially connected on the main discharging pipeline of reactor；The Article 3 passage of tee ball valve is connected and installed with the small-bore pipeline of conductivity meter and repid cut-off valve by reduced flange, conductivity meter is arranged on the top of repid cut-off valve, the other end connection reduced tee of small-bore pipeline, the power line and signal wire of electric elements are all connected to control system.Separation is initial, is layered by main discharge nozzle, when detecting that fluid flow reaches setting value, turning T-type tee ball valve, continue to be layered by small-bore pipeline, so as to control piper internal water system volume flow, the loss of organic phase is prevented, the separation of liquid liquid two media suitable for Chemical Manufacture.
Description
Technical field
A kind of water system separator is the utility model is related to, can especially be used for the dress of organic phase and aqueous phase Gravity Separation
Put.
Background technology
Usually need to separate organic phase-water system two media during Chemical Manufacture, Gravity Separation is profit
The separation method of different with the density of 2 kinds of media and immiscible principle, because its is easy to operate, equipment simply can directly exist
The separation of 2 kinds of liquid phase mediums is realized in reactor or storage tank, the extensive use in chemical process.At present, Chemical Manufacture
Middle organic phase-water system two media carry out separate use method be：Stop valve is arranged on kettle or storage tank blowing pipeline, is being divided
During layer, valve stays open, and when detecting the interface of aqueous phase and organic phase, closes valve and completes layering.
But due to closing the operating process having time delay of valve, part organic phase can be split into water system, so not only up to not
To the technological requirement being finely layered, and meeting generation environment pollutes, while causes potential safety hazard.
The content of the invention
The purpose of this utility model is to provide a kind of device for organic phase and aqueous phase Gravity Separation, device separation
Later stage is layered using osculum diametered duct, and the flow velocity of aqueous phase is controlled by the volume flow of aqueous phase in control piper, is subtracted
Few organic phase caused by closing valve time delay is lost in, while aqueous phase is in laminar condition, Neng Gouyou in control piper
Effect reduces the organic phase quality being separated in water system, prevents two-phase back-mixing, reaches the requirement of practical implementation.
Technical scheme is as follows used by the utility model solves its technical problem：
A kind of device for organic phase and aqueous phase Gravity Separation, described device is by reactor, electromagnetic flowmeter, T-shaped three
Pass ball valve, repid cut-off valve, reduced tee, reduced flange, conductivity meter and control system composition；The main discharge pipe of reactor
It is upper to be sequentially installed with by flange connection：Electromagnetic flowmeter, T-shaped tee ball valve, reduced tee；Installed on the discharge nozzle of small-bore
There are conductivity meter and pneumatic ball valve, conductivity meter is arranged on above repid cut-off valve；One end of small-bore discharge nozzle passes through reducing
Flange is connected with the 3rd passage of T-shaped tee ball valve, and the other end is connected with reduced tee, the power line of electric elements and
Signal wire is connected to control system.
The advantages of the utility model and effect are：
The utility model is layered in the later stage of separation process using osculum diametered duct, passes through aqueous phase in control piper
Volume flow and then the flow velocity for controlling aqueous phase, reduce the organic phase caused by closing valve time delay and be lost in, control simultaneously
Aqueous phase is in laminar condition in pipeline, prevents two-phase back-mixing, reaches the requirement of practical implementation.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Fig. 2 is Control System NetWork structural representation.
In figure：1st, organic phase, 2, aqueous phase, 3, electromagnetic flowmeter, 4, T-shaped tee ball valve, 5, reduced flange, 6, electrical conductivity
Instrument, 7, repid cut-off valve, 8, reduced tee.
Embodiment
The utility model is further described with reference to the accompanying drawings and examples.
In Fig. 1, electromagnetic flowmeter 3 is arranged on the main discharge pipe of reactor by flange connection, T-shaped tee ball valve 4
Two passages be arranged on the main discharge pipe of reactor, another passage passes through reduced flange 5 and small-bore discharge pipe and connected
Connect, conductivity meter 6 and repid cut-off valve 7 are arranged on small-bore discharge pipe by flange, and conductivity meter 6 is arranged on and quickly cut
The disconnected top of valve 7, the other end connection reducer tee 8 of small-bore discharge pipe, reducer tee 8 are arranged on reaction by flange connection
On the main discharge pipe of kettle.
In fig. 2, controlled stage is the system based on S7-300PLC, and monitoring system uses Siemens WinCC configuration software,
Operating system uses Siemens's TIA softwares, is communicated, realized to live executive component two-by-two by Ethernet between three
Control and condition monitoring.According to the characteristics of water and big organic phase electrical conductivity difference, the flow of water, root are detected using electromagnetic flowmeter
According to the comparison of measurement flow and fluid volume in kettle, prediction separation terminal；Conductivity meter is to separating end reaction high efficient and reliable, profit
With conductivity meter detection stream bulk conductivity, judge to separate terminal.
When layering starts, T-shaped tee ball valve 4 is opened, main discharge pipe is connected and is layered.When electromagnetism on reactor discharge nozzle
When flowmeter 3 detects that fluid flow reaches setting value, to ensure separation accuracy, fluid flow in the unit interval is reduced, rotates T
The valve opening door of type tee ball valve 4 top and right channel, close valve down channel, change fluid flow direction in valve body；Meanwhile change up
Fast stop valve 7, is continued to be layered by small-bore discharge nozzle.When the registration of conductivity meter 6 sports zero, repid cut-off valve 7 is closed, is closed
T-shaped tee ball valve 4 is closed, completes layering.
Claims (1)
1. a kind of device for organic phase and aqueous phase Gravity Separation, it is characterised in that described device is by reactor, Electromagnetic Flow
Meter, T-shaped tee ball valve, repid cut-off valve, reduced tee, reduced flange, conductivity meter and control system composition；Reactor master
It is sequentially installed with discharge pipe by flange connection：Electromagnetic flowmeter, T-shaped tee ball valve, reduced tee；Small-bore discharges
Conductivity meter and pneumatic ball valve are installed, conductivity meter is arranged on above repid cut-off valve on pipe；One end of small-bore discharge nozzle
It is connected by reduced flange with the 3rd passage of T-shaped tee ball valve, the other end is connected with reduced tee, electric elements
Power line and signal wire are connected to control system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720289415.4U CN206688290U (en) | 2017-03-23 | 2017-03-23 | A kind of device for organic phase and aqueous phase Gravity Separation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720289415.4U CN206688290U (en) | 2017-03-23 | 2017-03-23 | A kind of device for organic phase and aqueous phase Gravity Separation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206688290U true CN206688290U (en) | 2017-12-01 |
Family
ID=60442938
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720289415.4U Expired - Fee Related CN206688290U (en) | 2017-03-23 | 2017-03-23 | A kind of device for organic phase and aqueous phase Gravity Separation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206688290U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110152581A (en) * | 2019-05-15 | 2019-08-23 | 巴斯夫新材料有限公司 | Spent acid separation and processing system |
-
2017
- 2017-03-23 CN CN201720289415.4U patent/CN206688290U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110152581A (en) * | 2019-05-15 | 2019-08-23 | 巴斯夫新材料有限公司 | Spent acid separation and processing system |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171201 Termination date: 20180323 |
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| CF01 | Termination of patent right due to non-payment of annual fee |