CN206553412U - It is a kind of to be applied to the carbon carbon frock that melting siliconising method produces carbon ceramic composite material - Google Patents

It is a kind of to be applied to the carbon carbon frock that melting siliconising method produces carbon ceramic composite material Download PDF

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Publication number
CN206553412U
CN206553412U CN201720260445.2U CN201720260445U CN206553412U CN 206553412 U CN206553412 U CN 206553412U CN 201720260445 U CN201720260445 U CN 201720260445U CN 206553412 U CN206553412 U CN 206553412U
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carbon
reative cell
crucible
frock
cushion block
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闫根成
栾吉刚
魏金华
孙永涛
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YANTAI LUHANG MATERIAL SCIENCE AND TECHNOLOGY Co Ltd
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YANTAI LUHANG MATERIAL SCIENCE AND TECHNOLOGY Co Ltd
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Abstract

The utility model is related to a kind of carbon carbon frock for being applied to melting siliconising method production carbon ceramic composite material, the reative cell of cylindrical structure including several self connections, the bottom surface of the reative cell is provided with the crucible for holding silica flour, some cushion blocks are placed with inside the crucible, the top of the cushion block, which is placed, needs silication workpiece, the top of the reative cell is sealed by upper cover plate, and the reative cell, crucible, cushion block and upper cover plate are made by carbon carbon composite.The beneficial effects of the utility model are:Carbon carbon composite has that elevated temperature strength is high, thermal shock resistance is good, and the higher advantage with mechanical property after silicon liquid and silicon steam reaction generation carbon/carbon carborundum, Reusability does not ftracture, reusable and service life is long.

Description

It is a kind of to be applied to the carbon carbon frock that melting siliconising method produces carbon ceramic composite material
Technical field
The utility model is related to a kind of frock, more particularly to a kind of melting siliconising method that is applied to produces carbon ceramic composite material Carbon carbon frock.
Background technology
Carbon/pottery brake material is a kind of high property developed in recent years after powdered metallurgical material and carbon/carbon composite Energy brake material, has broad application prospects in fields such as bullet train, automobile, aircrafts.At present, carbon/pottery brake material Preparation technology mainly has 3 kinds:Chemical vapor infiltration (CVI) technique, precursor dipping-pyrolysis (PIP) technique and melting siliconising (RMI) technique.Compared with CVI and PIP techniques, RMI techniques have short preparation period, cost low and near-net-shape etc. is excellent Point, has become competitive Industrialized processing technique, is that production carbon/pottery brake material mainly produces work both at home and abroad at present Skill.
Needed during melting siliconising method production carbon/pottery brake material the progress siliconising of carbon carbon composite base substrate is anti- Should, the siliconising operation of prior art uses the graphite reative cell of vertical cylinder structure, reative cell be divided into bottom melt silicon area and Top reaction zone two parts, pending carbon/carbon compound material base substrate is placed in the top reaction zone of reative cell, silicon material is put Silicon area heating generation molten silicon is melted in the bottom of reative cell;Molten silicon area and reaction zone are separated with cushion block;Heat the reative cell liter Temperature is to 1650 DEG C~2000 DEG C and vacuumizes, and is incubated 2~8 hours, and molten silicon enters the top reaction zone of reative cell by cushion block, Adsorbed by carbon/carbon composite billet surface and react generation carborundum, it is low that natural or control is cooled to reaction chamber temperature In 150 DEG C, that is, obtain carbon/pottery brake material.Because the mechanical property of graphite material is relatively low, above-mentioned graphite reative cell, molten silicon earthenware Crucible, pillar and cover plate are in hot environment and silicon liquid and silicon steam reaction production carborundum.Due to heating-cooling repeatedly in production process With the effect of thermal stress, easily ftracture, service life is short;Simultaneously because reative cell serious cracking influences the siliconising effect of product.Lead Cause batch production carbon/pottery brake material product quality uniformity is unstable and low production efficiency.
Utility model content
The deficiency that the utility model exists for the graphite reative cell of existing melting siliconising method production carbon ceramic composite material, is carried It is applied to the carbon carbon frock that melting siliconising method produces carbon ceramic composite material for a kind of.
The technical scheme that the utility model solves above-mentioned technical problem is as follows:
It is a kind of to be applied to the carbon carbon frock that melting siliconising method produces carbon ceramic composite material, including several self connections Cylindrical structure reative cell, the bottom surface of the reative cell is provided with the crucible for holding silica flour, if being placed with inside the crucible Dry cushion block, the top of the cushion block, which is placed, needs silication workpiece base substrate, and the top of the reative cell is sealed by upper cover plate, described Reative cell, crucible, cushion block and upper cover plate are made by carbon carbon composite.
The beneficial effects of the utility model are:Carbon carbon composite has elevated temperature strength height, thermal shock resistance good, with silicon liquid And the higher advantage of mechanical property after silicon steam reaction generation carbon/carbon-silicon carbide, Reusability do not ftracture, it is reusable and Service life is long.The shortcoming that graphite frock is easy to crack, service life is short can be effectively solved, siliconising effect is good, and material property is consistent Property it is stable.
Brief description of the drawings
Fig. 1 is the utility model reaction chamber structure schematic diagram;
Fig. 2 is the utility model frock use state structural representation;
In Fig. 1 and Fig. 2,1, reative cell;2nd, crucible;3rd, silica flour;4th, cushion block;5th, silication workpiece base substrate is treated;6th, upper cover plate
Embodiment
Principle of the present utility model and feature are described below in conjunction with example, example is served only for explaining this practicality It is new, it is not intended to limit scope of the present utility model.
As shown in Figure 1, 2, it is a kind of to be applied to the carbon carbon frock that melting siliconising method produces carbon ceramic composite material, including several The reative cell 1 of the cylindrical structure of self connection, the bottom surface of reative cell is provided with the crucible 2 for holding silica flour 3, crucible internal pendulum Some cushion blocks 4 are placed with, the top of cushion block, which is placed, needs silication workpiece base substrate 5, and the top of reative cell is sealed by upper cover plate 6, instead Room, crucible, cushion block and upper cover plate is answered to be made by carbon carbon composite.
Preferred embodiment of the present utility model is the foregoing is only, it is all in this practicality not to limit the utility model Within new spirit and principle, any modification, equivalent substitution and improvements made etc. should be included in guarantor of the present utility model Within the scope of shield.

Claims (1)

1. a kind of carbon carbon frock for being applied to melting siliconising method production carbon ceramic composite material, including several self connections The reative cell of cylindrical structure, the bottom surface of the reative cell be provided with inside the crucible for holding silica flour, the crucible be placed with it is some Cushion block, the top of the cushion block, which is placed, needs silication workpiece base substrate, and the top of the reative cell is sealed by upper cover plate, described anti- Room, crucible, cushion block and upper cover plate is answered to be made by carbon carbon composite.
CN201720260445.2U 2017-03-17 2017-03-17 It is a kind of to be applied to the carbon carbon frock that melting siliconising method produces carbon ceramic composite material Active CN206553412U (en)

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CN201720260445.2U CN206553412U (en) 2017-03-17 2017-03-17 It is a kind of to be applied to the carbon carbon frock that melting siliconising method produces carbon ceramic composite material

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109176832A (en) * 2018-08-03 2019-01-11 深圳勒迈科技有限公司 Siliconising tooling
CN110713386A (en) * 2019-11-28 2020-01-21 湖南博云新材料股份有限公司 Preparation method of C/SiC friction material
CN112341213A (en) * 2020-11-26 2021-02-09 西安鑫垚陶瓷复合材料有限公司 Method for carrying out melt siliconizing on small-size circular-section ceramic matrix composite component
CN112457027A (en) * 2020-11-26 2021-03-09 西安鑫垚陶瓷复合材料有限公司 Large-size circular-section ceramic matrix composite component melting siliconizing tool and method
CN114634367A (en) * 2022-03-31 2022-06-17 西安航空制动科技有限公司 Process device for infiltration of reaction melt

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109176832A (en) * 2018-08-03 2019-01-11 深圳勒迈科技有限公司 Siliconising tooling
CN110713386A (en) * 2019-11-28 2020-01-21 湖南博云新材料股份有限公司 Preparation method of C/SiC friction material
CN110713386B (en) * 2019-11-28 2022-04-05 湖南博云新材料股份有限公司 Preparation method of C/SiC friction material
CN112341213A (en) * 2020-11-26 2021-02-09 西安鑫垚陶瓷复合材料有限公司 Method for carrying out melt siliconizing on small-size circular-section ceramic matrix composite component
CN112457027A (en) * 2020-11-26 2021-03-09 西安鑫垚陶瓷复合材料有限公司 Large-size circular-section ceramic matrix composite component melting siliconizing tool and method
CN112341213B (en) * 2020-11-26 2022-05-13 西安鑫垚陶瓷复合材料有限公司 Method for carrying out melt siliconizing on small-size circular-section ceramic matrix composite component
CN114634367A (en) * 2022-03-31 2022-06-17 西安航空制动科技有限公司 Process device for infiltration of reaction melt
CN114634367B (en) * 2022-03-31 2024-02-09 西安航空制动科技有限公司 Process device for infiltration of reaction melt

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