CN206476930U - A kind of preparation facilities of AVM - Google Patents
A kind of preparation facilities of AVM Download PDFInfo
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- CN206476930U CN206476930U CN201720120031.XU CN201720120031U CN206476930U CN 206476930 U CN206476930 U CN 206476930U CN 201720120031 U CN201720120031 U CN 201720120031U CN 206476930 U CN206476930 U CN 206476930U
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- extraction
- magnet coil
- preparation facilities
- filter
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Abstract
The utility model is related to a kind of preparation facilities of AVM, including filter, extraction equipment and evaporated crystallization device；The second charging aperture of the extraction equipment is connected with the first discharging opening of the filter, and the second liquid outlet of the extraction equipment is connected with the 3rd charging aperture of the evaporated crystallization device；The extraction equipment includes agitating device, extraction cylinder, the first magnet coil, the first temperature controller and screen pack；The agitating device is arranged in the extraction cylinder；First magnet coil rule is wrapped in the periphery of extraction cylinder；First magnet coil is electrically connected with first temperature controller；Screen pack is arranged on the bottom of the extraction cylinder；Multiple first temperature sensors are additionally provided with the inwall of extraction cylinder；Multiple first temperature sensors are electrically connected with the first temperature controller；The first gas outlet is additionally provided with the top of extraction cylinder.The beneficial effects of the utility model are：Simple to operate, production cost is low, energy-conserving and environment-protective, it is adaptable to industrialized mass production.
Description
Technical field
The utility model is related to chemical products preparation facilities technical field, more particularly to a kind of preparation of AVM is filled
Put.
Background technology
AVM is one group produced by A Foman streptomycete fermentations by ten hexa-atomic macrolides and two olives
The class antiinsect antibiotic that sugar is constituted, it has effect unique in preventing and treating agricultural pest and animal husbandry parasitic disease, and it spreads out
Biological such as emamectin-benzoate product is safer, more efficient, the wider array of novel pesticide of insecticidal spectrum, greatly
AVM of having widened use scope, show progressively to substitute the trend of AVM in the market.But because each producer exists
Quality control in subtractive process has fluctuation, and the AVM fine powder quality produced has larger difference, so as to subsequently spreading out
Biosynthesis causes large effect.How to improve the process for refining of AVM, it is ensured that product quality, be that each producer needs solution badly
Certainly the problem of.
The average fermentation level of AVM is in 4000ug/ml or so at this stage, with regard to this rough calculation, often produce 1 ton Ah
Tie up the fermentation waste water that rhzomorph (Avm) about produces 250 tons, then produce 1000 tons of Avm fermentation waste water yield per year up to 250,000 tons.State
Inside these waste water are mostly discharged into environment without handling at this stage, and what is had is handled slightly by anaerobism/oxygen consumption or two grades of oxygen consumptions
After discharge.The influence to environment certainly will be so caused, environmental pollution is even caused, while causing the waste of water resource.
Utility model content
Technical problem to be solved in the utility model is that there is provided a kind of AVM hereinafter the problem of extraction for existing AVM
The preparation facilities of rhzomorph, simple to operate, production cost is low, energy-conserving and environment-protective, it is adaptable to industrialized mass production.
The technical scheme that the utility model solves above-mentioned technical problem is as follows：A kind of preparation facilities of AVM, including
Filter, extraction equipment and evaporated crystallization device；The second charging aperture of the extraction equipment and the first of the filter
Discharging opening is connected, and the second liquid outlet of the extraction equipment is connected with the 3rd charging aperture of the evaporated crystallization device；The extraction
Device is taken to include agitating device, extraction cylinder, the first magnet coil, the first temperature controller and screen pack；The agitating device is arranged on
In the extraction cylinder；The first magnet coil rule is wrapped in the periphery of the extraction cylinder；First magnet coil and institute
State the electrical connection of the first temperature controller；The screen pack is arranged on the bottom of the extraction cylinder；It is additionally provided with the inwall of the extraction cylinder
Multiple first temperature sensors；Described multiple first temperature sensors are electrically connected with first temperature controller；In the extraction
The top of cylinder is taken to be additionally provided with the first gas outlet.
The beneficial effects of the utility model are：Simple to operate, production cost is low, energy-conserving and environment-protective, it is adaptable to industrialize
Batch production；By setting the first magnet coil in extraction cylinder periphery, and agitating device is set, makes extractant abundant with mycelia
Mixing, improves extraction efficiency, is heated in addition in extraction process, can significantly save extraction time, simultaneously
Extractant takes away the moisture in mycelia in heating process, without setting flash dryer to remove water in addition, environmental protection
And save the consumption of substantial amounts of electric energy and steam.
On the basis of above-mentioned technical proposal, the utility model can also do following improvement.
Further：The extraction equipment also includes the first heat-insulation layer；First heat-insulation layer is arranged on first electromagnetism
The periphery of coil.
The beneficial effect of above-mentioned further scheme is：Effect with insulation, prevents heat to scatter and disappear, and saves electric energy.
Further：The agitating device includes the mixing arm of stirring motor, agitating shaft and multiple different lengths；The stirring
Motor is arranged on the middle part on the extraction cylinder top；The output shaft of one end of the agitating shaft and the stirring motor, which is fixed, to be connected
Connect, the other end of the agitating shaft is stretched into the extraction cylinder；Described multiple mixing arms are disposed on the agitating shaft.
The beneficial effect of above-mentioned further scheme is：Using agitating device, accelerate the mixing of extractant and mycelia, improve extraction
Efficiency is taken, the time is saved.
Further：The stirring motor is variable-frequency motor.
The beneficial effect of above-mentioned further scheme is：The rotational frequency of stirring motor can be changed, so that material more fills
The mixing divided.
Further：The filter includes hydraulic pump, piston, first charging aperture, cartridge filter and milipore filter；The hydraulic pressure
Pump is arranged on the top of the cartridge filter；The piston is arranged in the cartridge filter and slided with the inwall of the cartridge filter
Coordinate；The piston is fixedly connected with the hydraulic pump；The milipore filter is inclined at the bottom of the cartridge filter；Described
One charging aperture is arranged on the side of the cartridge filter；First discharging opening is arranged on the filtering at the milipore filter downstream
On cylinder；The first liquid outlet is additionally provided with the bottom of the cartridge filter.
The beneficial effect of above-mentioned further scheme is：Air in cartridge filter is compressed by hydraulic pump, increases pressure, effectively
Mycelia and zymotic fluid are separated, filter efficiency is improved.
Further：Also include waste collecting device；The waste collecting device is connected with first liquid outlet.
The beneficial effect of above-mentioned further scheme is：Unified collection processing is carried out to the fermented waste fluid after filtering, phase is carried out
Discharged again after closing purified treatment, prevent from polluting environment, improve the utilization rate of water resource.
Further：Also include the first condensing unit and the first condensate collection device；First condensate collection device passes through
Tracheae is connected with first gas outlet；First condensing unit is positioned close to the tracheae of first condensate collection device
On；First condensing unit includes condenser pipe, cooling water inlet and coolant outlet；The condenser pipe is arranged on the tracheae
Periphery；The cooling water inlet is arranged on the bottom of the condenser pipe；The coolant outlet is arranged on the condenser pipe
Top.
The beneficial effect of above-mentioned further scheme is：The steam discharged by the first condensing unit to extraction cylinder is condensed
Processing, the first condensate collection device is collected to condensate liquid, facilitates recycling, saves production cost.
Further：The evaporated crystallization device includes the second temperature controller, the second magnet coil, evaporative crystallization cylinder, Duo Ge
Two temperature sensors and the second gas outlet；The second magnet coil rule is wrapped in the periphery of the evaporative crystallization cylinder；It is described
Multiple second temperature sensors be arranged on the inwall of evaporative crystallization cylinder；Second gas outlet is arranged on the evaporation knot
The top of brilliant cylinder；Second magnet coil, described multiple second temperature sensors are electrically connected with second temperature controller respectively
Connect.
The beneficial effect of above-mentioned further scheme is：Evaporative crystallization cylinder is heated by the second magnet coil, heat
It is evenly distributed, while measure the temperature in evaporative crystallization cylinder in real time using second temperature sensor, can root by the second temperature controller
According to needing to adjust the temperature in evaporative crystallization cylinder, accelerate the speed of evaporative crystallization.
Further：The evaporated crystallization device also includes the second heat-insulation layer；Second heat-insulation layer is arranged on described second
The periphery of magnet coil.
The beneficial effect of above-mentioned further scheme is：Effect with insulation, prevents heat to scatter and disappear, and saves electric energy.
Further：Also include the second condensing unit and the second condensate collection device；Second condensate collection device passes through
Tracheae is connected with second gas outlet；Second condensing unit is positioned close to the tracheae of second condensate collection device
On.
The beneficial effect of above-mentioned further scheme is：Second condensing unit is used to enter the steam of discharge in evaporative crystallization cylinder
Row condensation process, the second condensate collection device is used to carry out recycling to condensate liquid, reduces production cost.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Embodiment
Principle of the present utility model and feature are described below in conjunction with accompanying drawing, example is served only for explaining this practicality
It is new, it is not intended to limit scope of the present utility model.
As shown in figure 1, a kind of preparation facilities of AVM, it includes filter 1, extraction equipment 2 and evaporative crystallization
Device 8；The second charging aperture 21 of the extraction equipment 2 is connected with the first discharging opening 17 of the filter 1, the extraction dress
The second liquid outlet 29 for putting 2 is connected with the 3rd charging aperture 81 of the evaporated crystallization device 8.
The filter 1 includes hydraulic pump 11, piston 12, first charging aperture 13, cartridge filter 14 and milipore filter 15；It is described
Hydraulic pump 11 is arranged on the top of the cartridge filter 14；The piston 12 be arranged in the cartridge filter 14 and with the filtering
The inwall of cylinder 14 is slidably matched；The piston 12 is fixedly connected with the hydraulic pump 11；The milipore filter 15 is inclined at institute
State the bottom of cartridge filter 14；The first charging aperture 13 is arranged on the side of the cartridge filter 14；First discharging opening 17 is set
Put on the cartridge filter 14 at the downstream of milipore filter 15；The first liquid outlet is additionally provided with the bottom of the cartridge filter 14
16。
Also include waste collecting device 9；The waste collecting device 9 is connected with first liquid outlet 16.
Specifically, abamectin fermented liquid is added in cartridge filter 14 by first charging aperture 13, pushed away by hydraulic pump 11
Air in piston 12, compression cartridge filter 14, waste collecting device 9 is discharged to by fermented waste fluid by the first liquid outlet 16
In, recycled, after the completion of filtering, wet mycelium will be obtained and be added to by the first discharging opening 17 in extraction equipment 2, entered
Row extraction process.
The extraction equipment 2 includes agitating device 3, extraction cylinder 27, the first magnet coil 24, the first temperature controller 25 and filtering
Net 28；The agitating device 3 is arranged in the extraction cylinder 27；The rule of first magnet coil 24 is wrapped in the extraction cylinder
27 periphery；First magnet coil 24 is electrically connected with first temperature controller 25；The screen pack 28 is arranged on the extraction
Take the bottom of cylinder 27；Multiple first temperature sensors 23, in the present embodiment, first are additionally provided with the inwall of the extraction cylinder 27
The quantity of temperature sensor 23 is four, is separately positioned on the diverse location of the inwall of extraction cylinder 27, to measure extraction cylinder 27
The temperature of interior diverse location；Described multiple first temperature sensors 23 are electrically connected with first temperature controller 25.Described
It is toluene to extract the extractant added in cylinder 27.
The first gas outlet 22 is additionally provided with the top of the extraction cylinder 27；Second charging aperture 21 is arranged on the extraction cylinder 27
Top；Second liquid outlet 29 is arranged on the bottom of the extraction cylinder 27, and is obliquely installed, convenient discharge filtered fluid.Described
The position that the side of extraction cylinder 27 is on the lower side is additionally provided with the second discharging opening, and the second discharging opening is obliquely installed.
The extraction equipment 2 also includes the first heat-insulation layer 26；First heat-insulation layer 26 is arranged on first electromagnetic wire
The periphery of circle 24, the effect with insulation reduces scattering and disappearing for heat, saves the energy.The extraction equipment 2 is additionally provided with vacuum
Pump, for suctioning out the air in extraction cylinder 27, it is vacuum environment to make in extraction cylinder 27.
The agitating device 3 includes the mixing arm 33 of stirring motor 31, agitating shaft 32 and multiple different lengths；The stirring
Motor 31 is arranged on the middle part on extraction cylinder 27 top；One end of the agitating shaft 32 and the output shaft of the stirring motor 31
It is fixedly connected, the other end of the agitating shaft 32 is stretched into the extraction cylinder 27；Described multiple mixing arms 33 are disposed on
On the agitating shaft 32, and the length of described multiple mixing arms 33 is differed, convenient that material stirring is uniform, is sufficiently mixed.
The stirring motor 31 is variable-frequency motor, and the frequency of stirring motor 31 can be adjusted as needed, improves stirring mixing efficiency.
Also include the first condensing unit 4 and the first condensate collection device 5；First condensate collection device 5 passes through tracheae
It is connected with first gas outlet 22；First condensing unit 4 is positioned close to the tracheae of first condensate collection device 5
On；First condensing unit 4 includes condenser pipe 42, cooling water inlet 43 and coolant outlet 41；The condenser pipe 42 is set
In the periphery of the tracheae；The cooling water inlet 43 is arranged on the bottom of the condenser pipe 42；The coolant outlet 41 is set
Put on the top of the condenser pipe 42.
Specifically, the wet mycelium being filtrated to get is entered in extraction cylinder 27 by second charging aperture 21, and pass through second
Charging aperture 21 adds extractant toluene, suctions out the air extracted in cylinder 27 by vavuum pump, constructs vacuum environment；Start stirring
Motor 31, makes toluene be sufficiently mixed with wet mycelium；Heated up, passed through simultaneously by 24 pairs of extraction cylinders 27 of the first magnet coil
Temperature in first temperature controller 25 and the first temperature sensor 23 control extraction cylinder 27, by temperature control in toluene in vacuum condition
94 DEG C of the temperature of lower boiling, is kept for 30 minutes.
During extraction is heated, the steam in extraction cylinder 27 is discharged in tracheae by the first gas outlet 22, is passed through
The condensation of first condensing unit 4 enters in the first condensate collection device 5, and condensate liquid now is toluene and the mixture of water, toluene
It is water insoluble, it is layered in the first condensate collection device 5, the toluene recovery on upper strata is recycled.
The toluene extracted in cylinder 27 and mycelial mixed solution are cooled to normal temperature, the second liquid outlet 29 is opened, to mixed
Close solution to be filtered, filtrate enters in evaporated crystallization device 8, after the completion of filtering, close the second liquid outlet 29, to extraction cylinder 27
Interior addition toluene, the process for repeating above-mentioned extraction filtering, until that is collected in the first condensate collection device 5 is all toluene.
The evaporated crystallization device 8 includes the second temperature controller 82, the second magnet coil 83, evaporative crystallization cylinder 84, Duo Ge
Two temperature sensors 87 and the second gas outlet 88；The rule of second magnet coil 83 is wrapped in the outer of the evaporative crystallization cylinder 84
Week；Described multiple second temperature sensors 87 are arranged on the inwall of the evaporative crystallization cylinder 84, in the present embodiment, the second temperature
The quantity for spending sensor 87 is four, is separately positioned on the diverse location of the inwall of evaporative crystallization cylinder 84, to measure evaporation knot
The temperature of diverse location in brilliant cylinder 84；Second gas outlet 88 is arranged on the top of the evaporative crystallization cylinder 84；Described second
Magnet coil 83, described multiple second temperature sensors 87 are electrically connected with second temperature controller 82 respectively.3rd charging aperture
81 are arranged on the top of the evaporative crystallization cylinder 84；The 3rd discharging opening 85 is additionally provided with the bottom of evaporative crystallization cylinder 84.
The evaporated crystallization device 8 also includes the second heat-insulation layer 86；Second heat-insulation layer 86 is arranged on second electricity
The periphery of magnetic coil 83, the effect with insulation reduces scattering and disappearing for heat, saves the energy.
Also include the second condensing unit 6 and the second condensate collection device 7；Second condensate collection device 7 passes through tracheae
It is connected with second gas outlet 88；Second condensing unit 6 is positioned close to the tracheae of second condensate collection device 7
On.The structure of second condensing unit 6 is identical with the structure of first condensing unit 4, will not be repeated here.
Also include mixing arrangement；The 4th charging aperture is provided with the top of mixing arrangement, in the bottom of mixing arrangement provided with the
Four discharging openings, be additionally provided with mixing arrangement with the second agitating device of structure identical of agitating device 3, for stir mixing；For
The service life of extension mixing arrangement, on the inwall of mixing arrangement is coated with polyethylene anticorrosive coating.
Collected specifically, the toluene being filtrated to get by extracting extracts filtrate in evaporative crystallization cylinder 84, pass through the second electricity
Magnetic coil 83 heats to evaporative crystallization cylinder 84, filtrate is concentrated to give in paste semi-finished product, heating process and produces
Toluene vapor by the second condensing unit 6 and the second condensate collection device 7 condensation reclaim, in case using next time；Pass through second
Temperature controller 82 changes the temperature in evaporative crystallization cylinder 84, is evaporated crystallization；The crystalline solid that evaporative crystallization is separated out goes out by the 3rd
Material mouth 85 enters in mixing arrangement, and mixing is stirred together with other auxiliary materials in mixing arrangement, AVM finished product is prepared.
Preferred embodiment of the present utility model is the foregoing is only, it is all in this practicality not to limit the utility model
Within new spirit and principle, any modification, equivalent substitution and improvements made etc. should be included in guarantor of the present utility model
Within the scope of shield.
Claims (10)
1. a kind of preparation facilities of AVM, it is characterised in that：Including filter (1), extraction equipment (2) and evaporative crystallization
Device (8)；The second charging aperture (21) of the extraction equipment (2) is connected with the first discharging opening (17) of the filter (1),
The second liquid outlet (29) of the extraction equipment (2) is connected with the 3rd charging aperture (81) of the evaporated crystallization device (8)；It is described
Extraction equipment (2) includes agitating device (3), extraction cylinder (27), the first magnet coil (24), the first temperature controller (25) and screen pack
(28)；The agitating device (3) is arranged in the extraction cylinder (27)；First magnet coil (24) rule is wrapped in described
Extract the periphery of cylinder (27)；First magnet coil (24) electrically connects with first temperature controller (25)；The screen pack
(28) it is arranged on the bottom of the extraction cylinder (27)；Multiple first temperature sensors are additionally provided with the inwall of the extraction cylinder (27)
(23)；Described multiple first temperature sensors (23) electrically connect with first temperature controller (25)；In the extraction cylinder
(27) top is additionally provided with the first gas outlet (22).
2. a kind of preparation facilities of AVM according to claim 1, it is characterised in that：The extraction equipment (2) is also wrapped
Include the first heat-insulation layer (26)；First heat-insulation layer (26) is arranged on the periphery of first magnet coil (24).
3. a kind of preparation facilities of AVM according to claim 1, it is characterised in that：The agitating device (3) includes
The mixing arm (33) of stirring motor (31), agitating shaft (32) and multiple different lengths；The stirring motor (31) is arranged on described
Extract the middle part on cylinder (27) top；One end of the agitating shaft (32) is fixedly connected with the output shaft of the stirring motor (31),
The other end of the agitating shaft (32) is stretched into the extraction cylinder (27)；Described multiple mixing arms (33) are disposed on described
On agitating shaft (32).
4. a kind of preparation facilities of AVM according to claim 3, it is characterised in that：The stirring motor (31) is change
Frequency motor.
5. a kind of preparation facilities of AVM according to claim 1, it is characterised in that：The filter (1) includes
Hydraulic pump (11), piston (12), first charging aperture (13), cartridge filter (14) and milipore filter (15)；The hydraulic pump (11) is set
Top in the cartridge filter (14)；The piston (12) be arranged in the cartridge filter (14) and with the cartridge filter (14)
Inwall be slidably matched；The piston (12) is fixedly connected with the hydraulic pump (11)；The milipore filter (15) is inclined at
The bottom of the cartridge filter (14)；The first charging aperture (13) is arranged on the side of the cartridge filter (14)；Described first goes out
Material mouth (17) is arranged on the cartridge filter (14) at the milipore filter (15) downstream；In the bottom of the cartridge filter (14) also
Provided with the first liquid outlet (16).
6. a kind of preparation facilities of AVM according to claim 5, it is characterised in that：Also include waste collecting device
(9)；The waste collecting device (9) is connected with first liquid outlet (16).
7. a kind of preparation facilities of AVM according to claim 1, it is characterised in that：Also include the first condensing unit
And the first condensate collection device (5) (4)；First condensate collection device (5) passes through tracheae and first gas outlet (22)
Connection；First condensing unit (4) is positioned close on the tracheae of first condensate collection device (5)；Described first is cold
Solidifying device (4) includes condenser pipe (42), cooling water inlet (43) and coolant outlet (41)；The condenser pipe (42) is arranged on institute
State the periphery of tracheae；The cooling water inlet (43) is arranged on the bottom of the condenser pipe (42)；The coolant outlet (41)
It is arranged on the top of the condenser pipe (42).
8. a kind of preparation facilities of AVM according to claim 1, it is characterised in that：The evaporated crystallization device (8)
Including the second temperature controller (82), the second magnet coil (83), evaporative crystallization cylinder (84), multiple second temperature sensors (87) and the
Two gas outlets (88)；Second magnet coil (83) rule is wrapped in the periphery of the evaporative crystallization cylinder (84)；Described is more
Individual second temperature sensor (87) is arranged on the inwall of the evaporative crystallization cylinder (84)；Second gas outlet (88) is arranged on institute
State the top of evaporative crystallization cylinder (84)；Second magnet coil (83), described multiple second temperature sensors (87) are respectively
Electrically connected with second temperature controller (82).
9. a kind of preparation facilities of AVM according to claim 8, it is characterised in that：The evaporated crystallization device (8)
Also include the second heat-insulation layer (86)；Second heat-insulation layer (86) is arranged on the periphery of second magnet coil (83).
10. a kind of preparation facilities of AVM according to claim 8, it is characterised in that：Also include the second condensing unit
And the second condensate collection device (7) (6)；Second condensate collection device (7) passes through tracheae and second gas outlet (88)
Connection；Second condensing unit (6) is positioned close on the tracheae of second condensate collection device (7).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720120031.XU CN206476930U (en) | 2017-02-09 | 2017-02-09 | A kind of preparation facilities of AVM |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720120031.XU CN206476930U (en) | 2017-02-09 | 2017-02-09 | A kind of preparation facilities of AVM |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206476930U true CN206476930U (en) | 2017-09-08 |
Family
ID=59749410
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720120031.XU Expired - Fee Related CN206476930U (en) | 2017-02-09 | 2017-02-09 | A kind of preparation facilities of AVM |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206476930U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107970644A (en) * | 2017-11-15 | 2018-05-01 | 安徽工程大学 | A kind of extraction separation device for bio-pharmaceuticals |
-
2017
- 2017-02-09 CN CN201720120031.XU patent/CN206476930U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107970644A (en) * | 2017-11-15 | 2018-05-01 | 安徽工程大学 | A kind of extraction separation device for bio-pharmaceuticals |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170908 Termination date: 20180209 |