CN206476921U - A kind of system for improving methanol output and quality - Google Patents

A kind of system for improving methanol output and quality Download PDF

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Publication number
CN206476921U
CN206476921U CN201720072303.3U CN201720072303U CN206476921U CN 206476921 U CN206476921 U CN 206476921U CN 201720072303 U CN201720072303 U CN 201720072303U CN 206476921 U CN206476921 U CN 206476921U
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CN
China
Prior art keywords
tank
rectifying tower
quality
fusel oil
pipeline
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720072303.3U
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Chinese (zh)
Inventor
孙秀英
王伟
渠兵
陈永献
常亮
李冰
张鸾
董华
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YANKUANG GUOHONG CHEMICAL INDUSTRY Co Ltd
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YANKUANG GUOHONG CHEMICAL INDUSTRY Co Ltd
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Priority to CN201720072303.3U priority Critical patent/CN206476921U/en
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Publication of CN206476921U publication Critical patent/CN206476921U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

The utility model belongs to technological operation, improves the operating technology field of yield and product quality, more particularly to a kind of system for improving methanol output and quality;Including the pre-rectifying tower being sequentially connected by pipeline, pre-rectifying tower condenser A, pre-rectifying tower condenser B, extraction tank, fusel oil sump tank and recovery tower, this programme is by setting fusel oil sump tank, the pre- cut of pre-rectifying tower of methanol product quality will be influenceed, recovery tower fusel oil etc., which is collected separately, delivers to fusel oil sump tank, other anti-surge coolers condense methanol and servicing motor-pump discharge methanol is still collected and carries out rectifying again in underground tank, methanol output reduction consumption is improved to greatest extent in the case where meeting product quality so as to reach, it can ensure that product quality adds yield again.

Description

A kind of system for improving methanol output and quality
Technical field
The utility model belongs to technological operation, improves the operating technology field of yield and product quality, more particularly to a kind of The system for improving methanol output and quality.
Background technology
In the production of contemporary methanol fractionation system, product quality and yield are a pair of passes that are conflicting and being closely connected System, to ensure that product quality is often forced to sacrifice yield in actual production, so as to cause consumption and cost increase.
In conventional methanol distillation system, compressor process anti-surge cooler is condensed into methanol, daily each servicing motor-pump and arranged Put methanol and the pre- cut of pre-rectifying tower, recovery tower fusel oil etc. and collect the blending ingredients collected in underground tank, underground tank again Crude carbinol groove or fusel oil groove are delivered to by submerged pump, the part methanol has an impact the pre- cut and fusel of product quality because containing, If deliver to crude carbinol groove carries out rectifying again, for a long time rectifying product quality can be caused unqualified;Made if fusel oil groove is delivered to Increase is reduced and consumed into methanol output.
The content of the invention
In order to solve the above-mentioned technical problem, this application provides a kind of system for improving methanol output and quality, the application Realized by following proposal:
A kind of system for improving methanol output and quality, including pre-rectifying tower, the pre-rectifying tower being sequentially connected by pipeline Condenser A, pre-rectifying tower condenser B, extraction tank, fusel oil sump tank and recovery tower.
It is preferred that, pre-rectifying tower condenser A is connected by pipeline with pre-rectifying tower backflash, and the extraction tank passes through pipe Road is connected with pre-rectifying tower backflash, and the pre-rectifying tower backflash is connected by pipeline with the tower top of pre-rectifying tower.
It is preferred that, the pipeline between pre-rectifying tower backflash and pre-rectifying tower is provided with pre-rectifying tower reflux pump.
It is preferred that, pre-rectifying tower backflash is connected by pipeline with fusel oil sump tank, the fusel oil sump tank with Recovery tower intercommunication.
It is preferred that, improving the system of methanol output and quality also includes underground tank, and the underground tank is used to collect anti-surge Cooler condenses the methanol of methanol and servicing motor-pump discharge.
It is preferred that, underground tank is provided with underground tank pump, and the underground tank is collected by pipeline and crude carbinol groove or fusel oil Groove is connected.
It is preferred that, fusel oil sump tank and letdown tank intercommunication, the letdown tank are connected to set on the pipeline of fusel oil sump tank There is letdown tank pump.
It is preferred that, extraction tank is provided with desalination water inlet.
It is preferred that, the bottom of towe of recovery tower is connected by pipeline with gasification coal-grinding apparatus.
It is preferred that, pre-rectifying tower backflash is provided with overflow line, and the overflow line is connected with fusel oil sump tank; The extraction tank is provided with overflow line, and the overflow line is connected with fusel oil sump tank.
The light components such as the dimethyl ether in the methanol four tower rectifying technique that the application is used, i.e. pre-rectifying tower removing crude carbinol, In pressurizing tower, atmospheric tower extraction refined methanol, in recovery tower extraction part fusel, other heavy constituents such as waste water are sent to from recovery tower bottom Gasify coal-grinding.
The extraction tank of the application is arranged on two layers of rectifying framework, and it is cold that pre-rectifying tower tower top methanol steam first passes through pre-rectifying tower Condenser A, methanol steam is after pre-rectifying tower condenser A, and the temperature control of fixed gas out is in 65 DEG C or so, most of first Alcohol is condensed to pre-rectifying tower backflash, and the uncooled methanol of pre-rectifying tower condenser A and fixed gas are condensed by pre-rectifying tower Device B is condensed to extraction tank again, and the methanol of extraction removes pre-rectifying tower backflash, but pre-rectifying tower backflash is it is possible to have micro Influence product quality pre- cut, by control pre-rectifying tower backflash liquid level by influence product quality pre- cut swim in liquid Face upper strata is produced by overflow line.
The extraction tank of this reality application is arranged on three layers of rectifying framework, by controlling pre-rectifying tower tower top methanol steam temperature to exist 40 DEG C or so so as to by most light components(Dimethyl ether, acetaldehyde, acetone etc.)Removing is clean, and the light component of only a few passes through again Extraction tank addition extraction water is extracted, and the pre- cut of influence product quality swims in liquid level upper strata and produced by overflow line.
Purification is gone to be vented by the fixed gas after pre-rectifying tower condenser B.
Letdown tank is used for the cut of miscellaneous equipment in collection system, is not present invention point, excessive elaboration is not done.
This programme will influence the pre- cut of pre-rectifying tower, the recovery tower of methanol product quality by setting fusel oil sump tank Fusel oil etc., which is collected separately, delivers to fusel oil sump tank, and other anti-surge coolers condensation methanol and servicing motor-pump discharge methanol are still So collect and carry out rectifying again in underground tank, methanol production is improved to greatest extent in the case where meeting product quality so as to reach Amount reduction consumption, can ensure that product quality adds yield again.
Brief description of the drawings
Fig. 1 is the structural representation of embodiment 1;
Wherein, T2101, pre-rectifying tower, T2104, recovery tower, V2101, pre-rectifying tower backflash, V2107, underground tank, V2108, fusel oil sump tank, V2109, extraction tank, E2106, pre-rectifying tower condenser A, E2116, pre-rectifying tower condenser B, P2103, pre-rectifying tower reflux pump, P2109, underground tank pump, P2110, letdown tank pump, 1:Desalination water inlet.
In structural representation, dotted portion is former design, and it produces the fusel oil for influenceing product quality to underground tank;It is real Line part is this programme, will proceed processing by influenceing the fusel oil of product quality to be collected into fusel oil sump tank.
Embodiment
Embodiment 1
It is a kind of to improve the system of methanol output and quality, including be sequentially connected by pipeline pre-rectifying tower T2101, pre- essence Evaporate tower condenser A E2106, pre-rectifying tower condenser B E2116, extraction tank V2109, fusel oil sump tank V2108 and recovery tower T2104;
Pre-rectifying tower condenser A E2106 are connected by pipeline with pre-rectifying tower backflash V2101, the extraction tank V2109 is connected by pipeline with pre-rectifying tower backflash V2101, and the pre-rectifying tower backflash V2101 is by pipeline and in advance Rectifying column T2101 tower top is connected;
Pipeline between pre-rectifying tower backflash V2101 and pre-rectifying tower T2101 is provided with pre-rectifying tower reflux pump P2103;
Pre-rectifying tower backflash V2101 is connected by pipeline with fusel oil sump tank V2108, the fusel oil sump tank V2108 and recovery tower T2104 intercommunications;
Improving the system of methanol output and quality also includes underground tank V2107, the underground tank V2107 for collecting anti-asthma The cooler that shakes condenses the methanol of methanol and servicing motor-pump discharge;
Underground tank V2107 passes through pipeline and crude carbinol groove or miscellaneous provided with underground tank pump P2109, the underground tank V2107 Alcohol oil sump tank V2108 is connected;
Fusel oil sump tank V2108 and letdown tank intercommunication, the letdown tank are connected on fusel oil sump tank V2108 pipeline Provided with letdown tank pump P2110;
Extraction tank V2109 is provided with desalination water inlet 1;
Recovery tower T2104 bottom of towe is connected by pipeline with gasification coal-grinding apparatus;
Pre-rectifying tower backflash V2101 is provided with overflow line, and the overflow line is connected with fusel oil sump tank V2108 Connect;
Extraction tank V2109 is provided with overflow line, and the overflow line is connected with fusel oil sump tank V2108.

Claims (10)

1. a kind of system for improving methanol output and quality, it is characterised in that including be sequentially connected by pipeline pre-rectifying tower, Pre-rectifying tower condenser A, pre-rectifying tower condenser B, extraction tank, fusel oil sump tank and recovery tower.
2. a kind of system for improving methanol output and quality as claimed in claim 1, it is characterised in that the pre-rectifying tower is cold Condenser A is connected by pipeline with pre-rectifying tower backflash, and the extraction tank is connected by pipeline with pre-rectifying tower backflash, The pre-rectifying tower backflash is connected by pipeline with the tower top of pre-rectifying tower.
3. a kind of system for improving methanol output and quality as claimed in claim 1, it is characterised in that the pre-rectifying tower is returned Pipeline between chute and pre-rectifying tower is provided with pre-rectifying tower reflux pump.
4. a kind of system for improving methanol output and quality as claimed in claim 1, it is characterised in that the pre-rectifying tower is returned Chute is connected by pipeline with fusel oil sump tank, the fusel oil sump tank and recovery tower intercommunication.
5. a kind of system for improving methanol output and quality as claimed in claim 1, it is characterised in that the raising methanol production The system of amount and quality also includes underground tank, and the underground tank is used to collect anti-surge cooler condensation methanol and servicing motor-pump row The methanol put.
6. a kind of system for improving methanol output and quality as claimed in claim 5, it is characterised in that set on the underground tank There is underground tank pump, the underground tank is connected by pipeline with crude carbinol groove or fusel oil sump tank.
7. a kind of system for improving methanol output and quality as claimed in claim 1, it is characterised in that the fusel oil is collected Groove and letdown tank intercommunication, the pipeline that the letdown tank is connected to fusel oil collection tank are provided with letdown tank pump.
8. a kind of system for improving methanol output and quality as claimed in claim 1, it is characterised in that set on the extraction tank There is desalination water inlet.
9. a kind of system for improving methanol output and quality as claimed in claim 1, it is characterised in that the tower of the recovery tower Bottom is connected by pipeline with gasification coal-grinding apparatus.
10. a kind of system for improving methanol output and quality as claimed in claim 1, it is characterised in that the pre-rectifying tower Backflash is provided with overflow line, and the overflow line is connected with fusel oil sump tank;The extraction tank is provided with overflow pipe Line, the overflow line is connected with fusel oil sump tank.
CN201720072303.3U 2017-01-20 2017-01-20 A kind of system for improving methanol output and quality Expired - Fee Related CN206476921U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720072303.3U CN206476921U (en) 2017-01-20 2017-01-20 A kind of system for improving methanol output and quality

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720072303.3U CN206476921U (en) 2017-01-20 2017-01-20 A kind of system for improving methanol output and quality

Publications (1)

Publication Number Publication Date
CN206476921U true CN206476921U (en) 2017-09-08

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111450571A (en) * 2020-03-17 2020-07-28 安徽晋煤中能化工股份有限公司 System for realizing continuous extraction of methanol oil by double-effect utilization of extraction water
CN112516622A (en) * 2020-12-11 2021-03-19 安徽金禾实业股份有限公司 Extraction and impurity removal device and method for recovering methanol through chlorination in maltol production

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111450571A (en) * 2020-03-17 2020-07-28 安徽晋煤中能化工股份有限公司 System for realizing continuous extraction of methanol oil by double-effect utilization of extraction water
CN112516622A (en) * 2020-12-11 2021-03-19 安徽金禾实业股份有限公司 Extraction and impurity removal device and method for recovering methanol through chlorination in maltol production

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CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20170908

Termination date: 20190120