CN206474142U - A kind of tetrahydrofuran derivatives medicine intermediate reactor - Google Patents
A kind of tetrahydrofuran derivatives medicine intermediate reactor Download PDFInfo
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- CN206474142U CN206474142U CN201621407183.XU CN201621407183U CN206474142U CN 206474142 U CN206474142 U CN 206474142U CN 201621407183 U CN201621407183 U CN 201621407183U CN 206474142 U CN206474142 U CN 206474142U
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- inner cylinder
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- low head
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Abstract
The utility model discloses a kind of tetrahydrofuran derivatives medicine intermediate reactor, including kettle, and the kettle is made up of inner cylinder and chuck, the lower end connection inner cylinder low head of the inner cylinder, the upper end connection inner cylinder upper cover of inner cylinder, the outside of inner cylinder, which is fixed on jacket cylinder, the side wall of inner cylinder, sets ring flange；The lower end connection chuck low head of jacket cylinder；Agitating device is set on inner cylinder axis；The top of inner cylinder sets manhole and charging aperture, and the downside of inner cylinder sets discharging opening, and the outside of jacket cylinder sets ear mount；The bottom of chuck low head sets ethanol entrance port, and the upside of jacket cylinder sets nol outlet.The utility model has the advantages that：Using jacketed vessel, equipment heat-transfer effect is improved, production capacity is improved.
Description
Technical field
The utility model is related to field of chemical equipment, specifically a kind of tetrahydrofuran derivatives medicine intermediate reactor.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, and it is different using each component boiling point in mixing liquid or liquid-solid system,
Low boiling component is evaporated, then is condensed to separate the unit process of whole component, organic distillation still is that one kind can be more preferable
The mixing plant for realizing organic distillation.
Existing distillation still mixing effect is uneven, and heat transfer effect is bad.
Utility model content
Stirred in order to solve the above technical problems, the purpose of this utility model is to provide one kind, in good effect of heat exchange
Mesosome reactor, concrete technical scheme is as follows.
A kind of tetrahydrofuran derivatives medicine intermediate reactor, including kettle, the kettle is made up of inner cylinder and chuck, described
The lower end connection inner cylinder low head of inner cylinder, the upper end connection inner cylinder upper cover of inner cylinder, jacket cylinder, inner cylinder are fixed in the outside of inner cylinder
Side wall on ring flange is set；The lower end connection chuck low head of jacket cylinder；Agitating device is set on inner cylinder axis；Inner cylinder
Top sets manhole and charging aperture, and the downside of inner cylinder sets discharging opening, and the outside of jacket cylinder sets ear mount；Chuck low head
Bottom sets ethanol entrance port, and the upside of jacket cylinder sets nol outlet；Agitating device includes blade, and blade is provided with two layers, point
Not Wei upper strata blade and lower floor's blade, upper strata blade include inner ring, outer shroud and blade body, blade body be fixed on inner ring and outer rings it
Between and blade body be obliquely installed；Lower floor's blade is the multiple blade bodies being obliquely installed；In the discharge end of charging aperture is deep into
Cylinder low head.
The reactor total volume is 1m3, and jacket for heat exchange area is 4.51m2, and vessel media is：Tetrahydrofuran, container work
Make pressure -0.09/0.4Mpa, chuck medium is ethanol, and operating pressure is 0.4Mpa, and integral device is manufactured using TA2.
The utility model has the advantages that：Using jacketed vessel, equipment heat-transfer effect is improved, production capacity is improved.
Brief description of the drawings
Fig. 1 is assembly schematic diagram of the present utility model；
Fig. 2 is the schematic diagram of upper strata blade.
Embodiment
The utility model is illustrated below in conjunction with the accompanying drawings, as shown in figure 1, the utility model includes kettle, the kettle
It is made up of inner cylinder 3 and chuck, the lower end connection inner cylinder low head 1 of the inner cylinder 3, the upper end connection inner cylinder upper cover 6 of inner cylinder 3,
The outside of inner cylinder 3, which is fixed, sets ring flange 5 on jacket cylinder 4, the side wall of inner cylinder 3；Sealed under the lower end connection chuck of jacket cylinder 4
First 2；Agitating device 8 is set on the axis of inner cylinder 3；The top of inner cylinder 3 sets manhole 7 and charging aperture 11, and the downside of inner cylinder 3 is set
Discharging opening 12, the outside of jacket cylinder 4 sets ear mount 9；The bottom of chuck low head 2 sets ethanol entrance port 13, jacket cylinder
Upside sets nol outlet 14.
The agitating device 8 includes blade, and blade is provided with two layers, and upper strata blade 10-1 is oblique leaf disc turbine type blade,
Lower floor blade 10-2 is pusher blade.
As shown in Fig. 2 the oblique leaf disc turbine type blade includes inner ring 10-1-1, outer shroud 10-1-2 and blade body 10-
1-2, blade body is fixed between inner ring and outer rings and blade body is obliquely installed.The pusher blade is be obliquely installed multiple
Blade body.
The reactor total volume is 1m3, jacket for heat exchange area is 4.51m2, vessel media is：Tetrahydrofuran, container work
Make pressure -0.09/0.4Mpa, chuck medium is ethanol, and operating pressure is 0.4Mpa, and integral device is manufactured using TA2.
Claims (1)
1. a kind of tetrahydrofuran derivatives medicine intermediate reactor, it is characterised in that：Including kettle, the kettle is by inner cylinder and chuck
Composition, the lower end connection inner cylinder low head of the inner cylinder, the upper end connection inner cylinder upper cover of inner cylinder, chuck is fixed in the outside of inner cylinder
Ring flange is set on cylinder, the side wall of inner cylinder；The lower end connection chuck low head of jacket cylinder；Stirring dress is set on inner cylinder axis
Put；The top of inner cylinder sets manhole and charging aperture, and the downside of inner cylinder sets discharging opening, and the outside of jacket cylinder sets ear mount；Folder
The bottom for covering low head sets ethanol entrance port, and the upside of jacket cylinder sets nol outlet；Agitating device includes blade, and blade is set
There is two layers, respectively upper strata blade and lower floor's blade, upper strata blade includes inner ring, outer shroud and blade body, in blade body is fixed on
Between ring and outer shroud and blade body is obliquely installed；Lower floor's blade is the multiple blade bodies being obliquely installed；The discharging of charging aperture
End is deep into inner cylinder low head.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621407183.XU CN206474142U (en) | 2016-12-21 | 2016-12-21 | A kind of tetrahydrofuran derivatives medicine intermediate reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621407183.XU CN206474142U (en) | 2016-12-21 | 2016-12-21 | A kind of tetrahydrofuran derivatives medicine intermediate reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206474142U true CN206474142U (en) | 2017-09-08 |
Family
ID=59750170
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621407183.XU Active CN206474142U (en) | 2016-12-21 | 2016-12-21 | A kind of tetrahydrofuran derivatives medicine intermediate reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206474142U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114377613A (en) * | 2022-02-21 | 2022-04-22 | 一重集团大连工程建设有限公司 | High-efficient polymeric kettle with thin wall inner tube |
-
2016
- 2016-12-21 CN CN201621407183.XU patent/CN206474142U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114377613A (en) * | 2022-02-21 | 2022-04-22 | 一重集团大连工程建设有限公司 | High-efficient polymeric kettle with thin wall inner tube |
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