CN208711104U - A kind of new type of continuous extraction equipment - Google Patents
A kind of new type of continuous extraction equipment Download PDFInfo
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- CN208711104U CN208711104U CN201821231432.3U CN201821231432U CN208711104U CN 208711104 U CN208711104 U CN 208711104U CN 201821231432 U CN201821231432 U CN 201821231432U CN 208711104 U CN208711104 U CN 208711104U
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- kettle
- valve
- extraction
- extraction kettle
- vacuum distillation
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Abstract
The utility model provides a kind of new type of continuous extraction equipment, including extraction kettle and vacuum distillation kettle, extraction kettle upper end is communicated with materail tube and organic extractant pipe, Material valve, material head tank, mass flow meter and material bleeder valve are successively arranged on materail tube from top to bottom, is successively arranged vacuum valve, extractant valve, extractant head tank, extractant flowmeter and extractant bleeder valve on organic extractant pipe from top to bottom；Agitating paddle one is equipped in extraction kettle；Extraction kettle side is equipped with transparent linker form, and linker form is U-shaped, one end connection extraction kettle bottom, one end connection extraction kettle top；The top for being evaporated under reduced pressure kettle is connected to jet chimney, and the jet chimney other end is connected to organic extractant head tank, and jet chimney is equipped with cooling device, and extraction kettle bottom is equipped with bottom valve one, and vacuum distillation bottom portion is equipped with bottom valve two.After the utility model extraction and separation, without adjusting extraction kettle, it can repeatedly be extracted, substantially increase production efficiency.
Description
Technical field
The utility model relates to field of chemical equipment, and in particular to a kind of continuous extraction apparatus.
Background technique
Existing extraction equipment, after liquid separation, since water phase is separated, water phase need to be transferred in new extraction kettle,
Extractant can be rejoined and carry out reextraction, be unfavorable for continuous production, and existing extraction equipment does not have blender, no
Conducive to being uniformly mixed, in addition to this, existing extraction kettle cannot intuitively observe whether grease line of demarcation meets the requirements.Therefore,
The utility model provides a kind of new type of continuous extraction equipment, to solve problem above.
Utility model content
In order to solve the problems in the existing technology, the utility model provides a kind of new type of continuous extraction equipment, has
Head tank, timer and flowmeter, can store extractant, and under the premise of being changed without extraction kettle, material can be extracted repeatedly,
With blender convenient for being uniformly mixed, there is linker form, convenient for intuitively observing whether grease line of demarcation meets the requirements.
A kind of new type of continuous extraction equipment, including extraction kettle and vacuum distillation kettle, extraction kettle side are subtracted by conduit connection
Distillation still is pressed, further includes timer, the middle and upper part of the tube at one end connection extraction kettle, other end connection is evaporated under reduced pressure the upper of kettle
Portion, vacuum distillation kettle are lower than extraction kettle, organic phase are enable smoothly to flow into vacuum distillation kettle；The extraction kettle upper end is communicated with material
Pipe and organic extractant pipe are successively arranged Material valve, material head tank, mass flow meter and material on materail tube from top to bottom and put
Liquid valve is successively arranged vacuum valve, organic extractant valve, organic extractant head tank, organic on organic extractant pipe from top to bottom
Extractant flowmeter and organic extractant bleeder valve；Motor one, fixed company on the motor shaft of motor one are further fixed on extraction kettle
It is connected to agitating paddle one, agitating paddle one is set to inside extraction kettle；Extraction kettle side is equipped with transparent linker form, the linker
Form is that U-shaped, U-shaped a port is connected to extraction kettle bottom, another port is connected at the top of extraction kettle；The vacuum distillation kettle
Top be connected to jet chimney, the jet chimney other end be connected to organic extractant head tank, jet chimney is close to organic extractant
One end of head tank is equipped with cooling device, and the vacuum valve other end connects vacuum pump, and the extraction kettle bottom is equipped with bottom valve one,
The vacuum distillation bottom portion is equipped with bottom valve two.
A kind of above-mentioned new type of continuous extraction equipment, the vacuum distillation kettle are externally provided with collet, and collet side is equipped with steam
Import, the opposite other side are equipped with steam (vapor) outlet, are equipped with temp probe in vacuum distillation kettle.
A kind of above-mentioned new type of continuous extraction equipment, the vacuum distillation kettle top end are fixedly connected with motor two, motor two
Motor shaft on be fixedly connected with agitating paddle two, agitating paddle two is set to inside vacuum distillation kettle.
A kind of above-mentioned new type of continuous extraction equipment, the vacuum distillation kettle top portion are equipped with vacuum meter.
A kind of above-mentioned new type of continuous extraction equipment, the conduit middle part are equipped with communicating valve.
Compared with prior art, the utility model has the beneficial effects that
1, when liquid separation, by exporting upper organic phase, and new organic extractant is supplemented, carries out reextraction, it can be with
In the case where being changed without extraction kettle, material is repeatedly extracted, equipment cost and time cost is greatly saved.
2, the material and extractant being added in extraction kettle can be quantified by flowmeter, and by being connected on kettle
Linker form, observation grease line of demarcation whether meet the requirements, thus decide whether open communicating valve it is organic by what is extracted
It is mutually discharged in vacuum distillation kettle, equipment is simple, easy to implement the method.
3, by be evaporated under reduced pressure and organic extractant is recovered in organic extractant head tank to extraction phase, both may be used
Quickly obtain extraction extract, and may be implemented in extraction process synchronous recycling and reusing extractant, be greatly saved material at
Sheet and time cost.
4, by the temperature and vacuum degree in monitoring vacuum distillation kettle, its vacuum strength and the rate of heat addition, Ke Yishi are adjusted
Now different extractants are recovered under reduced pressure.
5, material is allowed quickly to be uniformly mixed and be layered by agitating paddle one and agitating paddle two.
Detailed description of the invention
The utility model is described in further detail in the following with reference to the drawings and specific embodiments.
Fig. 1 is the structural schematic diagram of the utility model.
In figure: 1, vacuum valve；2, organic extractant valve；3, Material valve；4, organic extractant head tank；5, material is high-order
Slot；6, organic extractant flowmeter；7, mass flow meter；8, organic extractant bleeder valve；9, material bleeder valve；10, motor one；
11, extraction kettle；12, agitating paddle one；13, linker form；14, bottom valve one；15, communicating valve；16, steam inlet；17, steam goes out
Mouthful；18, collet；19, motor two；20, agitating paddle two；21, vacuum meter；22, temp probe；23, bottom valve two；24, it is evaporated under reduced pressure
Kettle；25, jet chimney；26, cooling device.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
A kind of new type of continuous extraction equipment, including extraction kettle 11 and vacuum distillation kettle 24,11 side of extraction kettle passes through conduit
Connection vacuum distillation kettle 24, further includes timer, the middle and upper part of the tube at one end connection extraction kettle 11, other end connection decompression
The top of distillation still 24, vacuum distillation kettle is lower than extraction kettle (that is, the conduit mouth of connection vacuum distillation kettle is lower than connection extraction kettle
Conduit mouth), so that organic phase is smoothly flowed into vacuum distillation kettle；The extraction kettle upper end is communicated with materail tube and organic extractant
It manages, is successively arranged Material valve 3, material head tank 5, mass flow meter 7 and material bleeder valve 9 from top to bottom on materail tube, extract
Vacuum valve 1, organic extractant valve 2, organic extractant head tank 4, organic extraction agent flux are successively arranged on agent pipe from top to bottom
Meter 6 and organic extractant bleeder valve 8；It is further fixed on motor 1 on extraction kettle, is fixedly connected on the motor shaft of motor 1
Agitating paddle 1, agitating paddle 1 are set to inside extraction kettle, and hole, the motor shaft through hole of motor 1 are provided on the extraction kettle
Agitating paddle 1 is fixedly connected in into extraction kettle, this, which is fixedly connected, can be welding, and motor shaft and agitating paddle 1 can be by
Steel is made, and is sealed between motor shaft and extraction kettle with sealing ring；Extraction kettle side is equipped with transparent linker form 13, described
Linker form 13 is that U-shaped, U-shaped a port is connected to extraction kettle bottom, another port is connected at the top of extraction kettle；It is described to subtract
The top of distillation still is pressed to be connected to jet chimney 25,25 other end of jet chimney is connected to organic extractant head tank 4, jet chimney 25
It is equipped with cooling device 26 close to one end of organic extractant head tank 4, the extraction kettle bottom is equipped with bottom valve 1 (in extraction kettle
Bottom sets a short tube, and bottom valve one is located on short tube), the vacuum distillation bottom portion is equipped with bottom valve 2 23 (in vacuum distillation bottom
Portion sets a short tube, and bottom valve two is located on short tube).The cooling device uses the prior art, such as condenser pipe.Motor one and motor
Two are bolted respectively on extraction kettle and vacuum distillation kettle.The vacuum valve other end connects vacuum pump (having been omitted from figure).
The extraction equipment further includes timer, and timer and flowmeter are used cooperatively, quantitative to extractant by time and flow velocity.Timing
Device uses common stopwatch, may connect on device, also can be used alone.
Preferably, the vacuum distillation kettle is externally provided with collet 18, and 18 side upper end of collet is equipped with steam inlet 16, opposite
Other side upper end be equipped with steam (vapor) outlet 17, vacuum distillation kettle in be equipped with temp probe 22 (vacuum distillation kettle top portion open an aperture,
Temp probe 22 is inserted into vacuum distillation kettle from aperture, is sealed between aperture and temp probe with sealing ring).
Preferably, the vacuum distillation kettle top end is fixedly connected with motor 2 19, fixed company on the motor shaft of motor 2 19
It is connected to agitating paddle 2 20, agitating paddle 2 20 is set to inside vacuum distillation kettle, it is provided with hole on the vacuum distillation kettle, motor 2 19
Motor shaft through hole enter vacuum distillation kettle in is fixedly connected with agitating paddle 2 20, this, which is fixedly connected, can be welding, motor shaft with
Agitating paddle two can be made of steel, be sealed between motor shaft and vacuum distillation kettle with sealing ring.
Preferably, the vacuum distillation kettle top portion is equipped with vacuum meter 21.
Preferably, communicating valve 15 is equipped in the middle part of the conduit.
Before utility model works, all valves and equipment are closed.When bringing into operation, organic extractant valve 2 and object are opened
Expect valve 3, supplement organic extractant and material are carried out to organic extractant head tank 4 and material head tank 5.After supplement, open
Opening motor 1 drives one 12 pairs of extraction kettles 11 of agitating paddle to be stirred, while opening organic extractant bleeder valve 8 and material is put
Liquid valve 9 cooperates timer to be quantitatively adding extractant and material by organic extractant flowmeter 6 and mass flow meter 7.It extracts molten
Liquid after mixing evenly, stops the operation of motor 1, stratification, by linker form 13 observe liquid separation line it is whether clear,
Whether height is qualified.After the clear qualification of layering, all valves and equipment are closed, vacuum valve 1 and vacuum pump, cooling device are opened
26, motor 2 19 drives agitating paddle 2 20, carries out steam heating by 18 pairs of vacuum distillation kettles 24 of collet.Communicating valve 15 is opened,
Organic phase is transferred in vacuum distillation kettle 24 from extraction kettle 11, and is evaporated under reduced pressure, organic steam passes through jet chimney 25
It comes in cooling device 26, organic solvent is condensed into liquid phase, and is recovered in organic extractant head tank 4 and is recycled.Extraction
After taking, water phase is discharged into waste water treatment system by bottom valve 1, and extraction products obtained therefrom is carried out down by bottom valve 2 23
The processing of one step.
The foregoing is merely the utility model preferred embodiment, be not intended to limit the embodiments of the present invention and
Protection scope should can appreciate that all in the utility model specification and diagram to those skilled in the art
Hold the equivalent replacement made and obviously change obtained scheme, the protection scope of the utility model should all be included in
It is interior.
Claims (5)
1. a kind of new type of continuous extraction equipment, including extraction kettle and vacuum distillation kettle, extraction kettle side are connected to by conduit and are depressurized
Distillation still, which is characterized in that it further include timer, the middle and upper part of the tube at one end connection extraction kettle, other end connection decompression
The top of distillation still, vacuum distillation kettle are lower than extraction kettle, organic phase are enable smoothly to flow into vacuum distillation kettle；The extraction kettle upper end
It is communicated with materail tube and organic extractant pipe, is successively arranged Material valve, material head tank, mass flow on materail tube from top to bottom
It is high to be successively arranged vacuum valve, organic extractant valve, organic extractant on organic extractant pipe from top to bottom for meter and material bleeder valve
Position slot, organic extractant flowmeter and organic extractant bleeder valve；Motor one, the motor shaft of motor one are further fixed on extraction kettle
On be fixedly connected with agitating paddle one, agitating paddle one is set to inside extraction kettle；Extraction kettle side is equipped with transparent linker form, institute
Stating linker form is that U-shaped, U-shaped a port is connected to extraction kettle bottom, another port is connected at the top of extraction kettle；It is described to subtract
The top of distillation still is pressed to be connected to jet chimney, the jet chimney other end is connected to organic extractant head tank, and jet chimney is close to be had
One end of machine extractant head tank is equipped with cooling device, and the vacuum valve other end connects vacuum pump, and the extraction kettle bottom is set
There is bottom valve one, the vacuum distillation bottom portion is equipped with bottom valve two.
2. a kind of new type of continuous extraction equipment according to claim 1, which is characterized in that the vacuum distillation kettle is externally provided with
Collet, collet side are equipped with steam inlet, and the opposite other side is equipped with steam (vapor) outlet, is equipped with temp probe in vacuum distillation kettle.
3. a kind of new type of continuous extraction equipment according to claim 1, which is characterized in that the vacuum distillation kettle top end is solid
Surely it is connected with motor two, agitating paddle two is fixedly connected on the motor shaft of motor two, agitating paddle two is set to inside vacuum distillation kettle.
4. a kind of new type of continuous extraction equipment according to claim 1, which is characterized in that the vacuum distillation kettle top portion is set
There is vacuum meter.
5. a kind of new type of continuous extraction equipment according to claim 1, which is characterized in that be equipped with connection in the middle part of the conduit
Valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821231432.3U CN208711104U (en) | 2018-08-01 | 2018-08-01 | A kind of new type of continuous extraction equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821231432.3U CN208711104U (en) | 2018-08-01 | 2018-08-01 | A kind of new type of continuous extraction equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208711104U true CN208711104U (en) | 2019-04-09 |
Family
ID=65975734
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821231432.3U Expired - Fee Related CN208711104U (en) | 2018-08-01 | 2018-08-01 | A kind of new type of continuous extraction equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208711104U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115487537A (en) * | 2022-08-02 | 2022-12-20 | 湖南金凯循环科技有限公司 | Equipment for recovering waste extracting agent |
-
2018
- 2018-08-01 CN CN201821231432.3U patent/CN208711104U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115487537A (en) * | 2022-08-02 | 2022-12-20 | 湖南金凯循环科技有限公司 | Equipment for recovering waste extracting agent |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190409 Termination date: 20190801 |
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| CF01 | Termination of patent right due to non-payment of annual fee |