CN206470070U - A kind of detachable sampler of reactor - Google Patents
A kind of detachable sampler of reactor Download PDFInfo
- Publication number
- CN206470070U CN206470070U CN201720163931.2U CN201720163931U CN206470070U CN 206470070 U CN206470070 U CN 206470070U CN 201720163931 U CN201720163931 U CN 201720163931U CN 206470070 U CN206470070 U CN 206470070U
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- sampling
- reactor
- interface
- nitrogen
- hand valve
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Abstract
The utility model discloses a kind of detachable sampler of reactor, sample interpolation pipe below flange with being connected, sampling hand valve above flange with being connected, sample interpolation pipe one end is extend into reactor to be sampled, reactor is covered tightly by flange, the other end is connected with sampling hand valve, first bend pipe one end is connected with sampling hand valve, the other end is connected on sampling bottle interface, second bend pipe one end is connected with sampling bottle interface, the other end is connected on surge flask interface, 3rd bend pipe one end is connected with surge flask interface, the other end is connected with nitrogen valve, sampling bottle is arranged on sampling bottle interface, surge flask is arranged on surge flask interface.The sampler can be widely used in Chemical Manufacture reactor sampling process; have the advantages that sampling behaviour is convenient, applied widely, safe and reliable, avoid material from being blocked in pipeline; particularly whole sampling process all in nitrogen protect under, can effectively prevent air, moisture enter reaction system influence.
Description
Technical field
The utility model is related to a kind of detachable sampler of reactor, belongs to technical field of chemical.
Background technology
The sampling of reactor is the important foundation that chemical industry and medical industry production are smoothed out, the technique of complete set
Flow has usually contained substantial amounts of reactor sampling operation.In most of factories, the sampling of reactor is often opening reactor
Mirror mouth or other reactor kettle covers on flange port manual sampling, this operation not only easily makes reaction mass ingress of air
And moisture, cause the loss of material and influence the quality of product, particularly the sampling in dangerous larger medication chemistry product
In safe operation, directly there is serious potential safety hazard in operator from reactor sampling.Commercially available sampling equipment often manufactures multiple
Miscellaneous, price is expensive, and poor for applicability, generally requires for special consersion unit manufacture, and equipment installation and detection
Substantial amounts of logistic work is needed, causes the increase of production cost.
The characteristics of the utility model is simple in construction, and sampling operation is convenient, pollution-free, and operating process whole process is protected in nitrogen
Under shield, safe operation is reliable, passes through nitrogen blowback interpolation pipe Liquid Residue, it is ensured that the reactionless material residual of interpolation pipe, extracts reaction
Material can be in real embodiment reactor reactiveness, it is ensured that the authenticity and reliability of Product checking.
The content of the invention
In order to solve the above problems, the purpose of this utility model is the detachable sampling dress for providing a kind of reactor
Put, the sampler can be widely used in Chemical Manufacture reactor sampling process, with sampling, behaviour uses the convenient, scope of application
Extensively, it is safe and reliable, avoid the advantages of material is blocked or polluted in pipeline, particularly whole sampling process is protected all in nitrogen
Under, it can effectively prevent the environment such as air, moisture and human factor from entering reaction system and influenceing product quality.
The technical solution adopted in the utility model is as follows：
A kind of detachable sampler of reactor, including sample interpolation pipe, flange, sampling hand valve, the first bend pipe, the
Two bend pipes, the 3rd bend pipe, sampling bottle interface, surge flask interface, nitrogen hand valve, nitrogen valve, sample interpolation pipe and flange lower section
It is connected, sampling hand valve above flange with being connected, and sample interpolation pipe one end is extend into reactor to be sampled, is covered tightly by flange
Reactor, the other end is connected with sampling hand valve, and first bend pipe one end is connected with sampling hand valve, and the other end is connected to sampling bottle interface
On, second bend pipe one end is connected with sampling bottle interface, and the other end is connected on surge flask interface, the 3rd bend pipe one end and surge flask
Interface is connected, and the other end is connected with nitrogen valve, and sampling bottle is arranged on sampling bottle interface, and surge flask is arranged on surge flask interface
On.
Nitrogen hand valve is provided with 3rd bend pipe, nitrogen hand valve is arranged on the pipeline of nitrogen valve one end.
Sampling bottle interface routine sampling bottle is tightened, and surge flask interface is tightened as buffering, nitrogen gas with conventional surge flask
Mouth is connected in nitrogen pipeline.
Sample interpolation pipe is 316 stainless-steel pipes.The sampling hand valve is that DN10 samples hand valve.
First bend pipe, the second bend pipe, the material of the 3rd bend pipe are 316 stainless-steel pipes.
Sampling bottle interface is connected between first bend pipe and the second bend pipe, sampling bottle interface is used to install sampling bottle.
Surge flask interface is connected between second bend pipe and the 3rd bend pipe, surge flask interface is used to install surge flask.The
The three bend pipe other ends connect nitrogen hand valve and nitrogen valve, and nitrogen valve spends connection nitrogen pipeline.
During sampling, in sample interpolation pipe intercalation reaction kettle, flange tightens screw with reactor kettle cover installing port, installs
Into.During sampling operation, nitrogen hand valve is first opened, nitrogen is filled with into reactor and keeps pressure-fired in reactor, nitrogen hand is closed
Valve, opens sampling hand valve, material is filled into sampling bottle, material is reached after sampling amount, sampling hand valve is closed, by reactor
Pressure-emptying to normal pressure, by connecting nitrogen pipeline at nitrogen valve, nitrogen hand valve, sampling hand valve are opened successively, will be sampled
Residual material in interpolation pipe is pushed back in reactor, and nitrogen hand valve, sampling hand valve are closed after terminating and sampling bottle is removed, completes to take
Sample is operated, the sampler Whole-dismountable, and by increasing, buffering pipeline is gentle to rush bottle, effectively completely cuts off air, moisture etc.
The influence of environmental factor, it is ensured that the quality safety of sample and reaction mass.
Beneficial effect
A kind of detachable sampler for reactor that the utility model is provided, its is applied widely, may be mounted at
On the reactor of different volumes, installation process is simple, and without special training, sampling is convenient, and is provided with buffer unit and nitrogen
Air pipe, it is ensured that sampling process is all carried out under nitrogen protection, effectively completely cuts off the influence of the environmental factors such as air, moisture, it is ensured that
The quality safety of sample and reaction mass, nitrogen valve connection nitrogen pipeline, interpolation pipe can be effectively reduced by the purging of nitrogen
Road liquid residue, whole operation is safe and reliable, greatly improves the operating efficiency of sampling and production.
Brief description of the drawings
A kind of detachable sampler structure chart of reactors of Fig. 1；
Wherein：1- sample interpolations pipe, 2- flanges, 3- samplings hand valve, the bend pipes of 4- first, the bend pipes of 5- second, the bend pipes of 6- the 3rd,
7- sampling bottles interface, 8- surge flasks interface, 9- nitrogen hands valve, 10- nitrogen valve, 11- sampling bottles, 12- surge flasks.
Embodiment
Embodiment 1
The detachable sampler of a kind of reactor, as shown in figure 1, including sample interpolation pipe 1, flange 2, sampling hand valve
3rd, the first bend pipe 4, the second bend pipe 5, the 3rd bend pipe 6, sampling bottle interface 7, surge flask interface 8, nitrogen hand valve 9, nitrogen valve 10,
The one end of sample interpolation pipe 1 is extend into reactor to be sampled, and reactor, the other end and the sampling phase of hand valve 3 are covered tightly by flange 2
Even, the one end of the first bend pipe 4 is connected with sampling hand valve 3, and the other end is connected on sampling bottle interface 7, the one end of the second bend pipe 5 and sampling
Bottle interface 7 be connected, the other end is connected on surge flask interface 8, and the one end of the 3rd bend pipe 6 is connected with surge flask interface 8, the other end and
Nitrogen valve 10 is connected, and nitrogen hand valve 9 is arranged on the 3rd bend pipe on the pipeline of the one end of nitrogen valve 10, and sampling bottle 11 is pacified
On sampling bottle interface 7, surge flask 12 is arranged on surge flask interface 8.The nitrogen valve 10 is connected with nitrogen pipeline, takes
The material of sample interpolation pipe is 316 stainless steels, and sampling hand valve is that DN10 samples hand valve.
When equipment is installed, in the intercalation reaction kettle of sample interpolation pipe 1, flange 2 tightens screw with reactor kettle cover installing port, pacifies
Install into.During sampling operation, nitrogen is filled with into reactor and keeps pressure-fired in reactor, opened sampling hand valve 3, material is filled
Enter into sampling bottle, material is reached after sampling amount, close sampling hand valve, by the pressure-emptying in reactor to normal pressure, pass through nitrogen
Nitrogen pipeline is connected at gas valve, nitrogen hand valve, sampling hand valve are opened successively, the residual material in sample interpolation pipe is pushed back instead
Answer in kettle, nitrogen hand valve, sampling hand valve are closed after terminating and sampling bottle is removed, sampling operation is completed.Whole sampler is removable
Unload, sampling process under nitrogen protection, and is provided with surge flask and separator tube road, effectively prevents the environment such as air, moisture and people
Entering reaction system for factor influences product quality, it is ensured that the quality safety of sample and reaction mass.It is described detachable to take
Sampling device, its is applied widely, may be mounted on the reactor of different volumes, and installation process is simple, without special training, takes
Just, whole operation is safe and reliable for sample prescription, greatly improves the operating efficiency of sampling and production.
Claims (5)
1. the detachable sampler of a kind of reactor, it is characterised in that including sample interpolation pipe（1）, flange（2）, sampling
Hand valve（3）, the first bend pipe（4）, the second bend pipe（5）, the 3rd bend pipe（6）, sampling bottle interface（7）, surge flask interface（8）, nitrogen
Valve（10）, sample interpolation pipe（1）One end is extend into reactor to be sampled, passes through flange（2）Cover tightly reactor, the other end
With sampling hand valve（3）It is connected, the first bend pipe（4）One end and sampling hand valve（3）It is connected, the other end is connected to sampling bottle interface（7）
On, the second bend pipe（5）One end and sampling bottle interface（7）It is connected, the other end is connected to surge flask interface（8）On, the 3rd bend pipe（6）
One end and surge flask interface（8）It is connected, the other end and nitrogen valve（10）It is connected, sampling bottle（11）Installed in sampling bottle interface
（7）On, surge flask（12）Installed in surge flask interface（8）On.
2. a kind of detachable sampler of reactor according to claim 1, it is characterised in that the 3rd bend pipe
（6）On be provided with nitrogen hand valve（9）, nitrogen hand valve（9）It is arranged on nitrogen valve（10）On the pipeline of one end.
3. a kind of detachable sampler of reactor according to claim 1, it is characterised in that the nitrogen valve
（10）It is connected with nitrogen pipeline.
4. a kind of detachable sampler of reactor according to claim 1, it is characterised in that the sample interpolation
Pipe（1）For 316 stainless-steel pipes.
5. a kind of detachable sampler of reactor according to claim 1, it is characterised in that the sampling hand valve
Hand valve is sampled for DN10.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720163931.2U CN206470070U (en) | 2017-02-23 | 2017-02-23 | A kind of detachable sampler of reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720163931.2U CN206470070U (en) | 2017-02-23 | 2017-02-23 | A kind of detachable sampler of reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206470070U true CN206470070U (en) | 2017-09-05 |
Family
ID=59707597
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720163931.2U Active CN206470070U (en) | 2017-02-23 | 2017-02-23 | A kind of detachable sampler of reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206470070U (en) |
-
2017
- 2017-02-23 CN CN201720163931.2U patent/CN206470070U/en active Active
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