CN206415132U - Tube furnace crucible - Google Patents

Tube furnace crucible Download PDF

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Publication number
CN206415132U
CN206415132U CN201720037960.4U CN201720037960U CN206415132U CN 206415132 U CN206415132 U CN 206415132U CN 201720037960 U CN201720037960 U CN 201720037960U CN 206415132 U CN206415132 U CN 206415132U
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CN
China
Prior art keywords
crucible
groove
tripod
tube furnace
hole
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720037960.4U
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Chinese (zh)
Inventor
王涛
唐翠兰
杜凯
何小珊
黄景林
陈果
刘艳松
何智兵
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Laser Fusion Research Center China Academy of Engineering Physics
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Laser Fusion Research Center China Academy of Engineering Physics
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
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Priority to CN201720037960.4U priority Critical patent/CN206415132U/en
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Publication of CN206415132U publication Critical patent/CN206415132U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

It is a kind of simple in construction the utility model discloses a kind of tube furnace crucible, multiple or several samples experimental implementations can be completed simultaneously, the cost-effective, time, improve the tube furnace crucible of conventional efficient, the technical scheme of use is:Tube furnace crucible, including crucible groove, tripod and upper lid, crucible groove are in arc-shaped and closed at both ends, and the lower edge of upper lid sets raised and is adapted with crucible groove;At least one layer of tripod is placed in crucible groove, the both sides of tripod are curved and are adapted with crucible groove arc-shaped inner surface, to maintain each crucible frame horizontal;Multiple through holes and/or groove are set on tripod, and groove directly accommodates sample to be tested, when tripod is provided with through hole, small crucible body is placed respectively in through hole.Tube furnace is simple with crucible structure, easy to assemble, can carry out high temperature sintering, high temeperature chemistry compound experiment simultaneously to multiple or several samples, save experiment and take, reduce experimental cost, improve conventional efficient.

Description

Tube furnace crucible
Technical field
The utility model is related to a kind of crucible, especially a kind of to be used for the experiment productions such as high temperature sintering, high temeperature chemistry synthesis The tube furnace crucible of process.
Background technology
Crucible is a kind of important chemical experimental instrument, is made up of refractory material, available for solid, powdered rubber burn Burn, evaporative crystallization of solution etc., is to ensure the basis that physical-chemical reaction is smoothed out.Lead in existing sintering or smelting process Crucibles agglomerated material is often utilized, but generally each crucible can only accommodate one or two sample and be tested.For example it is public Cloth number discloses a kind of detachable crucible of double-purpose for CN105783510A patent document, and two kinds of different materials can be completed simultaneously Experimental implementation.However, generally requiring multiple material during experimental implementation while being operated, need to waste big when carrying out successively The time of amount, test efficiency is low.
Utility model content
Technical problem to be solved in the utility model is to provide a kind of simple in construction, and multiple or a variety of samples can be completed simultaneously The experimental implementation of product, the cost-effective, time, improves the tube furnace crucible of conventional efficient.
The utility model solves the technical scheme that its technical problem used:Tube furnace crucible, including crucible groove, earthenware Crucible frame and upper lid, the crucible groove are in arc-shaped and closed at both ends, and the arc angle of crucible groove is no more than 180 °, the upper lid Lower edge sets raised, raised rectangular ring-type, and is adapted with the crucible groove upper surface;Placed at least in the crucible groove One layer of tripod, the both sides of tripod are curved and are adapted with crucible groove arc-shaped inner surface, set many on tripod Individual through hole and/or groove;And when tripod is provided with through hole, small crucible body is placed respectively in through hole, small crucible body is in top The tubular of portion's opening.
It is further:At least two layers tripod is placed in the crucible groove, each crucible frame is parallel to each other;Work as tripod Quantity when reaching 3, each crucible frame equidistantly distributed in crucible groove;The through hole is circle, and the groove is hemispherical.
It is further:The hemispherical groove of equidistant spread configuration, the tripod of other layers on the tripod of the bottom The circular through hole of upper equidistant spread configuration.
It is further:When the upper cover buckle is together on crucible groove, the projection of upper lid is located at the outside of crucible groove.
It is further:At least one steam vent is also set up on the upper lid.
It is further:The center of the upper surface of the upper lid sets drop handle.
It is further:The two ends of the crucible groove set the handle of semicircle shape respectively.
It is further:The top outer edge of the small crucible body, which has, sets through hole, flange on turnup structure, tripod The diameter of structure is more than the diameter of through hole.
The beneficial effects of the utility model are:Tube furnace is simple with crucible structure, easy to assemble, can be placed on tripod multiple Small crucible body, small crucible body is used to accommodate sample to be tested, and small crucible body is stuck on the through hole of tripod, places firm peace Entirely;Groove on tripod also can directly accommodate sample to be tested.Tube furnace is realized to multiple samples with crucible while entering Several samples can also be tested by row high temperature sintering, high temeperature chemistry compound experiment simultaneously, are greatlyd save experiment and are taken, have Experimental cost is reduced to effect, conventional efficient is drastically increased.
Brief description of the drawings
Fig. 1 is the explosive view of the utility model tube furnace crucible.
Fig. 2 is the overall appearance figure of the utility model tube furnace crucible.
Fig. 3 is the bottom view of the upper lid of the utility model tube furnace crucible.
Fig. 4 is the overall appearance figure of the small crucible body of the utility model tube furnace crucible.
Parts, position and numbering in figure:Crucible groove 1, tripod 2, upper lid 3, projection 4, through hole 5, groove 6, small crucible Body 7, steam vent 8, drop handle 9, handle 10.
Embodiment
The utility model is described in further detail below in conjunction with the accompanying drawings.
As illustrated in fig. 1 and 2, the utility model tube furnace crucible, including crucible groove 1, tripod 2 and upper lid 3, crucible groove 1 is in arc-shaped and closed at both ends, and the arc angle of crucible groove 1 is no more than 180 °, such as shown in Fig. 1 and Fig. 2, the circle of crucible groove 1 Arc angle is 180 °, and now crucible groove 1 is in semi-cylindrical.The two ends of crucible groove 1 set the handle 10 of semicircle shape respectively, facilitate hand-held Take and moved using hook in tube furnace.At least one layer of tripod 2 is placed in crucible groove 1, the both sides of tripod 2 are in Arc and it is adapted respectively with the arc-shaped inner surface of crucible groove 1, multiple through holes 5 and/or groove 6 is set on tripod 2.Groove 6 is used In directly accommodating sample to be tested.Also, when tripod 2 is provided with through hole 5, small crucible body 7 is placed respectively in through hole 5, Small crucible body 7 is in open-topped tubular.Through hole 5 on tripod 2 is used to place small crucible body 7, such as Fig. 4 institutes of small crucible body 7 Show.The top outer edge of small crucible body 7 has turnup structure, and diameter of the diameter more than through hole 5 of turnup structure, small to avoid Crucible body 7 slides out of through hole 5.In addition, the outline of small crucible body 7 can also be in big top and small bottom, in order to which small crucible body 7 is in earthenware Picking and placeing in the through hole 5 of crucible frame 2.
At least one layer of tripod 2 is placed in crucible groove 1.Specifically, at least two layers tripod 2, each layer are placed in crucible groove 1 Tripod 2 is parallel to each other.When the quantity of tripod 2 reaches 3, each crucible frame 2 equidistantly distributed, i.e. phase in crucible groove 1 The distance between adjacent two layers of tripod 2 is equal.Through hole 5 on tripod 2 is used to place small crucible body 7, and through hole 5 is rounded;Earthenware Groove 6 on crucible frame 2 is used to accommodate sample to be tested, and groove 6 is in hemispherical.
The both sides of tripod 2 are curved and are adapted with the arc-shaped inner surface of crucible groove 1, after the horizontal positioned of crucible groove 1, earthenware The arc of the both sides of crucible frame 2 can ensure that upper tripod 2 is horizontal, or keep horizontal trend, and this contributes to dimension Hold each crucible frame 2 and keep horizontal, and make full use of the inner space of crucible groove 1.
Equidistant spread configuration on two layers of tripod 2, the tripod 2 of bottom is placed in such as Fig. 1, crucible groove 1 hemispherical The circular through hole 5 of equidistant spread configuration on groove 6, the tripod 2 on upper strata.It is equal that through hole 5 and groove 6 press certain ranks number Arrange evenly.The tripod 2 of the upper layer of tripod 2 of bottom is thick, and enough depth can be set on the tripod 2 to ensure bottom Groove 6, to accommodate sample to be tested.
As Figure 1-3, the lower edge setting projection 4 of upper lid 3, raised 4 rectangular ring-types, and on upper lid 3 and crucible groove 1 Surface is adapted.When upper lid 3 is fastened on crucible groove 1, the projection 4 of upper lid 3 is located at the outside of crucible groove 1.Also set on upper lid 3 At least one steam vent 8 is put, such as the upper edge of lid 3 sets a steam vent 8, it is ensured that the discharge of gas in experimentation.Upper lid 3 The center of upper surface drop handle 9 is set, drop handle 9 can play a part of mobile upper lid 3.
Raw material to be sintered is put into small crucible body 7, small crucible body 7 is placed in the through hole 5 of tripod 2, tripod 2 it is recessed Groove 6 also can directly accommodate sample to be tested, and keep parallel to each other between tripod 2, then upper lid 3 is placed on crucible groove 1, It is placed in tube furnace and is sintered again.Sintering is finished, after cooling, and handle 10 is hooked with hook and is taken out.

Claims (8)

1. tube furnace crucible, it is characterised in that:Including crucible groove (1), tripod (2) and upper lid (3), the crucible groove (1) In arc-shaped and closed at both ends, the arc angle of crucible groove (1) is no more than 180 °, and the lower edge of the upper lid (3) sets raised (4), raised (4) rectangular ring-type, and being adapted with crucible groove (1) upper surface;At least one is placed in the crucible groove (1) The layer tripod (2), the both sides of tripod (2) are curved and are adapted with crucible groove (1) arc-shaped inner surface, tripod (2) multiple through holes (5) and/or groove (6) are set on;And when tripod (2) is provided with through hole (5), in through hole (5) respectively Small crucible body (7) is placed, small crucible body (7) is in open-topped tubular.
2. tube furnace crucible as claimed in claim 1, it is characterised in that:At least two layers earthenware is placed in the crucible groove (1) Crucible frame (2), each crucible frame (2) is parallel to each other;When the quantity of tripod (2) reaches 3, each crucible frame (2) is in crucible groove (1) interior equidistantly distributed;The through hole (5) is circle, and the groove (6) is hemispherical.
3. tube furnace crucible as claimed in claim 2, it is characterised in that:Equidistantly arranged on the tripod (2) of the bottom The circular through hole (5) of equidistant spread configuration on hemispherical groove (6), the tripod (2) of other layers is set.
4. the tube furnace crucible as described in claims 1 to 3 any claim, it is characterised in that:The upper lid (3) fastens When on crucible groove (1), the projection (4) of upper lid (3) is located at the outside of crucible groove (1).
5. the tube furnace crucible as described in claims 1 to 3 any claim, it is characterised in that:On the upper lid (3) also At least one steam vent (8) is set.
6. the tube furnace crucible as described in claims 1 to 3 any claim, it is characterised in that:It is described it is upper lid (3) it is upper The center on surface sets drop handle (9).
7. the tube furnace crucible as described in claims 1 to 3 any claim, it is characterised in that:The crucible groove (1) Two ends set the handle (10) of semicircle shape respectively.
8. the tube furnace crucible as described in claims 1 to 3 any claim, it is characterised in that:The small crucible body (7) Top outer edge have through hole (5) be set on turnup structure, tripod (2), the diameter of turnup structure is more than the straight of through hole (5) Footpath.
CN201720037960.4U 2017-01-13 2017-01-13 Tube furnace crucible Expired - Fee Related CN206415132U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720037960.4U CN206415132U (en) 2017-01-13 2017-01-13 Tube furnace crucible

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720037960.4U CN206415132U (en) 2017-01-13 2017-01-13 Tube furnace crucible

Publications (1)

Publication Number Publication Date
CN206415132U true CN206415132U (en) 2017-08-18

Family

ID=59571800

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720037960.4U Expired - Fee Related CN206415132U (en) 2017-01-13 2017-01-13 Tube furnace crucible

Country Status (1)

Country Link
CN (1) CN206415132U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106732850A (en) * 2017-01-13 2017-05-31 中国工程物理研究院激光聚变研究中心 Tube furnace crucible

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106732850A (en) * 2017-01-13 2017-05-31 中国工程物理研究院激光聚变研究中心 Tube furnace crucible

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170818

Termination date: 20210113

CF01 Termination of patent right due to non-payment of annual fee