CN206330835U - A kind of microscope tensilometer adapted on light microscope - Google Patents

A kind of microscope tensilometer adapted on light microscope Download PDF

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Publication number
CN206330835U
CN206330835U CN201621293167.2U CN201621293167U CN206330835U CN 206330835 U CN206330835 U CN 206330835U CN 201621293167 U CN201621293167 U CN 201621293167U CN 206330835 U CN206330835 U CN 206330835U
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China
Prior art keywords
sample
stationary fixture
side plate
tensilometer
sample stationary
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Expired - Fee Related
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CN201621293167.2U
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Chinese (zh)
Inventor
张占平
宋小飞
齐育红
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Dalian Maritime University
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Dalian Maritime University
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Abstract

The utility model discloses a kind of microscope tensilometer adapted on light microscope, the tensilometer includes sample stationary fixture, it is V-arrangement, circular arc or trapezoidal with the clamping face of sample contacts clamped by sample, the sample stationary fixture includes upper grip and lower chuck, and the upper grip and lower chuck clamp sample by tightening fastening screw.Tensilometer of the present utility model has special-shaped sample stationary fixture, can guarantee that macromolecular elastomer material will not deviate from drawing process because of thinning, the stretching experiment complete to the very high macromolecular elastomer material progress of deformation rate;A series of light microscopes that can be adapted in laboratory, it is easy to operate, without being modified to light microscope, when using, to good position, it is horizontal forward to be pushed into portable microscope tensilometer below the camera lens of light microscope, sample is in the field of view of optical microphotograph lens head.

Description

A kind of microscope tensilometer adapted on light microscope
Technical field
The utility model is related to elastomeric material to carry out using during modification of surface morphology observation under different stretch state Light microscope on compact tensile instrument.
Background technology
Existing common stretching instrument can only carry out macromechanics test, and the mechanics of macromolecular elastomer material to sample Performance and its structure change etc. are closely related, therefore material mechanical performance change procedure and material structure etc. are combined into progress Research, is conducive to carrying out more in-depth study to macromolecular material.Although also having some by material mechanical performance and microcosmic chi Degree combines the document in the test device studied, such as following table:
But it is main both for the extremely limited instrument of infrared spectrometry instrument, this sample pool space of ESEM, it is high Molecular flexibility body material deformation quantity in drawing process is larger, and the volume for being limited to sample cell is limited, and the device in upper table is not Can completely observes material from being stretched to the whole change procedure broken, and using being needed before scanning electron microscopic observation sample pair Sample surfaces carry out the processing such as metal spraying, can also influence the observation to material real topography.Light microscope can be open Used in environment, it is very not strict for size requirement of sample etc. due to its structure design, do not have to the lateral dimension of sample It is restricted, and as technology develops, light microscope can also reach very high resolution ratio, particularly super depth of field optical microphotograph Mirror and laser confocal scanning microscope, can not only meet the observation requirement to material microscopic appearance structure, and can enter The three-dimensional geometry measurement of row material surface pattern, the brand-new visual field is provided for material surface morphology observation research.
Utility model content
The purpose of this utility model is to solve the problems, such as that material uses the microscopical observation and analysis of optics in drawing process, no Change any structure of existing light microscope, Tensile Tester can be erected on microscope, made in drawing process Sample is under microscopical camera lens, and does not influence the operation during microscope use.
The technical solution of the utility model is as follows:
A kind of sample stationary fixture on light microscope tensilometer, it is with the clamping face of clamped sample contacts V-arrangement, circular arc or trapezoidal.
Further, the sample stationary fixture includes upper grip and lower chuck, and the upper grip and lower chuck are by twisting Tight fastening screw clamps sample.When tightening fastening screw, fastening screw can drive direction of the upper grip along fastening screw The axial movement close to lower chuck is done, plays a part of clamping sample.The clamping face of the upper grip and the clamping face of lower chuck It is adapted, the clamping face formed with clamped sample contacts is V-arrangement, circular arc or trapezoidal sample stationary fixture.
Further, it is respectively equipped with tooth line on the upper grip of the sample stationary fixture and the clamping face of lower chuck.
The utility model also provides a kind of light microscope tensilometer adapted on light microscope, and it includes above-mentioned Sample stationary fixture, fixed mount, pulling force sensor, drive mechanism and biaxial tension mechanism;
The sample stationary fixture is made up of sample stationary fixture I and sample stationary fixture II;The biaxial tension mechanism Including driving section, the side plate II of side plate I;The drive mechanism connects the driving section, drives the side plate I and side plate II to do conversely The displacement movement in direction;The sample stationary fixture I is fixedly connected with the side plate I, the sample stationary fixture II with it is described Side plate II is fixedly connected, and the pulling force sensor is fixedly connected between sample stationary fixture I and side plate I or sample stationary fixture Between II and side plate II.Preferably, the pulling force sensor is fixedly connected between sample stationary fixture II and side plate II, i.e. institute The one end for stating pulling force sensor is fixedly connected on sample stationary fixture II, and the other end is fixedly connected on side plate II, test sample Tensile load.
Further, the drive mechanism includes closed loop stepper motor, bellows coupling;
The driving section includes nut I, nut II and left-right rotary screw rod, and nut I and nut II and left-right rotary screw rod are with spiral shell The mode of line connection is connected;The closed loop stepper motor is fixedly connected with the left-right rotary screw rod by bellows coupling; The sample stationary fixture I is fixedly connected nut I by side plate I, and the sample stationary fixture II is fixedly connected by side plate II Nut II.Preferably, sample stationary fixture II is fixedly connected nut II by pulling force sensor with side plate II.
Further, described light microscope tensilometer, also including support base, fixed seat, polished rod, fixed mount and branch Frame;The polished rod wears the even support base, fixed seat, is slidably connected with side plate I and side plate II;The left-right rotary screw rod passes through institute Support base and fixed seat is stated to be fixedly connected with the bellows coupling;The support base, fixed seat and drive mechanism are fixed and set Put on fixed mount;The support is square set, and the fixed mount is welded and fixed on the bracket.
Light microscope tensilometer described in the utility model, also including controllor for step-by-step motor, can drive to stepper motor Dynamic device sends instruction on request, controls rotating speed, the rotating cycle of stepper motor, thus the draw speed of Control Assay and stretching away from From so the parameter such as draw speed, stretching displacement, incipient extension length can be according to the situation flexible modulation of sample.Stretching The returning quickly of stretching device can be realized by the program setting of controller after end.Data collecting card can real-time high-precision height The analog signal of the collection S type pulling force sensors of frequency, is converted into data signal, is then imported into by USB data line On computer, processing and analysis are acquired to test data by softwares such as Labview conventional in engineering on computers.
The use principle and method of microscope tensilometer described in the utility model are as follows:One end of tensile sample is consolidated Sample stationary fixture I is scheduled on, the other end is fixed on sample stationary fixture II, drives closed loop stepper motor, stepper motor occurs Rotate, bellows coupling starts rotation, drive the left-right rotary screw rod for being secured to connection to rotate, this can drive and left-right rotary again Two nuts of screw slide connection are equidistantly moved to relative to opposite direction constant speed respectively, and nut drives two side plates and two Sample stationary fixture is also to relative opposite direction constant speed equidistance motion, so that tensile sample is elongated, and sample center is protected Hold constant.
The utility model, which is specially devised, is directed to light microscope (including super depth of field light microscope and laser co-focusing Flying-spot microscope) the portable microscope tensilometer that uses, the mechanics of some testers before overcoming in measurement material The drawbacks of Fine Texture of Material morphology observation being carried out while performance:
(1) distinctive special-shaped sample stationary fixture, can guarantee that macromolecular elastomer material will not be because of in drawing process It is thinning and deviate from, complete stretching experiment is carried out to deformation rate very high macromolecular elastomer material;
(2) a series of light microscopes that can be adapted in laboratory, easy to operate, without being carried out to light microscope Change etc., in use, to good position, it is horizontal forward to be pushed into portable microscope tensilometer below the camera lens of light microscope, Sample is set to be in the field of view of optical microphotograph lens head.
(3) stepper motor can be by its rotating speed of programme-control and step number, so that indirect control sample stationary fixture clips examination Sample carries out specific draw speed, the tension test of specific tensile elongation, and drawing process can pass through strain gauge and motor rotation Step number, which converts, obtains the load-deformation curve of material, and observes the corresponding surface in sample certain point on load-deformation curve Pattern, this changes for the tissue topography of research material drawing process and analysis of material fracture process is significant.
(4) due to controllor for step-by-step motor can flexible programming, pulling force sensor and stepper motor can be combined, The experiment that can carry out having particular/special requirement by programming, for example, allow sample to keep constant strain amount, observe the stress relaxation of sample Phenomenon, the load for allowing sample two ends to load keeps constant, the creep properties of observation sample under permanent load etc..
(5) macromolecular elastomer material deformation quantity in drawing process is larger, and sample is easily slided from fixture in drawing process Go out, cause surveyed deformation quantity not to be inconsistent with the true deformation quantity of material, and there is also the phenomenon that sample is slipped from fixture, cause drawing Stretching experiment can not be normally carried out, and fixture is optimized the utility model, and the V-arrangement fixture of design effectively prevent high score bullet The phenomenon for skidding off and slipping from fixture in elastomer material drawing process.
(6) size limitation of the light microscope to sample be not strict, is not limited on horizontal space, effectively stretching length Degree is larger, disclosure satisfy that the requirement of macromolecular elastomer material stretching, and can keep macromolecular elastomer in drawing process The micro- lens head of its center opposing optical keeps constant, meets the demand of home position observation.Carried out using the equipment in situ dynamic State is observed, during sample tensile test is carried out, and can see that the surface topography of tensile sample becomes in real time on microscope The molecularly oriented that change, occurs, such as there is crystallizing at the phenomenon in material in drawing process, obtains in macromolecular material drawing process per a flash Between certain point in the change that occurs, and the load-deformation curve that the change that the moment material occurs is obtained with measurement it is direct It is mapped.
Brief description of the drawings
Fig. 1 is sample stationary fixture schematic diagram of the present utility model, and wherein A is V-arrangement sample stationary fixture, and B is circular arc Sample stationary fixture, C is trapezoidal sample stationary fixture;
Fig. 2 is the structural representation of the utility model tensilometer;
Fig. 3 is the utility model tensilometer step motor control case;
Fig. 4 is schematic diagram when the utility model tensilometer is used for laser confocal microscope;
Fig. 5 is schematic diagram when the utility model tensilometer is used for ordinary optical microscope;
1st, support base;
2nd, left-right rotary screw rod;
3rd, polished rod;
4th, side plate I;
5th, the lower chuck of fixture I;
6th, the upper grip of fixture I;
7th, the upper grip of fixture II;
8th, the lower chuck of fixture II;
9th, pulling force sensor;
10th, side plate II;
11st, fixed seat;
12nd, bellows coupling;
13rd, closed loop stepper motor;
14th, stepper motor coding line interface;
15th, stepper motor power supply interface;
16th, nut I;
17th, pulling force sensor data line interface;
18th, nut II;
19th, fixed mount;
20th, electric machine support;
21st, support;
22nd, pulling force sensor data line interface;
23rd, stepper motor coding line interface;
24th, stepper motor power supply interface;
25th, total power switch;
26th, display control region;
27th, USB data line interface.
Embodiment
Following non-limiting examples can make one of ordinary skill in the art that the utility model is more fully understood, but The utility model is not limited in any way.
As depicted in figs. 1 and 2, the light microscope tensilometer of the present utility model adapted on light microscope, it is wrapped Include sample stationary fixture, fixed mount, pulling force sensor, drive mechanism and biaxial tension mechanism;The sample stationary fixture is by sample Product stationary fixture I and sample stationary fixture II are constituted;The biaxial tension mechanism includes driving section, the side plate II of side plate I;It is described to drive Motivation structure connects the driving section, drives the side plate I and side plate II to do the displacement movement of opposite direction;The sample geometrical clamp Tool I is fixedly connected with the side plate I, and the sample stationary fixture II is fixedly connected with the pulling force sensor, and the pulling force is passed Sensor is fixedly connected with the side plate II.
The sample stationary fixture I has upper grip and lower chuck, and the upper grip and lower chuck are by tightening fastening spiral shell Silk clamps sample.When tightening fastening screw, fastening screw can drive direction of the upper grip along fastening screw to do under The axial movement of chuck, plays a part of clamping sample.The clamping face of the upper grip and the clamping face of lower chuck are adapted, shape Into with the clamping face of clamped sample contacts be V-arrangement, circular arc or trapezoidal sample stationary fixture.The folder of upper grip and lower chuck Hold and be respectively equipped with face tooth line, improve the fixed effect of stretching sample.
The drive mechanism includes closed loop stepper motor, bellows coupling;The driving section includes nut I, nut II and left-right rotary screw rod, nut I and nut II are connected with left-right rotary screw rod by the way of threaded connection;The closed loop stepping The output end of motor is fixedly connected with bellows coupling, bellows coupling and motor linkage, the bellows coupling with The left-right rotary screw rod is fixedly connected, and left-right rotary screw rod can be driven to rotate;The lower chuck and nut I of the sample stationary fixture I On the facade for being fixedly connected on side plate I, the sample stationary fixture II is fixed on the vertical of the side plate II by pulling force sensor On face, i.e., one end of described pulling force sensor is fixedly connected on sample stationary fixture II, and the other end is fixedly connected on side plate II, surveys The tensile strength of test agent.The same pulling force sensor can be fixedly connected between sample stationary fixture I and side plate I.
As shown in Fig. 2 described light microscope tensilometer, also including support base, fixed seat, polished rod, fixed mount and branch Frame;The polished rod wears the even support base, fixed seat, is slidably connected with side plate I and side plate II;The left-right rotary screw rod passes through institute Support base and fixed seat is stated to be fixedly connected with the bellows coupling;The support base, fixed seat and drive mechanism are fixed and set Put on fixed mount;The support is square set, and the fixed mount setting is on the bracket.
A series of light microscopes that light microscope tensilometer described in the utility model can be adapted in laboratory, behaviour Facilitate, without being modified to light microscope, in use, to good position, it is horizontal forward to stretch portable microscope Below the camera lens of instrument push-in light microscope, sample is set to be in the field of view of optical microphotograph lens head.
When being detected using light microscope tensilometer described in the utility model:One end of tensile sample is fixed on sample Product stationary fixture I, the other end is fixed on sample stationary fixture II, drives closed loop stepper motor, and stepper motor rotates, ripple Line pipe shaft coupling starts rotation, drives the left-right rotary screw rod for being secured to connection to rotate, this can drive and left-right rotary screw rod spiral shell again Two nuts of line connection are equidistantly moved to relative to opposite direction constant speed respectively, and nut drives two side plates and two samples to consolidate Clamp has also to relative opposite direction constant speed equidistance motion, so that tensile sample is elongated, and sample center keeps constant.
As shown in figure 3, light microscope tensilometer described in the utility model, controllable also including step motor control case The rotating speed of stepper motor processed, rotating cycle, so that the draw speed and stretching distance of Control Assay, so draw speed, stretching The parameters such as displacement, incipient extension length can be according to the situation flexible modulation of sample.Tension test terminate after by control The program setting of device can realize the returning quickly of stretching device.Built-in data collecting card can real-time high-precision high frequency in control cabinet The analog signal of the collection S type pulling force sensors of rate, is converted into data signal, then imported into electricity by USB data line On brain, processing and analysis are acquired to test data by softwares such as Labview conventional in engineering on computers.In Fig. 3 The pulling force sensor data line interface indicated is connected with the pulling force sensor data line interface in Fig. 2, stepper motor line of codes Interface is connected with the stepper motor coding line interface in Fig. 2, stepper motor power supply interface and the stepper motor power supply interface in Fig. 2 It is connected, display control region is that the USB data line interface in the guidance panel of controllor for step-by-step motor, figure can even on computers The data of the pulling force sensor collected for output data capture card.
Fig. 4 is schematic diagram when the utility model tensilometer is used for laser confocal microscope, and Fig. 5 draws for the utility model The schematic diagram for stretching instrument when being used for ordinary optical microscope.Such as Fig. 4 and Fig. 5, when using portable microscope tensilometer, only need by It is pushed into below micro- lens head and adjusted, and sample center is just placed in below microscopical camera lens.It is applied to The operating method in Fig. 4 and Fig. 5 is can refer to during other microscopes.

Claims (6)

1. a kind of sample stationary fixture on light microscope tensilometer, it is characterised in that itself and sample clamped by sample The clamping face of contact is V-arrangement, circular arc or trapezoidal.
2. sample stationary fixture according to claim 1, it is characterised in that the sample stationary fixture include upper grip and Lower chuck, the upper grip and lower chuck clamp sample by tightening fastening screw.
3. sample stationary fixture according to claim 2, it is characterised in that the sample clamping of the upper grip and lower chuck Tooth line is respectively equipped with face.
4. a kind of light microscope tensilometer adapted on light microscope, it includes fixed mount, pulling force sensor, driving machine Sample stationary fixture described in any one of structure and biaxial tension mechanism and claims 1 to 3;
The sample stationary fixture is made up of sample stationary fixture I and sample stationary fixture II;
The biaxial tension mechanism includes driving section, side plate I and side plate II;
The drive mechanism connects the driving section, drives the side plate I and side plate II to do the displacement movement of opposite direction;
The sample stationary fixture I is fixedly connected with the side plate I, and the sample stationary fixture II is fixed with the side plate II to be connected Connect, the pulling force sensor be fixedly connected between sample stationary fixture I and side plate I or sample stationary fixture II and side plate II it Between.
5. light microscope tensilometer according to claim 4, it is characterised in that
The drive mechanism includes closed loop stepper motor, bellows coupling;
The driving section includes nut I, nut II and left-right rotary screw rod, and nut I and nut II are connected with left-right rotary screw rod with screw thread The mode connect is connected;
The closed loop stepper motor is fixedly connected with the left-right rotary screw rod by bellows coupling;
The sample stationary fixture I is fixedly connected nut I by side plate I, and the sample stationary fixture II is fixed by side plate II Attaching nut II.
6. light microscope tensilometer according to claim 5, it is characterised in that
The tensilometer also includes support base, fixed seat, polished rod, fixed mount and support;
The polished rod wears the even support base, fixed seat, is slidably connected with side plate I and side plate II;
The left-right rotary screw rod is fixedly connected through the support base and fixed seat with the bellows coupling;
The support base, fixed seat and drive mechanism are fixedly installed on fixed mount;
The support is square set, and the fixed mount setting is on the bracket.
CN201621293167.2U 2016-11-29 2016-11-29 A kind of microscope tensilometer adapted on light microscope Expired - Fee Related CN206330835U (en)

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Publication Number Publication Date
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107687991A (en) * 2017-09-07 2018-02-13 国家纳米科学中心 A kind of test method of the device for simulating small bowel peristalsis and Nano medication diffusion
CN109883839A (en) * 2019-03-28 2019-06-14 广东工业大学 A kind of stretcher of material sample and system for infrared spectrum analysis
CN110618048A (en) * 2019-09-23 2019-12-27 武汉大学 Bellows simulation fatigue test device and test method thereof
CN113049362A (en) * 2021-03-18 2021-06-29 凯尔测控试验系统(天津)有限公司 Miniature in-situ biaxial mechanical testing machine for confocal microscope

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107687991A (en) * 2017-09-07 2018-02-13 国家纳米科学中心 A kind of test method of the device for simulating small bowel peristalsis and Nano medication diffusion
CN107687991B (en) * 2017-09-07 2020-10-16 国家纳米科学中心 Device for simulating small intestine peristalsis and test method for nano-drug diffusion
CN109883839A (en) * 2019-03-28 2019-06-14 广东工业大学 A kind of stretcher of material sample and system for infrared spectrum analysis
CN109883839B (en) * 2019-03-28 2022-04-19 广东工业大学 Material sample stretching device and system for infrared spectroscopy
CN110618048A (en) * 2019-09-23 2019-12-27 武汉大学 Bellows simulation fatigue test device and test method thereof
CN110618048B (en) * 2019-09-23 2020-12-29 武汉大学 Bellows simulation fatigue test device and test method thereof
CN113049362A (en) * 2021-03-18 2021-06-29 凯尔测控试验系统(天津)有限公司 Miniature in-situ biaxial mechanical testing machine for confocal microscope

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Granted publication date: 20170714