CN206240488U - Initiation material reactor is used in a kind of doxepin hydrochloride production - Google Patents
Initiation material reactor is used in a kind of doxepin hydrochloride production Download PDFInfo
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- CN206240488U CN206240488U CN201621337401.7U CN201621337401U CN206240488U CN 206240488 U CN206240488 U CN 206240488U CN 201621337401 U CN201621337401 U CN 201621337401U CN 206240488 U CN206240488 U CN 206240488U
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- reaction chamber
- initiation material
- rotating shaft
- chuck
- stirring vane
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model is related to a kind of reactor, more particularly to a kind of production of doxepin hydrochloride to use initiation material reactor.The technical problems to be solved in the utility model is to provide that a kind of reaction speed is fast, react uniform doxepin hydrochloride production initiation material reactor.In order to solve the above-mentioned technical problem, the utility model provides the production of such a doxepin hydrochloride and uses initiation material reactor, includes chuck, ear mount, steam inlet, condensation-water drain, reaction chamber, discharge nozzle, first bearing seat, first rotating shaft, the first stirring vane, first bevel gear etc.；Jackets outer wall is symmetrical to be provided with ear mount, and reaction chamber is provided with chuck, and chuck top is symmetrical to be provided with steam inlet, and chuck bottom is symmetrical to be provided with condensation-water drain.The utility model is rotated by controlling electric rotating machine, drives the first stirring vane and the rotation of the second stirring vane so that initiation material Quick uniform mixes, while injecting steam by steam inlet, reaction chamber is heated.
Description
Technical field
The utility model is related to a kind of reactor, more particularly to a kind of production of doxepin hydrochloride to use initiation material reactor.
Background technology
Doxepin hydrochloride, preparation：Doxepin hydrochloride piece is coating tablet, removes whitening color after being coated.For treating depression
And anxiety neurosis.
Reactor is widely used in oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrifying,
The pressure vessel of the technical process such as hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.；Material
Matter typically has carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan, Monel, inconel) alloy and other composites.Reactor
The rustless steel container for having and physically or chemically reacting is broadly understood, is set according to the structure that different process conditions demands carries out container
Meter and parameter configuration, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards, to realize technological requirement
The mixture response function of heating, evaporation, cooling and low high speed.
, it is necessary to be closed to the initiation material of doxepin hydrochloride using to reactor in the production technology of doxepin hydrochloride
Into reaction, initiation material being stirred can accelerate reaction speed during the course of the reaction, and current reactor has reaction speed
Degree is slow, react uneven shortcoming, therefore needs that a kind of reaction speed of research and development is fast, react uniform doxepin hydrochloride production uses badly
Beginning raw material reaction kettle.
Utility model content
(1) technical problem to be solved
The utility model haves the shortcomings that reaction speed is slow, react uneven, this practicality to overcome current reactor
The new technical problem to be solved is to provide that a kind of reaction speed is fast, it is anti-to react uniform doxepin hydrochloride production initiation material
Answer kettle.
(2) technical scheme
In order to solve the above-mentioned technical problem, the utility model provides such a doxepin hydrochloride production initiation material
Reactor, include chuck, ear mount, steam inlet, condensation-water drain, reaction chamber, discharge nozzle, first bearing seat, first rotating shaft,
First stirring vane, first bevel gear, second bevel gear, flange, second bearing seat, case lid, hand hole, visor, feed pipe, temperature
Meter mouth, frame, electric rotating machine, the second rotating shaft and the second stirring vane, jackets outer wall is symmetrical to be provided with ear mount, is provided with chuck
Reaction chamber, chuck top is symmetrical to be provided with steam inlet, and chuck bottom is symmetrical to be provided with condensation-water drain, reaction chamber bottom
Be provided with discharge nozzle, reaction chamber inner wall lower is respectively arranged on the left side and the right side first bearing seat and second bearing seat, first bearing seat and
Interference is connected with first rotating shaft between bearing in second bearing seat, symmetrical in first rotating shaft to be connected with the first paddle
Piece, first rotating shaft left part is connected with first bevel gear by way of being bonded and connecing, and reaction chamber top is connected with case lid by flange,
Case lid upper left side is provided with hand hole, and hand hole is provided with visor, and case lid top center is provided with frame, and frame top is provided with electric rotating machine,
The second rotating shaft is connected with by shaft coupling on the output shaft of electric rotating machine, the second rotating shaft is provided with the second stirring vane, and second stirs
Blade is mixed in the reaction chamber, the second rotating shaft bottom is connected with second bevel gear by way of being bonded and connecing, second bevel gear with
First bevel gear is connected, and case lid right side is provided with feed pipe and thermometer mouthful, and thermometer mouthful is located at feed pipe right side.
Preferably, it is provided with aperture on the first stirring vane and the second stirring vane.
Preferably, swash plate is also included, reaction chamber inner bottom part is provided with swash plate.
Preferably, filter screen is also included, filter screen is provided with feed pipe.
Preferably, electric rotating machine is servomotor.
Preferably, the material of reaction chamber is stainless steel.
Operation principle：When workman needs to carry out synthetic reaction to the initiation material of doxepin hydrochloride, workman pass through first into
Expects pipe injects in reaction chamber initiation material, and workman is observed by visor, it was observed that in reaction chamber during saturation, workman stops
Injection initiation material.Then workman's control electric rotating machine rotation, drives the second rotating shaft rotation, on the one hand, the second rotating shaft drives the
Two stirring vanes rotate, and on the other hand, the second rotating shaft drives second bevel gear rotation, and then second bevel gear drives first to bore tooth
Wheel rotation, first bevel gear drives first rotating shaft rotation, and first rotating shaft drives the rotation of the first stirring vane, so repeatedly, first
Stirring vane and the second stirring vane are constantly rotated, and initiation material is stirred, and make it quick well mixed.At the same time,
Workman is by steam by the cavity between steam inlet injection chuck and reaction chamber so that steam is heated to reaction chamber,
Reaction temperature is improved, reaction speed is further speeded up, the steam after cooling becomes condensed water, flowed out by condensation-water drain.Work
Thermometer is stretched into measurement temperature in reaction chamber, convenient regulation reaction temperature by people by thermometer mouthful.When initiation material has reacted
Bi Hou, workman's control electric rotating machine stops the rotation, while stopping injection steam, the initiation material that the reaction in reaction chamber is completed leads to
Cross discharge nozzle outflow.When staff needs to overhaul reactor, hand hole can be opened, facilitate the inspection inside reaction chamber
Repair.
Because being provided with aperture on the first stirring vane and the second stirring vane, in the first stirring vane and the second paddle
When piece rotates, initiation material can mix evenly quickly through aperture.
Because also including swash plate, reaction chamber inner bottom part is provided with swash plate so that reaction complete initiation material quickly through
Discharge nozzle flows out.
Because also including filter screen, filter screen is provided with feed pipe, prevents solid impurity from entering in reaction chamber.
Because electric rotating machine is servomotor, servomotor can preferably control its rotating speed, make device effective more steady.
Because the material of reaction chamber is stainless steel, stainless steel is corrosion-resistant, effectively extends the service life of reaction chamber.
(3) beneficial effect
The utility model is rotated by controlling electric rotating machine, drives the first stirring vane and the rotation of the second stirring vane, is made
The mixing of initiation material Quick uniform is obtained, while injecting steam by steam inlet, reaction chamber is heated, regulation reaction is warm
Degree, has reached that reaction speed is fast, react uniform effect.
Brief description of the drawings
Fig. 1 is the first main structure diagram of the present utility model.
Fig. 2 is second main structure diagram of the present utility model.
Fig. 3 is the third main structure diagram of the present utility model.
Fig. 4 is the 4th kind of main structure diagram of the present utility model.
Mark in accompanying drawing for：1- chucks, 2- ear mounts, 3- steam inlets, 4- condensation-water drains, 5- reaction chambers,
6- discharge nozzles, 7- first bearing seats, 8- first rotating shafts, the stirring vanes of 9- first, 10- first bevel gears, 11- second is bored
Gear, 12- flanges, 13- second bearing seats, 14- case lids, 15- hand holes, 16- visors, 17- feed pipes, 18- thermometers
Mouthful, 19- frames, 20- electric rotating machines, the rotating shafts of 21- second, the stirring vanes of 22- second, 23- apertures, 24- swash plates, 25-
Filter screen.
Specific embodiment
The utility model is further described with reference to the accompanying drawings and examples.
Embodiment 1
Initiation material reactor is used in a kind of doxepin hydrochloride production, as Figure 1-4, is included chuck 1, ear mount 2, is steamed
Vapor inlet 3, condensation-water drain 4, reaction chamber 5, discharge nozzle 6, first bearing seat 7, first rotating shaft 8, the first stirring vane 9, first
Bevel gear 10, second bevel gear 11, flange 12, second bearing seat 13, case lid 14, hand hole 15, visor 16, feed pipe 17, temperature
Meter mouth 18, frame 19, electric rotating machine 20, the second rotating shaft 21 and the second stirring vane 22, the outer wall of chuck 1 is symmetrical to be provided with ear mount
2, reaction chamber 5 is provided with chuck 1, the top of chuck 1 is symmetrical to be provided with steam inlet 3, and the bottom of chuck 1 is symmetrical to be provided with condensation
Water out 4, the bottom of reaction chamber 5 is provided with discharge nozzle 6, and the inner wall lower of reaction chamber 5 is respectively arranged on the left side and the right side first bearing seat 7 and
Two bearing bracket 13, interference is connected with first rotating shaft 8, first rotating shaft 8 between the bearing in first bearing seat 7 and second bearing seat 13
Above symmetrical to be connected with the first stirring vane 9, the left part of first rotating shaft 8 is connected with first bevel gear by way of being bonded and connecing
10, the top of reaction chamber 5 is connected with case lid 14 by flange 12, and the upper left side of case lid 14 is provided with hand hole 15, and hand hole 15 is provided with visor
16, the top center of case lid 14 is provided with frame 19, and the top of frame 19 is provided with electric rotating machine 20, passes through on the output shaft of electric rotating machine 20
Shaft coupling is connected with the second rotating shaft 21, and the second rotating shaft 21 is provided with the second stirring vane 22, and the second stirring vane 22 is located at reaction
In case 5, the bottom of the second rotating shaft 21 is connected with second bevel gear 11, the cone tooth of second bevel gear 11 and first by way of being bonded and connecing
Wheel 10 is connected, and the right side of case lid 14 is provided with feed pipe 17 and thermometer mouthful 18, and thermometer mouthful 18 is located at the right side of feed pipe 17.
Aperture 23 is provided with first stirring vane 9 and the second stirring vane 22.
Swash plate 24 is also included, the inner bottom part of reaction chamber 5 is provided with swash plate 24.
Also include in filter screen 25, feed pipe 17 and be provided with filter screen 25.
Electric rotating machine 20 is servomotor.
The material of reaction chamber 5 is stainless steel.
Operation principle：When workman needs to carry out synthetic reaction to the initiation material of doxepin hydrochloride, workman pass through first into
Expects pipe 17 injects in reaction chamber 5 initiation material, and workman is observed by visor 16, it was observed that in reaction chamber 5 during saturation, work
People stops injection initiation material.Then workman's control electric rotating machine 20 rotates, and drives the second rotating shaft 21 to rotate, on the one hand, second
Rotating shaft 21 drives the second stirring vane 22 to rotate, and on the other hand, the second rotating shaft 21 drives second bevel gear 11 to rotate, and then second
Bevel gear 11 drives first bevel gear 10 to rotate, and first bevel gear 10 drives first rotating shaft 8 to rotate, and first rotating shaft 8 drives first
Stirring vane 9 is rotated, and so repeatedly, the first stirring vane 9 and the second stirring vane 22 are constantly rotated, and initiation material is stirred
Mix, make it quick well mixed.At the same time, workman injects between chuck 1 and reaction chamber 5 steam by steam inlet 3
In cavity so that steam is heated to reaction chamber 5, reaction temperature is improved, further speed up reaction speed, the steam after cooling
Become condensed water, flowed out by condensation-water drain 4.Thermometer is stretched into measurement temperature in reaction chamber 5 by workman by thermometer mouthful 18
Degree, convenient regulation reaction temperature.When initiation material after completion of the reaction, workman control electric rotating machine 20 stop the rotation, while stop
Injection steam, the initiation material that the reaction in reaction chamber 5 is completed is flowed out by discharge nozzle 6.When staff is needed to reactor
When being overhauled, hand hole 15 can be opened, facilitate the maintenance inside reaction chamber 5.
Because being provided with aperture 23 on the first stirring vane 9 and the second stirring vane 22, in the first stirring vane 9 and second
When stirring vane 22 rotates, initiation material can mix evenly quickly through aperture 23.
Because also including swash plate 24, the inner bottom part of reaction chamber 5 is provided with swash plate 24 so that the initiation material that reaction is completed is quick
Flowed out by discharge nozzle 6.
Because also including filter screen 25, filter screen 25 is provided with feed pipe 17, prevents solid impurity from entering in reaction chamber 5.
Because electric rotating machine 20 is servomotor, servomotor can preferably control its rotating speed, make device effectively more flat
Surely.
Because the material of reaction chamber 5 is stainless steel, stainless steel is corrosion-resistant, effectively extends the service life of reaction chamber 5.
Embodiment described above only expresses preferred embodiment of the present utility model, and its description is more specific and detailed,
But therefore can not be interpreted as the limitation to the utility model the scope of the claims.It should be pointed out that common for this area
For technical staff, without departing from the inventive concept of the premise, some deformations, improvement can also be made and substituted, these are all
Belong to protection domain of the present utility model.Therefore, the protection domain of the utility model patent should be determined by the appended claims.
Claims (6)
1. initiation material reactor is used in a kind of doxepin hydrochloride production, it is characterised in that included chuck (1), ear mount (2), steamed
Vapor inlet (3), condensation-water drain (4), reaction chamber (5), discharge nozzle (6), first bearing seat (7), first rotating shaft (8), first stir
Mix blade (9), first bevel gear (10), second bevel gear (11), flange (12), second bearing seat (13), case lid (14), hand hole
(15), visor (16), feed pipe (17), thermometer mouthful (18), frame (19), electric rotating machine (20), the second rotating shaft (21) and the
Two stirring vanes (22), symmetrical being provided with ear mount (2), chuck (1) of chuck (1) outer wall is provided with reaction chamber (5), chuck (1)
Top is symmetrical to be provided with steam inlet (3), and chuck (1) bottom is symmetrical to be provided with condensation-water drain (4), reaction chamber (5) bottom
Portion is provided with discharge nozzle (6), and reaction chamber (5) inner wall lower is respectively arranged on the left side and the right side first bearing seat (7) and second bearing seat
(13), interference is connected with first rotating shaft (8), first rotating shaft between the bearing in first bearing seat (7) and second bearing seat (13)
(8) symmetrical on to be connected with the first stirring vane (9), first rotating shaft (8) left part is connected with first by way of being bonded and connecing
Bevel gear (10), reaction chamber (5) top is connected with case lid (14) by flange (12), and case lid (14) upper left side is provided with hand hole
(15), hand hole (15) is provided with visor (16), and case lid (14) top center is provided with frame (19), and frame (19) top is provided with rotation
Motor (20), the second rotating shaft (21) is connected with the output shaft of electric rotating machine (20) by shaft coupling, and the second rotating shaft sets on (21)
There is the second stirring vane (22), in reaction chamber (5), the second rotating shaft (21) bottom connects the second stirring vane (22) by being bonded
Mode be connected with second bevel gear (11), second bevel gear (11) is connected with first bevel gear (10), case lid (14) right side set
There are feed pipe (17) and thermometer mouthful (18), thermometer mouthful (18) is positioned at feed pipe (17) right side.
2. initiation material reactor is used in a kind of doxepin hydrochloride production according to claim 1, it is characterised in that first stirs
Mix and be provided with aperture (23) on blade (9) and the second stirring vane (22).
3. initiation material reactor is used in a kind of doxepin hydrochloride production according to claim 1, it is characterised in that also included
There is swash plate (24), reaction chamber (5) inner bottom part is provided with swash plate (24).
4. initiation material reactor is used in a kind of doxepin hydrochloride production according to claim 1, it is characterised in that also included
Have in filter screen (25), feed pipe (17) and be provided with filter screen (25).
5. initiation material reactor is used in a kind of doxepin hydrochloride production according to claim 1, it is characterised in that electric rotating
Machine (20) is servomotor.
6. initiation material reactor is used in a kind of doxepin hydrochloride production according to claim 1, it is characterised in that reaction chamber
(5) material is stainless steel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621337401.7U CN206240488U (en) | 2016-12-07 | 2016-12-07 | Initiation material reactor is used in a kind of doxepin hydrochloride production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621337401.7U CN206240488U (en) | 2016-12-07 | 2016-12-07 | Initiation material reactor is used in a kind of doxepin hydrochloride production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206240488U true CN206240488U (en) | 2017-06-13 |
Family
ID=59004808
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621337401.7U Expired - Fee Related CN206240488U (en) | 2016-12-07 | 2016-12-07 | Initiation material reactor is used in a kind of doxepin hydrochloride production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206240488U (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107224889A (en) * | 2017-07-21 | 2017-10-03 | 苏州长鸿机械设备有限公司 | A kind of sewage-treatment plant |
| CN107349815A (en) * | 2017-07-21 | 2017-11-17 | 深圳荣行智能科技有限公司 | A kind of environmental protection coating material device |
| CN107970122A (en) * | 2017-12-31 | 2018-05-01 | 梁楠 | A kind of steam pressurization type Fang Nian Di is decocted medicinal herbs device |
| CN107970123A (en) * | 2017-12-31 | 2018-05-01 | 梁楠 | A kind of steam agitating type is decocted medicinal herbs device |
| CN107998935A (en) * | 2017-07-21 | 2018-05-08 | 广州峥航机械设备有限公司 | A kind of new type environment friendly coating device |
| CN107998912A (en) * | 2017-07-21 | 2018-05-08 | 广州峥航机械设备有限公司 | A kind of improved environment protection application device |
| CN108097082A (en) * | 2017-12-05 | 2018-06-01 | 芜湖市诺康生物科技有限公司 | A kind ofization glue tank |
| CN108479664A (en) * | 2018-04-04 | 2018-09-04 | 陈洁 | A kind of chemical industry reaction kettle |
| CN109908782A (en) * | 2019-03-27 | 2019-06-21 | 江苏金山啤酒原料有限公司 | A kind of agitating device of material production |
| CN112516853A (en) * | 2019-10-25 | 2021-03-19 | 江西农业大学 | Modifier mixing apparatus is used in improvement of tea-oil camellia forest acid soil |
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2016
- 2016-12-07 CN CN201621337401.7U patent/CN206240488U/en not_active Expired - Fee Related
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107224889A (en) * | 2017-07-21 | 2017-10-03 | 苏州长鸿机械设备有限公司 | A kind of sewage-treatment plant |
| CN107349815A (en) * | 2017-07-21 | 2017-11-17 | 深圳荣行智能科技有限公司 | A kind of environmental protection coating material device |
| CN107998935A (en) * | 2017-07-21 | 2018-05-08 | 广州峥航机械设备有限公司 | A kind of new type environment friendly coating device |
| CN107998912A (en) * | 2017-07-21 | 2018-05-08 | 广州峥航机械设备有限公司 | A kind of improved environment protection application device |
| CN107224889B (en) * | 2017-07-21 | 2018-07-17 | 山东东环环境科技股份有限公司 | A kind of sewage-treatment plant |
| CN108097082A (en) * | 2017-12-05 | 2018-06-01 | 芜湖市诺康生物科技有限公司 | A kind ofization glue tank |
| CN107970122A (en) * | 2017-12-31 | 2018-05-01 | 梁楠 | A kind of steam pressurization type Fang Nian Di is decocted medicinal herbs device |
| CN107970123A (en) * | 2017-12-31 | 2018-05-01 | 梁楠 | A kind of steam agitating type is decocted medicinal herbs device |
| CN108479664A (en) * | 2018-04-04 | 2018-09-04 | 陈洁 | A kind of chemical industry reaction kettle |
| CN109908782A (en) * | 2019-03-27 | 2019-06-21 | 江苏金山啤酒原料有限公司 | A kind of agitating device of material production |
| CN112516853A (en) * | 2019-10-25 | 2021-03-19 | 江西农业大学 | Modifier mixing apparatus is used in improvement of tea-oil camellia forest acid soil |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170613 Termination date: 20191207 |