CN206168387U - Integrated form solid catalyst activating treatment reactor - Google Patents
Integrated form solid catalyst activating treatment reactor Download PDFInfo
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- CN206168387U CN206168387U CN201621149879.7U CN201621149879U CN206168387U CN 206168387 U CN206168387 U CN 206168387U CN 201621149879 U CN201621149879 U CN 201621149879U CN 206168387 U CN206168387 U CN 206168387U
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- solid catalyst
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- form solid
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Abstract
The utility model provides an integrated form solid catalyst activating treatment reactor mainly includes retort main part and supporting agitator, and operations such as the activation that can relate to solid catalyst activating treatment in -process, washing, filtration integrate and go on. Adopt the filter structure of the supporting retort low head of the nearly wall type stirring rake of lower floor, in filter process, can prevent effectively that solid catalyst from carrying out the deposit and stopping up the filtration pore by a wide margin on the filter screen for filter speed. The utility model discloses an integrated form solid catalyst activating treatment reactor can save equipment input by a wide margin, the simplified operation process, and the operation is high -efficient convenient.
Description
Technical field
This utility model is related to activation of catalyst, reuse field, at more particularly to a kind of integrated form solid catalyst activation
Reason reactor.
Background technology
According to statistics, more than 80% reaction is there are about in modern chemical industry production process needs corresponding catalyst, such as
Petrochemical industry, fine chemistry industry, biochemistry, environmental protection etc..With the development of modern chemical industry, the species and usage amount of catalyst have very fast growth
Trend.
Used in chemical reaction process after the regular hour, the active component on catalyst can be due to overheated burning for catalyst
Knot, pollutant cover, poisonous substance infringement etc. reason cause its activity decrease, even inactivate, due to the commercial value of catalyst it is very high,
If directly abandoned decaying catalyst, larger economic loss and the wasting of resources can be caused, while also bringing to ecological environment
Certain pressure.Therefore, the correlation technique of activation of catalyst reuse is also greatly paid close attention to and is deeply developed.Fraction solids are urged
After agent is inactivated during the course of the reaction, activation processing can be carried out by adding treatment fluid, then through cleaning, filtration, dry etc.
Sequence of maneuvers is regenerated reuse.General operation thinking and method is that catalyst carries out activation processing in retort, activation
Afterwards recovered material imports filter and is filtered, and returns in retort after filtration and is cleaned, then imports filter filtration,
Finally it is dried.It is cumbersome but this kind of technical scheme needs to be switched repeatedly between plurality of devices, it is less efficient.
For the deficiency of existing solid catalyst activation processing technology, the utility model proposes a kind of integration type is solid
Body catalyst activation processing reactor and its related work mode.
Utility model content
The purpose of this utility model is to provide one kind and can realize that solid catalyst is efficiently activated, cleaned, filtering etc. to grasp
The integrated form solid catalyst activation processing reactor of work.
Adopted the technical scheme that for achieving the above object：
A kind of integrated form solid catalyst activation processing reactor, it is characterised in that the integrated form solid catalyst is lived
Changing treatment reactor mainly includes reaction can body and supporting agitator；
The upper cover of the reaction kettle body of the reaction can body is provided with solid material entrance, liquid material entrance, nitrogen pressurization mouth, aerofluxuss
Mouthful；The straight tube shell ring outside of the reaction kettle body of the reaction can body carries heating jacket A, and the heating jacket A is provided with and adds
Thermal medium inlet A and Crude product input A, are equipped with thermometer on the straight tube shell ring, the inwall of the straight tube shell ring is equipped with gear
Plate；The low head of the reaction kettle body of the reaction can body is taper, and the outside of the low head carries heating jacket B, described
Heating jacket B is provided with plus thermal medium inlet B and Crude product input B, and the inside of the low head is equipped with drainage screen, it is described under
End socket is provided with liquid material outlet, and the bottom of the low head is provided with solid material floss hole, equipped with bottom valve；
The supporting agitator includes motor, reductor, shaft coupling, axle envelope, frame, shaft, stirring paddle.
Thermometer can be monitored to the temperature of kettle in-vivo medium.Low head is taper, is conducive to the discharge of solid material.
The liquid material outlet of low head, the discharge and cleaning for terminating aftertreatment fluid for priming reaction terminates the discharge of rear cleanout fluid.Under
The solid material floss hole of end socket, for solid catalyst to be drained into into finished product after the operation such as priming reaction, cleaning, filtration terminates
Tank.
The drainage screen is wedge shaped filter net or sintered metal mesh, the chi of the precision of the drainage screen according to solid catalyst
Little progress row is selected.
The stirring paddle is at least two-layer, and depending on the straight tube shell ring draw ratio more than three layers are added to.The stirring paddle it is upper
Which floor is axial flow pattern stirring pattern, such as propeller-type, air foil profile；The bottom of the stirring paddle is straight blade profile stirring pattern, such as
Leafy to upwarp straight oar, blade upwarps cone angle of the angle corresponding to the low head, and the lower limb of blade ensureing parts not
Under conditions of interference with the inner surface of the drainage screen close proximity to.Be conducive to expecting to be difficult admittedly when discharging treatment fluid and cleanout fluid
Deposited thereon is filtered, accelerates the velocity of discharge.
The beneficial effects of the utility model are：
1st, the operation such as the activation being related in solid catalyst activated process, cleaning, filtration is integrated in into this practicality new
Carry out in type, save equipment investment, simplify operation sequence, operation is efficiently convenient；
2nd, the filter screen structure using nearly wall type stirring paddle and retort low head is supporting, effectively anti-in filter process
Only solid catalyst is deposited on drainage screen and is significantly blocked filter opening, accelerates the rate of filtration.
Description of the drawings
Fig. 1 is front view of the present utility model；
Reference：
1 reaction can body
1-1 reaction kettle bodies 1-2 expects entrance 1-3 liquid material entrance 1-4 nitrogen pressurization mouth 1-5 air vents 1-6 heating folders admittedly
Set A 1-7 add thermal medium inlet A 1-8 Crude product inputs A 1-9 thermometer 1-10 heating jacket B 1-11 plus thermal medium to enter
Mouth B 1-12 Crude product input B 1-13 drainage screen 1-14 liquid material outlet 1-15 expect floss hole 1-16 baffle plates admittedly；
2 supporting agitators
2-1 motor 2-2 reductor 2-3 shaft coupling 2-4 axle envelope 2-5 frame 2-6 shaft 2-7 upper stratas stirring paddle
2-8 middle levels stirring paddle 2-9 bottom stirring paddles.
Specific embodiment
This utility model is described in further details below in conjunction with the accompanying drawings.
In Fig. 1, a kind of integrated form solid catalyst activation processing reactor mainly includes reaction can body 1 and supporting stirring
Device 2.
The upper cover of the reaction kettle body 1-1 of reaction can body 1 is provided with solid material entrance 1-2, liquid material entrance 1-3, nitrogen pressurization
Mouth 1-4, air vent 1-5 etc.；
The straight tube shell ring outside of the reaction kettle body 1-1 of reaction can body 1 carries heating jacket A1-6, on heating jacket A1-6
It is provided with plus thermal medium inlet A1-7 and Crude product input A1-8, while thermometer 1-9 is housed on straight tube shell ring, straight tube shell ring
Inwall is equipped with baffle plate 1-16；
The low head of the reaction kettle body 1-1 of reaction can body 1 is taper；The outside of low head carries heating jacket B1-10,
Heating jacket B1-10 is provided with plus thermal medium inlet B1-11 and Crude product input B1-12；The inside of low head is equipped with filtration
Net 1-13, drainage screen 1-13 can select sintered metal mesh, the size of the supporting solid catalyst of precision of sintered meshwork；Low head is provided with
Liquid material exports 1-14；The bottom of low head is provided with solid material floss hole 1-15.
Supporting agitator include motor 2-1, reductor 2-2, shaft coupling 2-3, axle envelope 2-4, frame 2-5, shaft 2-6,
Stirring paddle 2-7~2-9.Stirring paddle has three layers, and upper strata stirring paddle 2-7 and middle level stirring paddle 2-8 adopt axial-flow mixing paddle；Bottom
Using upwarping the straight oar of two leaves, blade upwarps that angle is consistent with the cone angle of low head to stirring paddle 2-9, the lower limb of blade and lower envelope
Head drainage screen inner surface close proximity to.
A kind of working method of solid catalyst activation processing reactor of the present utility model is as follows：
During activation processing, respectively by solid catalyst to be activated from solid catalyst entrance 1-2, activation processing liquid from liquid material
Entrance 1-3 add reaction can body 1 reaction kettle body 1-1 in, start agitator 2, while by plus thermal medium inlet A1-7, heating
Medium entrance B1-11 and Crude product input A1-8, Crude product input B1-12 are passed through plus thermal medium is circulated heating；Treat
Temperature is reached after technique assigned temperature, carries out priming reaction.After priming reaction terminates, solid material filtration is carried out, open liquid material outlet
1-14, treatment fluid is flowed out by liquid material outlet 1-14, and solid catalyst is then trapped in be cleaned in reaction kettle body by drainage screen 1-13
Process.
During cleaning, cleanout fluid is added from liquid material entrance 1-3, cleanout fluid and solid catalysis are promoted by supporting agitator 2
Agent is fully contacted, and technological temperature is ensured by chuck circulating-heating.After cleaning terminates, solid material filtration is carried out, open liquid material outlet 1-
14, cleanout fluid is flowed out by liquid material outlet 1-14, and solid catalyst is trapped in reaction kettle body by drainage screen 1-13.Wash liquid stream
Finish, open the bottom valve for expecting floss hole 1-15 admittedly, solid catalyst is drained into into finished pot.If occurred in discharge process slight
The excessively slow phenomenon of blocking or mass rate of emission, can add nitrogen to carry out supercharging in kettle by nitrogen pressurization mouth 1-4, to be discharged to finish
Afterwards, overbottom pressure can be drained by air vent 1-5 in kettle.
This utility model be directed to the deficiencies in the prior art, can by the activation being related in solid catalyst activated process,
Cleaning, filter etc. that operation is integrated to be carried out, it is efficiently convenient, save equipment investment and artificial running cost.
Specific embodiment utilized above is anti-to a kind of integrated form solid catalyst activation processing provided by the utility model
Answer device to be described in detail, elaborate principle of the present utility model and embodiment, the explanation of the embodiment is only intended to
Help understands the principle and core concept of utility model.It should be pointed out that for those skilled in the art,
On the premise of without departing from this utility model principle, some improvement and modification can also be carried out to this utility model, these improve and
Modification is also fallen in this utility model scope of the claims.
Claims (5)
1. a kind of integrated form solid catalyst activation processing reactor, it is characterised in that the integrated form solid catalyst activation
Treatment reactor mainly includes reaction can body and supporting agitator；
The upper cover of the reaction kettle body of the reaction can body is provided with solid material entrance, liquid material entrance, nitrogen pressurization mouth, air vent；
The straight tube shell ring outside of the reaction kettle body of the reaction can body carries heating jacket A, and the heating jacket A is provided with heating and is situated between
Matter import A and Crude product input A, is equipped with thermometer on the straight tube shell ring, the inwall of the straight tube shell ring is equipped with baffle plate；Institute
The low head for stating the reaction kettle body of reaction can body is taper, and the outside of the low head carries heating jacket B, the heating folder
Set B is provided with plus thermal medium inlet B and Crude product input B, and the inside of the low head is equipped with drainage screen, and the low head sets
There is liquid material to export, the bottom of the low head is provided with solid material floss hole, equipped with bottom valve；
The supporting agitator includes motor, reductor, shaft coupling, axle envelope, frame, shaft, stirring paddle.
2. a kind of integrated form solid catalyst activation processing reactor according to claim 1, it is characterised in that the mistake
Filter screen is wedge shaped filter net or sintered metal mesh, and the precision of the drainage screen is selected according to the size of solid catalyst.
3. a kind of integrated form solid catalyst activation processing reactor according to claim 1, it is characterised in that described to stir
Mix oar and be at least two-layer, depending on the straight tube shell ring draw ratio more than three layers are added to.
4. a kind of integrated form solid catalyst activation processing reactor according to claim 3, it is characterised in that described to stir
Mix oar it is upper which floor be axial flow pattern stirring pattern, the bottom of the stirring paddle is straight blade profile stirring pattern.
5. a kind of integrated form solid catalyst activation processing reactor according to claim 4, it is characterised in that described to stir
Mix oar it is upper which floor be propeller-type, air foil profile；The bottom of the stirring paddle upwarps straight oar for leafy, and blade upwarps angle pair
The cone angle of low head described in Ying Yu, the lower limb of blade is ensureing the interior table under conditions of parts are not interfered with the drainage screen
Face close proximity to.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621149879.7U CN206168387U (en) | 2016-10-24 | 2016-10-24 | Integrated form solid catalyst activating treatment reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621149879.7U CN206168387U (en) | 2016-10-24 | 2016-10-24 | Integrated form solid catalyst activating treatment reactor |
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| Publication Number | Publication Date |
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| CN206168387U true CN206168387U (en) | 2017-05-17 |
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| CN201621149879.7U Active CN206168387U (en) | 2016-10-24 | 2016-10-24 | Integrated form solid catalyst activating treatment reactor |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108745254A (en) * | 2018-08-06 | 2018-11-06 | 江苏兆辉防腐科技有限公司 | A kind of steel lining tetrafluoro reactor |
| CN110997123A (en) * | 2017-08-04 | 2020-04-10 | 夏尔人类遗传性治疗公司 | Antibody-resin coupling apparatus and method |
| CN111268884A (en) * | 2020-03-31 | 2020-06-12 | 浙江科茂环境科技有限公司 | Oil sludge treatment system and method |
| CN113832510A (en) * | 2021-09-09 | 2021-12-24 | 张家口原轼新型材料有限公司 | Steel grit with high-phosphorus nickel alloy plated on surface, plating solution, plating process, plating device and steel wire containing steel grit |
-
2016
- 2016-10-24 CN CN201621149879.7U patent/CN206168387U/en active Active
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110997123A (en) * | 2017-08-04 | 2020-04-10 | 夏尔人类遗传性治疗公司 | Antibody-resin coupling apparatus and method |
| US11969703B2 (en) | 2017-08-04 | 2024-04-30 | Takeda Pharmaceutical Company Limited | Antibody-resin coupling apparatus and methods |
| CN108745254A (en) * | 2018-08-06 | 2018-11-06 | 江苏兆辉防腐科技有限公司 | A kind of steel lining tetrafluoro reactor |
| CN111268884A (en) * | 2020-03-31 | 2020-06-12 | 浙江科茂环境科技有限公司 | Oil sludge treatment system and method |
| CN111268884B (en) * | 2020-03-31 | 2024-04-09 | 浙江科茂环境科技有限公司 | Oil sludge treatment system and method |
| CN113832510A (en) * | 2021-09-09 | 2021-12-24 | 张家口原轼新型材料有限公司 | Steel grit with high-phosphorus nickel alloy plated on surface, plating solution, plating process, plating device and steel wire containing steel grit |
| CN113832510B (en) * | 2021-09-09 | 2023-03-10 | 张家口原轼新型材料股份有限公司 | Steel grit with surface plated with high-phosphorus nickel alloy, plating solution, plating process, plating device and steel wire containing steel grit |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 075000 workshop 2, No. 10, East Ring Road, Zhangjiakou Economic Development Zone, Hebei Province Patentee after: Zhangjiakou Yuanshi New Material Co.,Ltd. Address before: 075000 3, 06, 12 West Street, 2 Yongxing West Avenue, Zhangjiakou High-tech Zone, Hebei. Patentee before: ZHANGJIAKOU YUANSHI NEW MATERIAL CO.,LTD. |
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| CP03 | Change of name, title or address |