CN201644093U - Reaction and filter dryer - Google Patents
Reaction and filter dryer Download PDFInfo
- Publication number
- CN201644093U CN201644093U CN2010201691112U CN201020169111U CN201644093U CN 201644093 U CN201644093 U CN 201644093U CN 2010201691112 U CN2010201691112 U CN 2010201691112U CN 201020169111 U CN201020169111 U CN 201020169111U CN 201644093 U CN201644093 U CN 201644093U
- Authority
- CN
- China
- Prior art keywords
- filter
- filtering
- cylinder
- filtering table
- part cylinder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000006243 chemical reaction Methods 0.000 title abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 32
- 238000001035 drying Methods 0.000 claims abstract description 22
- 229910001220 stainless steel Inorganic materials 0.000 claims abstract description 4
- 239000010935 stainless steel Substances 0.000 claims abstract description 4
- 238000005245 sintering Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 abstract description 12
- 239000000047 product Substances 0.000 abstract description 9
- 238000003756 stirring Methods 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 6
- 239000012065 filter cake Substances 0.000 abstract description 5
- 230000008569 process Effects 0.000 abstract description 5
- 239000007788 liquid Substances 0.000 abstract description 3
- 238000007599 discharging Methods 0.000 abstract description 2
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 239000012847 fine chemical Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 description 8
- 239000000706 filtrate Substances 0.000 description 7
- 238000004140 cleaning Methods 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000003507 refrigerant Substances 0.000 description 4
- 230000005540 biological transmission Effects 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000006253 efflorescence Methods 0.000 description 3
- 206010037844 rash Diseases 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000010977 unit operation Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Filtration Of Liquid (AREA)
- Drying Of Solid Materials (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model relates to the field of chemical equipment, in particular to a material reaction and filter dryer in the fine chemical industry. The reaction and filter dryer forms a whole pressed container consisting of a standard elliptical head at the upper part, a cylinder at the middle part and a chassis at the lower part, wherein a filter disc is installed between the cylinder at the middle part and the chassis at the lower part; the filter disc and the cylinder at the middle part are connected by a quick-open pressure container flange; the filter disc adopts various filter layers of a stainless steel sinter net and the like to carry out filtration; the pressed container is internally provided with a stirring device which consists of a vertical stirring shaft, a stirring blade and an arc-shaped scraper; and the vertical stirring shaft is a hollow shaft, the stirring blade is an elliptical arc-shaped hollow stirring blade, and the filter disc is designed into elliptical. The material reaction and filter dryer can effectively save energy, reduce the production cost, optimize the production technique process, reduce the environmental pollution, realize CIP (clearing in place), reduce the labor intensity, has high drying efficiency for a product, effectively pulverizes filter cakes with thorough discharging; and the filter liquid are recovered and utilized accurately.
Description
Technical field:
The utility model relates to chemical industry equipment field, especially reacting filtering drying machine.
Background technology:
In modernization industry is produced, for the upstream solidliquid mixture that makes through reaction, extraction, absorption, concentrates, technology such as crystallization is produced is able to effective separation, and be refined into product, and must pass through the kinds of processes unit operations, be combined into a rational production line and realize.
At present, equipment such as existing cone type filtering drying machine, rotary filtration washing drying machine, Highefficientpulverizer, bag-turning pattern centrifugal separator.As patent " a kind of cone type filtering drying machine ", its patent No. is ZL96229672.4, introduced a kind of cone type filtering drying machine, had on same machine, finish filtration, washing, concentrate, multiple unit operations such as crystallization, drying, have easy to operate, take up an area of less, advantage such as product efficiency height, work personnel are few, but the spiral agitator structure does not possess functions such as the effective efflorescence of the filter cake of making, discharge be thorough, can not meet the needs of production, more can not implement cleaning on the throne, accurately reclaim filtrate etc.As patent " hollow ribbon stirring inner heating device ", its patent No. is ZL01245396.X, disclose a kind of hollow ribbon and stirred inner heating device, and the top mechanically-sealing apparatus that matches with this inner heating device, this device has proposed to add in the hollow ribbon thermal concept, but do not consider that the ribbon stirring structure must have certain lead angle, for not stockpiled on the ribbon surface, material is difficult to unload, so ribbon spirals the number of turns can not be too many, so just make ribbon not have bigger heating surface (area) (HS, then drying effect is just undesirable, in the dry run easy " caking " or " balling-up ", rate of drying is slow.
Summary of the invention:
The utility model purpose is to provide a kind of effectively energy savings, reduce production costs, optimize the technological process of production, reduce environmental pollution, realize CIP cleaning on the throne, reduce labour intensity, and reach product drying efficient height, the effective efflorescence of filter cake, discharge are thorough, the reacting filtering drying machine that filtrate is accurately recycled.
Reacting filtering drying machine, form whole pressure-vessel by top standard elliptical head, middle part cylinder and bottom chassis, filtering table is installed between middle part cylinder and the bottom chassis, connect by fast-open type pressure vessel flange between filtering table and the middle part cylinder, multiple filter courses such as filtering table employing stainless steel sintering net filter, there is agitating device pressure-vessel inside, agitating device is made up of vertical shaft, stirrer paddle and arcuation scraper, vertical shaft is a quill shaft, stirrer paddle is oval arcuation hollow stirrer paddle, and filtering table is designed to ellipse.
The middle part cylinder is provided with chuck outward, and the chuck upper end is provided with the media inlet, the chuck lower end is provided with the media outlet.
The filtering table below is provided with back-shaped pipe, and back-shaped Guan Yiduan is provided with the media inlet, and the other end is provided with the media outlet.
The beneficial effects of the utility model are:
Adopt the elliptic agitating device, avoid dead angle and bigger with the material contact area, can make the material rapid mixing complete, sufficient reacting, arcuation doctor blade device can realize that the effective efflorescence and the discharge of product is thorough; Can feed thermal medium and carry out heat drying cylindrical shell chuck, hollow shaft and hollow stirrer paddle, the back-shaped pipe in filter disc below simultaneously, ensure heating surface (area) (HS, improve production efficiency greatly.
Description of drawings
Fig. 1 is this utility model equipment organigram
1 transmission device, 2 lowering or hoisting gears, 3 vertical shaft 4 cleaning devices 5 middle part cylinders 6 stirrer paddles 7 filtering tables 8 frames 9 bleeder valves 10 exhaust outlets 11 charging apertures, 12 filter washing water inlets, 13 filtrate (liquids, 14 media, 15 media that enter the mouth export 16 packaged type bracing frames, 17 media, 18 media that enter the mouth and export 19 air inlets, 20 arcuation scrapers, 21 chucks, 22 bottom chassis, 23 hydraulic jacks, 24 fast-open type pressure vessel flanges, 25 ellipse heads, 26 back-shaped pipes
Specific embodiment
Reacting filtering drying machine is formed whole pressure-vessel by top standard elliptical head, middle part cylinder 5 and bottom chassis 22.Filtering table 7 is installed between middle part cylinder 5 and the bottom chassis 22, connects by fast-open type pressure vessel flange 24 between bottom chassis 22 and the middle part cylinder 5.Multiple filter mediums such as filtering table 7 employing stainless steel sintering nets filter, and there is agitating device pressure-vessel inside.Agitating device is made up of the vertical shaft 3 of hollow, oval arcuation hollow stirrer paddle 6 and arcuation scraper 20.Agitating device is driven by transmission devices such as top motor and reductor 1.Filtering table 7 is designed to ellipse.
The middle part cylinder 5 external chucks 21 that are provided with, the upper end of chuck 21 are provided with media inlet 14, and the lower end is provided with media outlet 15.
Filtering table 7 belows are provided with back-shaped pipe 26, and back-shaped pipe 26 1 ends are provided with media inlet 17, and the other end is provided with media outlet 18.
The utility model is as follows to the technical process of the reaction of product, filtration, drying process:
During work, at first open exhaust outlet 10, under the effect of pump, feed raw material successively by charging aperture 11.Charging is closed exhaust outlet 10 after finishing.Needs according to course of reaction are controlled temperature, then feed refrigerant or heating agent by 14 pairs of chucks of media inlet 21, media is discharged by media outlet 15, simultaneously media inlet 17 is fed refrigerant or heating agent, discharge by media outlet 18, guarantee thus to react temperature required.Then, open transmission device 1, drive agitating device and realize speed change, rotatablely move, and agitating device realizes constant speed rising, descending motion under the effect of lowering or hoisting gear 2, stir by stirrer paddle 6 and 20 pairs of materials of scraper mechanism along being rotated counterclockwise motion.Because this equipment adopts the elliptic agitating device, has avoided dead angle and bigger with the material contact area, can make the material rapid mixing complete, sufficient reacting.After reaction finishes, in chuck 21, feed refrigerant by media inlet 14, and discharge by media outlet 15, simultaneously media inlet 17 is fed refrigerant, discharge by media outlet 18, the product crystallization is separated out.After crystallization is finished, connect vacuum extractor, allow filtrate and crystal separation, and discharge by filtrate (liquid 13 at exhaust outlet 10.In separation process, owing to equipment is operated under air-tight state, thus can on air inlet 19, feed nitrogen, and can vacuumize, do not improved the rate of filtration when in protection crystal dry run, not being destroyed, make faster, the discharge more completely of filtrate.After filtrate is discharged, feed steam, feed heating agent by 14 pairs of chucks of media inlet 21 by 17 pairs of back-shaped pipes 26 of media inlet and agitating device, three aspects are used in combination carries out heat drying to product, and control dry temperature required by the thermal source of access to plant, vacuumize by vavuum pump simultaneously and take away the solvent that is evaporated, condenser of device reclaims solvent before vavuum pump.
Because material is to move in a circle in dry run, " balling-up " easily after the balling-up, is difficult for drying in the inside of ball, and easy knot so just is difficult to the purity and the quality of control product.In such cases, we can start special elliptic agitating device, and when arcuation scraper 20 rotates weeks, the material powder just contacts once with agitating device.Generally in rotation process, the time that the control blade contacts with material is 1/3 commentaries on classics.The rotating speed of stirrer paddle 6 is regulated by frequency converter and be can reach 280 rev/mins.Like this, balling-up, the agglomeration problems of material in the rotary drying process just solved easily.
At last, dry filter cake completely is under the effect of arcuation scraper 20, and filter cake is swept and arrived in bleeder valve 9 positions, can manually discharge outside the machine.After the discharging, can clean equipment.This equipment bottom chassis 22 is removable chassis, adopts flange 24 to be connected with middle part cylinder 5.Hydraulic jack 23 is realized installation and removal.Bottom chassis 22 bottoms have packaged type bracing frame 16, are convenient to shift out bottom chassis 22 and clean elliptic filtering table 7.Device interior is cleaned employing cleaning device 4 on the throne spray, easy to operate, raise the efficiency.
Should be noted that at last: above embodiment only is not intended to limit in order to the explanation the technical solution of the utility model; Although with reference to preferred embodiment the utility model is had been described in detail, those of ordinary skill in the field are to be understood that: still can make amendment or the part technical characterictic is equal to replacement the specific embodiment of the present utility model; And not breaking away from the spirit of technical solutions of the utility model, it all should be encompassed in the middle of the technical scheme scope that the utility model asks for protection.
Claims (3)
1. reacting filtering drying machine, by the top standard elliptical head, middle part cylinder and bottom chassis are formed whole pressure-vessel, filtering table is installed between middle part cylinder and the bottom chassis, connect by fast-open type pressure vessel flange between filtering table and the middle part cylinder, multiple filter courses such as filtering table employing stainless steel sintering net filter, there is agitating device pressure-vessel inside, agitating device is by vertical shaft, stirrer paddle and arcuation scraper are formed, it is characterized in that, vertical shaft is a quill shaft, stirrer paddle is oval arcuation hollow stirrer paddle, and filtering table is designed to ellipse.
2. according to the described reacting filtering drying machine of claim 1, it is characterized in that the middle part cylinder is provided with chuck outward, the chuck upper end is provided with the media inlet, the chuck lower end is provided with the media outlet.
3. according to the described reacting filtering drying machine of claim 1, it is characterized in that the filtering table below is provided with back-shaped pipe, back-shaped Guan Yiduan is provided with the media inlet, and the other end is provided with the media outlet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010201691112U CN201644093U (en) | 2010-03-25 | 2010-03-25 | Reaction and filter dryer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010201691112U CN201644093U (en) | 2010-03-25 | 2010-03-25 | Reaction and filter dryer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201644093U true CN201644093U (en) | 2010-11-24 |
Family
ID=43109289
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010201691112U Expired - Lifetime CN201644093U (en) | 2010-03-25 | 2010-03-25 | Reaction and filter dryer |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201644093U (en) |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102607256A (en) * | 2012-03-16 | 2012-07-25 | 常州市宇通干燥设备有限公司 | Multifunctional drying host |
| CN103464080A (en) * | 2013-09-25 | 2013-12-25 | 南京威安新材料科技有限公司 | Preparation device of solid mixed-type catalyst |
| CN103599743A (en) * | 2013-10-18 | 2014-02-26 | 昆山珍实复合材料有限公司 | Reaction kettle with scraper cleaning mechanism |
| CN103752250A (en) * | 2014-01-20 | 2014-04-30 | 德清县维康生物科技有限公司 | Multifunctional integrated pot |
| CN103949083A (en) * | 2014-05-07 | 2014-07-30 | 无锡市张华医药设备有限公司 | Crystallization tank |
| CN105498328A (en) * | 2014-09-25 | 2016-04-20 | 中国石油化工股份有限公司 | Washing tower |
| ITUB20152211A1 (en) * | 2015-07-15 | 2017-01-15 | Delta Costruzioni Mecc S R L | DEVICE AND METHOD TO SEPARATE THE SOLID FRACTION FROM THE LIQUID FRACTION OF A TURBID |
| CN106824898A (en) * | 2017-01-10 | 2017-06-13 | 浙江亚光科技股份有限公司 | Filtration washing drying equipment |
| CN109224500A (en) * | 2018-09-25 | 2019-01-18 | 陈同翔 | A kind of crystallization Optimizing manufacture technique of edible salt |
| CN111921434A (en) * | 2020-07-21 | 2020-11-13 | 合肥通用机械研究院有限公司 | Integrated production process for ternary material |
| CN113070016A (en) * | 2021-04-21 | 2021-07-06 | 临沂市海鑫化工设备有限公司 | Glass lining filter |
| CN113941181A (en) * | 2021-06-17 | 2022-01-18 | 中化学科学技术研究有限公司 | Ultra-high molecular weight polyethylene filtering and drying method and device |
| CN114602224A (en) * | 2022-01-24 | 2022-06-10 | 合肥通用机械研究院有限公司 | Intrinsic safety type filtering and washing dual-purpose machine for energetic materials |
-
2010
- 2010-03-25 CN CN2010201691112U patent/CN201644093U/en not_active Expired - Lifetime
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102607256A (en) * | 2012-03-16 | 2012-07-25 | 常州市宇通干燥设备有限公司 | Multifunctional drying host |
| CN102607256B (en) * | 2012-03-16 | 2015-06-10 | 江苏宇通干燥工程有限公司 | Multifunctional drying host |
| CN103464080A (en) * | 2013-09-25 | 2013-12-25 | 南京威安新材料科技有限公司 | Preparation device of solid mixed-type catalyst |
| CN103599743A (en) * | 2013-10-18 | 2014-02-26 | 昆山珍实复合材料有限公司 | Reaction kettle with scraper cleaning mechanism |
| CN103599743B (en) * | 2013-10-18 | 2015-05-20 | 昆山珍实复合材料有限公司 | Reaction kettle with scraper cleaning mechanism |
| CN103752250A (en) * | 2014-01-20 | 2014-04-30 | 德清县维康生物科技有限公司 | Multifunctional integrated pot |
| CN103949083A (en) * | 2014-05-07 | 2014-07-30 | 无锡市张华医药设备有限公司 | Crystallization tank |
| CN103949083B (en) * | 2014-05-07 | 2016-04-20 | 无锡市张华医药设备有限公司 | A kind of crystallizing tank |
| CN105498328A (en) * | 2014-09-25 | 2016-04-20 | 中国石油化工股份有限公司 | Washing tower |
| CN105498328B (en) * | 2014-09-25 | 2017-07-14 | 中国石油化工股份有限公司 | Scrubbing tower |
| WO2017009709A1 (en) * | 2015-07-15 | 2017-01-19 | Delta Costruzioni Meccaniche S.R.L. | Device and method for separating the solid fraction from the liquid fraction of a slurry |
| ITUB20152211A1 (en) * | 2015-07-15 | 2017-01-15 | Delta Costruzioni Mecc S R L | DEVICE AND METHOD TO SEPARATE THE SOLID FRACTION FROM THE LIQUID FRACTION OF A TURBID |
| RU2712698C2 (en) * | 2015-07-15 | 2020-01-30 | Дельта Коструцьони Мекканике С.Р.Л. | Device and method of separation of solid fraction from liquid fraction of suspension |
| CN106824898A (en) * | 2017-01-10 | 2017-06-13 | 浙江亚光科技股份有限公司 | Filtration washing drying equipment |
| CN109224500A (en) * | 2018-09-25 | 2019-01-18 | 陈同翔 | A kind of crystallization Optimizing manufacture technique of edible salt |
| CN111921434A (en) * | 2020-07-21 | 2020-11-13 | 合肥通用机械研究院有限公司 | Integrated production process for ternary material |
| CN113070016A (en) * | 2021-04-21 | 2021-07-06 | 临沂市海鑫化工设备有限公司 | Glass lining filter |
| CN113941181A (en) * | 2021-06-17 | 2022-01-18 | 中化学科学技术研究有限公司 | Ultra-high molecular weight polyethylene filtering and drying method and device |
| CN114602224A (en) * | 2022-01-24 | 2022-06-10 | 合肥通用机械研究院有限公司 | Intrinsic safety type filtering and washing dual-purpose machine for energetic materials |
| CN114602224B (en) * | 2022-01-24 | 2024-01-12 | 合肥通用机械研究院有限公司 | Intrinsic safety type energy-containing material filtering and washing dual-purpose machine |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: PUYANG HUICHENG ELECTRONIC MATERIAL CO., LTD. Free format text: FORMER NAME: PUYANG HUICHENG CHEMICAL CO., LTD. |
|
| CP03 | Change of name, title or address |
Address after: 457001 west section of Shengli Road, Henan, Puyang Patentee after: Puyang Huicheng Electronic Material Co., Ltd. Address before: 457000 the Yellow River Road, Henan, Puyang Patentee before: Puyang Huicheng Chemical Co., Ltd. |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Horizontal reacting filtering drying machine and its method Effective date of registration: 20130927 Granted publication date: 20101124 Pledgee: Bank of China Limited by Share Ltd Puyang Development Zone Branch Pledgor: Puyang Huicheng Electronic Material Co., Ltd. Registration number: 2013990000714 |
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| PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20170327 Granted publication date: 20101124 Pledgee: Bank of China Limited by Share Ltd Puyang Development Zone Branch Pledgor: Puyang Huicheng Electronic Material Co., Ltd. Registration number: 2013990000714 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Horizontal reacting filtering drying machine and its method Effective date of registration: 20170517 Granted publication date: 20101124 Pledgee: Zhongyuan bank, Limited by Share Ltd, Puyang branch Pledgor: Puyang Huicheng Electronic Material Co., Ltd. Registration number: 2017410000014 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| CX01 | Expiry of patent term |
Granted publication date: 20101124 |
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| CX01 | Expiry of patent term | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20200326 Granted publication date: 20101124 Pledgee: Zhongyuan bank, Limited by Share Ltd, Puyang branch Pledgor: PUYANG HUICHENG ELECTRONIC MATERIAL Co.,Ltd. Registration number: 2017410000014 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right |