CN206037739U - Novel prevent foam rotary evaporato condenser - Google Patents

Novel prevent foam rotary evaporato condenser Download PDF

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Publication number
CN206037739U
CN206037739U CN201620968152.5U CN201620968152U CN206037739U CN 206037739 U CN206037739 U CN 206037739U CN 201620968152 U CN201620968152 U CN 201620968152U CN 206037739 U CN206037739 U CN 206037739U
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China
Prior art keywords
solvent
condenser
foam
condensing tube
shell
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CN201620968152.5U
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Chinese (zh)
Inventor
王文钦
孙立水
凌坤华
范阳海
纪明智
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JIANGSU STERRIC CHEMICAL INDUSTRY Co Ltd
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JIANGSU STERRIC CHEMICAL INDUSTRY Co Ltd
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Priority to CN201620968152.5U priority Critical patent/CN206037739U/en
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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model provides a novel prevent foam rotary evaporato condenser, a serial communication port, condenser shells inner wall is equipped with the solvent catch tank, the solvent catch tank is the heliciform, condenser shells inner wall still is equipped with the solvent groove of gathering, solvent in the solvent catch tank collects the solvent groove of gathering, the solvent gathers tank bottom portion and is equipped with a plurality of solvent exhaust ports, the foam is collected a mouthful upper end and is connected the solvent trough rim reason that gathers. The utility model discloses a novel prevent foam rotary evaporato condenser with solvent and foam clean separation, forms spiral collecting vat at the internal surface of condenser shell, then the solvent in the collecting vat is unified collects the groove of gathering, is equipped with the solvent exhaust port in the groove of gathering, collects produced foam this moment and can collect the foam and collect mouthful, and is fine with solvent and foam separation.

Description

A kind of new foam-resistant rotary evaporator condenser
Technical field
This utility model is related to a kind of condenser technology field, more particularly to a kind of new foam-resistant Rotary Evaporators condensation Device.
Background technology
Rotary Evaporators are to realize the ideal instrument such as extract or product concentration, crystallization, separation, recovery. At present, in the field such as biology, medicine, chemical industry, food there is in lab scale, pilot scale and production application widely.Its master If by electronic speed regulation, making evaporative flask constant speed rotary under suitable speed, the boiling point of solution is reduced under condition of negative pressure, is made Bottle internal solvent diffusive evaporation, then realizes the heat-sensitive ingredients in protection concentrated solution at low temperature by condenser recycling design again While realize to the concentration of extract or the separation of product and purification.
But, separating and purification some special materials, during solution such as containing foaming class surfactant, can be rapid Substantial amounts of foam is produced, these foams are difficult timely to eliminate, will directly spill in solvent receiving flask along pipeline, cause Detached failure.
Utility model content
Based on this, in order to solve the technical problem of the above, this utility model provides a kind of new foam-resistant Rotary Evaporators Condenser.
Technical solutions of the utility model are as follows:A kind of new foam-resistant rotary evaporator condenser, it is characterised in that include Condenser shell, condenser water inlet, condensing tube, leaving condenser water mouth, condenser air inlet, evaporative flask connector, solvent are received Collection bottle interface, foam receiving flask interface, foam collection port and condensing tube solvent collecting board;The condensing tube is installed on described cold In condenser housing, the condenser water inlet connects the condensing tube top, and the leaving condenser water mouth is arranged at the condensation Ttom of pipe end, the condenser air inlet and evaporative flask connector are located at the condenser shell lower right, and the solvent is collected Bottle interface is located at below the condenser shell, and the foam receiving flask interface is located at the condenser shell lower left, described Foam collection port and condensing tube solvent collecting board are fixed inside the condenser shell, and are located under the condensing tube Side;
The condenser shell inwall is provided with solvent catch tank, the solvent catch tank in the shape of a spiral, the condenser shell Wall is additionally provided with solvent aggregation slot in vivo, and the solvent in the solvent catch tank is pooled to the solvent aggregation slot, and the solvent converges Total trench bottom is provided with some solvent taps, and the foam collection port upper end connects the solvent and collects groove edge.
Wherein in an embodiment, the foam collection port is connected with the foam receiving flask interface by connecting tube.
Wherein in an embodiment, described condensing tube solvent collecting board one end is arranged at below the leaving condenser water mouth, The other end connects the solvent aggregation slot.
Wherein in an embodiment, the condensing tube solvent collecting board is 30 ° ~ 56 ° with horizontal direction angle.
The beneficial effects of the utility model:
A kind of new foam-resistant rotary evaporator condenser of the present utility model, solvent and foam are kept completely separate, The inner surface of condenser shell forms screw type collecting tank, and the then solvent unification in collecting tank is pooled in aggregation slot, is converged Solvent tap is provided with total groove, now collect produced by foam can be pooled in foam collection port, well by solvent and Foam separation.
Description of the drawings
In order to be illustrated more clearly that this utility model embodiment or technical scheme of the prior art, below will be to embodiment Or accompanying drawing to be used is briefly described needed for description of the prior art.
Fig. 1 is a kind of new foam-resistant rotary evaporator condenser structural representation;
Fig. 2 is a kind of new foam-resistant rotary evaporator condenser inner wall section structural representation.
Specific embodiment
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is carried out Clearly and completely describe, it is clear that described embodiment is only this utility model a part of embodiment, rather than whole Embodiment.Based on the embodiment in this utility model, those of ordinary skill in the art are not under the premise of creative work is made The every other embodiment for being obtained, belongs to the scope of this utility model protection.
It should be noted that when element is referred to as " being arranged at " another element, it can directly on another element Or can also there is element placed in the middle.When an element is considered as " connection " another element, it can be directly connected to To another element or may be simultaneously present centering elements.Term as used herein " vertical ", " level ", " left side ", For illustrative purposes only, it is unique embodiment to be not offered as " right side " and similar statement.
Unless otherwise defined, all of technology used herein and scientific terminology are led with technology of the present utility model is belonged to The implication that the technical staff in domain is generally understood that is identical.Description is intended merely in term used in the description of the present utility model The purpose of specific embodiment, it is not intended that in restriction this utility model.Term as used herein "and/or" includes one Or the arbitrary and all of combination of multiple related Listed Items.
Refer to Fig. 1 and Fig. 2, a kind of new foam-resistant rotary evaporator condenser, it is characterised in that including condenser Housing 10, condenser water inlet 20, condensing tube 21, leaving condenser water mouth 22, condenser air inlet 30, evaporative flask connector 31, Solvent receiving flask interface 32, foam receiving flask interface 33, foam collection port 40 and condensing tube solvent collecting board 50;The condensation Pipe 21 is installed in the condenser shell 10, and the condenser water inlet 20 connects 21 top of the condensing tube, the condensation Device outlet 22 is arranged at 21 bottom of the condensing tube, and the condenser air inlet 30 and evaporative flask connector 31 are positioned at described 10 lower right of condenser shell, the solvent receiving flask interface 32 are located at below the condenser shell 10, and the foam is collected Bottle interface 33 is located at 10 lower left of the condenser shell, and the foam collection port 40 and condensing tube solvent collecting board 50 are fixed Inside the condenser shell 10, and it is located at below the condensing tube 21;
10 inwall of the condenser shell is provided with solvent catch tank 60, and the solvent catch tank 60 is in the shape of a spiral, described cold 10 inwall of condenser housing is additionally provided with solvent aggregation slot 70, and the solvent in the solvent catch tank 60 is pooled to the solvent aggregation slot 70,70 bottom of solvent aggregation slot is provided with some solvent taps 71, and 40 upper end of foam collection port connects the solvent 70 edge of aggregation slot.
Another preferred version, the foam collection port 40 are connected with the foam receiving flask interface 33 by connecting tube.
Another preferred version, described 50 one end of condensing tube solvent collecting board are arranged at below the leaving condenser water mouth 22, The other end connects the solvent aggregation slot 70.
Another preferred version, the condensing tube solvent collecting board 50 are 30 ° ~ 56 ° with horizontal direction angle.
A kind of new foam-resistant rotary evaporator condenser of the present utility model, solvent and foam are kept completely separate, The inner surface of condenser shell forms screw type collecting tank, and the then solvent unification in collecting tank is pooled in aggregation slot, is converged Solvent tap is provided with total groove, now collect produced by foam can be pooled in foam collection port, well by solvent and Foam separation.
It is understandable for enabling above-mentioned purpose of the present utility model, feature and advantage to become apparent from, above in conjunction with accompanying drawing to this The specific embodiment of utility model is described in detail.Elaborate many details in order to abundant in superincumbent description Understand this utility model.But this utility model can be implemented with being much different from alternate manner described above, this area Technical staff can do similar improvement, therefore this utility model in the case of without prejudice to this utility model intension not by public above The restriction of the specific embodiment opened.Also, each technical characteristic of embodiment described above arbitrarily can be combined, for making to retouch State succinctly, combination not all possible to each technical characteristic in above-described embodiment is all described, as long as however, these skills There is no contradiction in the combination of art feature, be all considered to be the scope of this specification record.
Embodiment described above only expresses several embodiments of the present utility model, and its description is more concrete and detailed, But therefore can not be interpreted as the restriction to this utility model the scope of the claims.It should be pointed out that common for this area For technical staff, without departing from the concept of the premise utility, some deformations and improvement can also be made, these all belong to In protection domain of the present utility model.Therefore, the protection domain of this utility model patent should be defined by claims.

Claims (4)

1. a kind of new foam-resistant rotary evaporator condenser, it is characterised in that including condenser shell(10), condenser water inlet Mouthful(20), condensing tube(21), leaving condenser water mouth(22), condenser air inlet(30), evaporative flask connector(31), solvent collect Bottle interface(32), foam receiving flask interface(33), foam collection port(40)And condensing tube solvent collecting board(50);The condensation Pipe(21)It is installed on the condenser shell(10)It is interior, the condenser water inlet(20)Connect the condensing tube(21)Top, The leaving condenser water mouth(22)It is arranged at the condensing tube(21)Bottom, the condenser air inlet(30)And evaporative flask connects Interface(31)Positioned at the condenser shell(10)Lower right, the solvent receiving flask interface(32)Positioned at the condenser shell (10)Lower section, the foam receiving flask interface(33)Positioned at the condenser shell(10)Lower left, the foam collection port (40)And condensing tube solvent collecting board(50)It is fixed at the condenser shell(10)Inside, and it is located at the condensing tube (21)Lower section;
The condenser shell(10)Inwall is provided with solvent catch tank(60), the solvent catch tank(60)In the shape of a spiral, it is described Condenser shell(10)Inwall is additionally provided with solvent aggregation slot(70), the solvent catch tank(60)In solvent be pooled to it is described molten Agent aggregation slot(70), the solvent aggregation slot(70)Bottom is provided with some solvent taps(71), the foam collection port(40) Upper end connects the solvent aggregation slot(70)Edge.
2. a kind of new foam-resistant rotary evaporator condenser as claimed in claim 1, it is characterised in that the foam is collected Mouthful(40)By connecting tube and the foam receiving flask interface(33)Connection.
3. a kind of new foam-resistant rotary evaporator condenser as claimed in claim 1, it is characterised in that the condensing tube is molten Agent collecting board(50)One end is arranged at the leaving condenser water mouth(22)Lower section, the other end connect the solvent aggregation slot(70).
4. a kind of new foam-resistant rotary evaporator condenser as claimed in claim 3, it is characterised in that the condensing tube is molten Agent collecting board(50)It it is 30 ° ~ 56 ° with horizontal direction angle.
CN201620968152.5U 2016-08-30 2016-08-30 Novel prevent foam rotary evaporato condenser Active CN206037739U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620968152.5U CN206037739U (en) 2016-08-30 2016-08-30 Novel prevent foam rotary evaporato condenser

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620968152.5U CN206037739U (en) 2016-08-30 2016-08-30 Novel prevent foam rotary evaporato condenser

Publications (1)

Publication Number Publication Date
CN206037739U true CN206037739U (en) 2017-03-22

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109442809A (en) * 2018-10-25 2019-03-08 广州科奥版权服务有限公司 A kind of dry evaporator that the expanding foam removal for Water Cooled Centrifugal Machine group is dredged

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109442809A (en) * 2018-10-25 2019-03-08 广州科奥版权服务有限公司 A kind of dry evaporator that the expanding foam removal for Water Cooled Centrifugal Machine group is dredged

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