CN206535537U - A kind of multifunctional chemical reacts preparation facilities - Google Patents

A kind of multifunctional chemical reacts preparation facilities Download PDF

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Publication number
CN206535537U
CN206535537U CN201720097851.1U CN201720097851U CN206535537U CN 206535537 U CN206535537 U CN 206535537U CN 201720097851 U CN201720097851 U CN 201720097851U CN 206535537 U CN206535537 U CN 206535537U
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China
Prior art keywords
valve group
preparation facilities
cohobation
pipeline
condenser
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CN201720097851.1U
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Chinese (zh)
Inventor
陆敏羽
黄强
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Shanghai Enika Technology Development Co Ltd
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Shanghai Enika Technology Development Co Ltd
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Abstract

The utility model is related to a kind of multifunctional chemical reaction preparation facilities, including reactor, condenser, lime set tank, gas-liquid separation groove, cohobation valve group, vacuum valve group, point drum valve group, hydrophobic valve group;Condenser, cohobation valve group, point drum valve group, hydrophobic valve group are linked together between reactor using pipeline;Linked together between lime set tank and cohobation valve group using pipeline;Gas-liquid separation groove is arranged on the pipeline between condenser and lime set tank;Vacuum valve group is on the pipeline that gas-liquid separation groove, cohobation valve group are connected with external pipe, and hydrophobic valve group connects outdoor sewage well.Material in the utility model enters after reactor, is chemically reacted according to technological requirement, by switching corresponding valve operation, can carry out reduced pressure distillation process operation, reduced-pressure backflow technological operation, air-distillation technological operation, atmospheric pressure reflux technological operation.The utility model, which realizes separate unit reaction unit, can carry out the function of a variety of chemical reaction operations.

Description

A kind of multifunctional chemical reacts preparation facilities
Technical field
The utility model is related to a kind of chemical reaction preparation facilities, and in particular to one kind can carry out vacuum distillation chemical reaction Operation, the operation of reduced-pressure backflow chemical reaction, the operation of air-distillation chemical reaction, the multifunction of atmospheric pressure reflux chemical reaction operation Learn reaction preparation facilities.
Background technology
Conventional chemical reaction preparation facilities can only carry out one or two kinds of simple chemosynthesis reaction operations at present, so Inefficiency, and not only waste raw material but also the pollution of site environment can be caused.
Utility model content
In view of the above-mentioned problems, main purpose of the present utility model is that vacuum distillation chemical reaction behaviour can be carried out by providing one kind Make, reduced-pressure backflow chemical reaction is operated, air-distillation chemical reaction is operated, the multifunctional chemical of atmospheric pressure reflux chemical reaction operation React preparation facilities.
The utility model is to solve above-mentioned technical problem by following technical proposals:A kind of multifunctional chemical reaction system Standby device, the multifunctional chemical reaction preparation facilities includes:Reactor, condenser, lime set tank, gas-liquid separation groove, backflow are steamed Evaporate valve group, vacuum valve group, point drum valve group, hydrophobic valve group;Condenser, cohobation valve group, point drum valve group, hydrophobic valve group are equal Linked together between reactor using pipeline;Linked together between lime set tank and cohobation valve group using pipeline;Gas Liquid separating tank is arranged on the pipeline between condenser and lime set tank;Vacuum valve group is arranged on gas-liquid separation groove, cohobation valve On the pipeline that group is connected with external pipe, hydrophobic valve group connects outdoor sewage well.
In specific embodiment of the utility model, the reactor is also equipped with flowmeter, differential manometer, is provided with observation Mouthful.
In specific embodiment of the utility model, the vacuum valve group connects external vavuum pump and engine manifold.
In specific embodiment of the utility model, described point of drum valve group is connected with main steam range, recirculated cooling water and entered Water pipe, cooling water return pipe.
In specific embodiment of the utility model, thermometer and flowmeter are installed in described point of drum valve group.
In specific embodiment of the utility model, the condenser is connected with recirculated cooling water water inlet pipe, circulating cooling Water return pipe.
Positive effect of the present utility model is:The utility model can realize continuous operation not in a reactor Same chemical reaction process.Material in the utility model enters after reactor, is chemically reacted, passed through according to technological requirement Switch corresponding valve operation, the reduced pressure distillation process operation, reduced-pressure backflow technological operation, normal pressure in being chemically reacted are steamed Evaporate technological operation, atmospheric pressure reflux technological operation.The utility model uses pipeline combined system, is truly realized separate unit reaction unit The function of a variety of chemical reaction operations can be carried out;Not only reaction efficiency is high, and does not pollute the environment.
Brief description of the drawings
Fig. 1 is overall structure diagram of the present utility model.
Embodiment
The utility model preferred embodiment is provided below in conjunction with the accompanying drawings, to describe the technical solution of the utility model in detail.
Fig. 1 is overall structure diagram of the present utility model.As shown in figure 1, the multifunctional chemical that the utility model is provided Reaction preparation facilities includes:Reactor 1, condenser 2, lime set tank 3, gas-liquid separation groove 4, cohobation valve group 5, vacuum valve group 6, Divide drum valve group 7, hydrophobic valve group 8;Condenser 2, cohobation valve group 5, point drum valve group 7, hydrophobic valve group 8 are and reactor 1 Between linked together using pipeline;Linked together between lime set tank 3 and cohobation valve group 5 using pipeline;Gas-liquid separation Groove 4 is arranged on the pipeline between condenser 2 and lime set tank 3;Vacuum valve group 6 is arranged on gas-liquid separation groove 4, cohobation valve group On 5 pipelines being connected with external pipe, hydrophobic valve group 8 connects outdoor sewage well 9.
Reactor 1 is also equipped with flowmeter, differential manometer, is provided with observation port.Vacuum valve group 6 connects external vavuum pump and tail gas House steward.Drum valve group 7 is divided to be connected with main steam range, recirculated cooling water water inlet pipe, cooling water return pipe.Divide drum valve group 7 On thermometer and flowmeter are installed.Condenser 2 is connected with recirculated cooling water water inlet pipe, cooling water return pipe.
Multifunctional chemical reaction preparation facilities can realize the operation of vacuum distillation chemical reaction, reduced-pressure backflow chemical reaction behaviour Make, air-distillation chemical reaction is operated, atmospheric pressure reflux chemical reaction operation.
1st, vacuum distillation chemical reaction operation:
Reactor stirring is opened, a point drum valve 101,102,106 is closed, opening valve 103 is passed through steam and begun to warm up Material in reactor, simultaneously closes off valve 302,201,202,205, opens the valve 203 in vacuum valve 301 and distillation valve group Start to vacuumize with 204, when temperature reaches the vapo(u)rizing temperature of the material under vacuum conditions, the fraction in material starts evaporation Into gas and it is condensed into liquid under the cooling of condenser and enters distillate drum.
2nd, reduced-pressure backflow chemical reaction operation
Reactor stirring is opened, a point drum valve 101,102,106 is closed, opening valve 103 is passed through steam and begun to warm up Material in reactor, simultaneously closes off valve 302,203,204,205, opens vacuum valve 301 and starts to vacuumize, opens return valve 201 in group and 202, when temperature reaches the vapo(u)rizing temperature of the material under vacuum conditions, the fraction in material starts evaporation Liquid is condensed into gas and under the cooling of condenser, and is back to through return duct in reactor.
3rd, air-distillation chemical reaction operation
Reactor stirring is opened, a point drum valve 101,102,106 is closed, opening valve 103 is passed through steam and begun to warm up Material in reactor, simultaneously closes off valve 301,201,202, opens atmospheric valve 302, opens 203 Hes in distillation valve group 204, when temperature reaches vapo(u)rizing temperature, the fraction in material starts to flash to gas and is condensed into liquid under the cooling of condenser Body enters distillate drum.
4th, atmospheric pressure reflux chemical reaction operation
Reactor stirring is opened, a point drum valve 101,102,106 is closed, opening valve 103 is passed through steam and begun to warm up Material in reactor, simultaneously closes off valve 301,203,204, opens atmospheric valve 302, opens 201 Hes in backflow valve group 202, when temperature reaches vapo(u)rizing temperature, the fraction in material starts to flash to gas and is condensed into liquid under the cooling of condenser Body, and be back to through return duct in reactor.
The utility model can be realized in a reactor operates continuously different chemical reaction process.
General principle of the present utility model and principal character and advantage of the present utility model has been shown and described above.One's own profession The technical staff of industry is it should be appreciated that the utility model is not restricted to the described embodiments, described in above-described embodiment and specification Simply illustrate principle of the present utility model, on the premise of the utility model spirit and scope are not departed from, the utility model is also Various changes and modifications are had, these changes and improvements are both fallen within the range of claimed the utility model, the utility model Claimed scope is by appended claims and its equivalent thereof.

Claims (6)

1. a kind of multifunctional chemical reacts preparation facilities, it is characterised in that:The multifunctional chemical reaction preparation facilities includes:Instead Answer kettle, condenser, lime set tank, gas-liquid separation groove, cohobation valve group, vacuum valve group, point drum valve group, hydrophobic valve group;Condensation Device, cohobation valve group, point drum valve group, hydrophobic valve group are linked together between reactor using pipeline;Lime set tank and Linked together between cohobation valve group using pipeline;Gas-liquid separation groove is arranged on the pipeline between condenser and lime set tank On;Vacuum valve group is on the pipeline that gas-liquid separation groove, cohobation valve group are connected with external pipe, and hydrophobic valve group connects outdoor Bilge well.
2. multifunctional chemical according to claim 1 reacts preparation facilities, it is characterised in that:The reactor is also equipped with Flowmeter, differential manometer, is provided with observation port.
3. multifunctional chemical according to claim 1 reacts preparation facilities, it is characterised in that:The vacuum valve group connects external Vavuum pump and engine manifold.
4. multifunctional chemical according to claim 1 reacts preparation facilities, it is characterised in that:Described point of drum valve group connection There are main steam range, recirculated cooling water water inlet pipe, cooling water return pipe.
5. multifunctional chemical according to claim 1 reacts preparation facilities, it is characterised in that:Pacify in described point of drum valve group Equipped with thermometer and flowmeter.
6. multifunctional chemical according to claim 1 reacts preparation facilities, it is characterised in that:The condenser, which is connected with, to follow Ring cooling water inlet pipe, cooling water return pipe.
CN201720097851.1U 2017-01-25 2017-01-25 A kind of multifunctional chemical reacts preparation facilities Active CN206535537U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720097851.1U CN206535537U (en) 2017-01-25 2017-01-25 A kind of multifunctional chemical reacts preparation facilities

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720097851.1U CN206535537U (en) 2017-01-25 2017-01-25 A kind of multifunctional chemical reacts preparation facilities

Publications (1)

Publication Number Publication Date
CN206535537U true CN206535537U (en) 2017-10-03

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CN201720097851.1U Active CN206535537U (en) 2017-01-25 2017-01-25 A kind of multifunctional chemical reacts preparation facilities

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CN (1) CN206535537U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110052235A (en) * 2019-05-14 2019-07-26 台州道致科技股份有限公司 A kind of multi-functional automation reaction control system
CN110787755A (en) * 2019-11-08 2020-02-14 李德祥 Arrangement method of reaction kettle steam drum and related pipelines

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110052235A (en) * 2019-05-14 2019-07-26 台州道致科技股份有限公司 A kind of multi-functional automation reaction control system
CN110052235B (en) * 2019-05-14 2023-11-24 台州道致科技股份有限公司 Multifunctional automatic reaction control system
CN110787755A (en) * 2019-11-08 2020-02-14 李德祥 Arrangement method of reaction kettle steam drum and related pipelines

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