CN205925689U - Stirring formula reaction unit - Google Patents

Stirring formula reaction unit Download PDF

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Publication number
CN205925689U
CN205925689U CN201620816886.1U CN201620816886U CN205925689U CN 205925689 U CN205925689 U CN 205925689U CN 201620816886 U CN201620816886 U CN 201620816886U CN 205925689 U CN205925689 U CN 205925689U
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China
Prior art keywords
retort
shaft
stirred reactor
wall
heating
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CN201620816886.1U
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Chinese (zh)
Inventor
张基明
杨长满
蒋家均
杨金明
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Zunyi Beiyuan Chemical Co Ltd
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Zunyi Beiyuan Chemical Co Ltd
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  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The utility model provides a the utility model provides a pair of stirring formula reaction unit, including electricity, retort and setting at the inside agitating unit of retort, the motor passes through the support frame to be installed at the retort top, and the deferent segment of motor is continuous with agitating unit, the retort top is located the support frame both sides and sets up feed inlet A and feed inlet B respectively, the bottom of retort still is provided with the discharge gate, there is the casing through flange joint on the retort outer wall, from interior to having set gradually zone of heating and heat preservation outward between retort outer wall and the casing, it has arranged the condenser pipe to be the heliciform on the retort inner wall, the condensation both ends are provided with inlet tube and drain pipe respectively, and are provided with water intaking valve and drain valve on inlet tube and drain pipe respectively. The utility model discloses a set up the zone of heating on the reation kettle outer wall to outside wrap heat insulation layer realizes the heat preservation function at the zone of heating, through setting up the purpose that the condenser pipe reaches circulative cooling.

Description

A kind of stirred reactor
Technical field
This utility model belongs to chemical reaction device technical field, is specifically related to a kind of stirred reactor.
Background technology
It is known that commonly using reactor in industries such as oil, chemical industry, food, medicine, pesticide, scientific researches to complete polymerization, contracting The chemical enginnering processes such as conjunction, sulfuration, hydrocarbonylation, hydrogenation, reactor is as output organic dyestuff and intermediate many technical processs Consersion unit, in order to promote the response speed in reactor and effect, is arranged at existing reactor typically axis in tank body One stirring rotating shaft, rotating shaft upper end is connected with the electric machine assembly being arranged on tank body top, and rotating shaft lower end is provided with paddle, with When in order to increase stirring scope, paddle is generally configured to and inner tank wall shape same shape, and the entirety enabling material is stirred Mix.But the viscosity of partial material is higher, or the stage of reaction can produce the high material of viscosity, leads to stir resistance increase.
For reducing stirring resistance, it is anti-that the Chinese patent of Publication No. CN203540547U discloses a kind of high intensity stirring-type Answer kettle, including tank body, tank wall upper end is uniformly provided with some bearings, and tank wall bottom is provided with discharging opening, tank body top Middle part is provided with electric machine assembly, and electric machine assembly is respectively provided on two sides with charging aperture A and charging aperture B, and electric machine assembly bottom is connected with rotating shaft, In rotating shaft lower end insertion tank body, shaft end is connected with paddle;Described paddle is U-shaped, paddle upper end and inner tank wall Pull bar is connected with parallel segmentation, the pull bar other end is affixed with rotating shaft.This reactor anchor paddle upper end and rotating shaft it Between be connected with pull bar, the same fixed of paddle upper end is realized by this pull bar, it is to avoid the big resistance stirring of high viscosity material causes Stirring phyllomorphosis.But the rotating shaft of this reactor is an entirety, deposits unadjustable in use, therefore in course of reaction In can lead to stir not in place, thus leading to stir uneven and affecting reaction effect;This reactor does not possess heating and protects simultaneously Temperature function, it is impossible to the reaction that satisfaction needs are carried out at a certain temperature requires, does not possess the refrigerating function in course of reaction yet, because This existing reactor is preferable not enough, awaits perfect further.
Utility model content
For solving above-mentioned technical problem, this utility model provides a kind of stirred reactor.
This utility model is achieved by the following technical programs.
A kind of stirred reactor that this utility model provides, includes electric, retort and is arranged within retort Agitating device, described motor is arranged on reaction tank top by bracing frame, and the deferent segment of motor is connected with agitating device, described Reaction tank top is respectively provided with charging aperture A and charging aperture B positioned at bracing frame both sides, and the bottom of described retort is additionally provided with discharging Mouthful, described reaction tank wall is connected with housing by flange, sets successively from the inside to the outside between described reaction tank wall and housing It is equipped with zone of heating and heat-insulation layer;It is disposed with condensing tube in the shape of a spiral, described condensation two ends are respectively provided with described reaction top tank structure There are water inlet pipe and drain pipe, and water intaking valve and drain valve are respectively arranged with water inlet pipe and drain pipe.
Described agitating device includes shaft A and shaft B, and described shaft A upper end is connected with the outfan of motor, institute State shaft A lower end to be connected with shaft B by adjusting rod, described shaft B stirs at least provided with one layer from the bottom to top Part, wherein, mixing component includes sleeve and the paddle along its circumference direction arrangement, and described sleeve set is in shaft B On, and locked by securing member.
Described housing upper end is fixed with housing annulus ring flange, and housing annulus ring flange passes through bolt and is fixed on retort Tank body annulus ring flange on outer wall is connected.
Described paddle is arcuate structure outwardly.
At least two pieces of described paddle is along its circumference direction arrangement.
The heater of the flat that described zone of heating processes for Fe-based perovskite-like oxide.
On described reaction tank wall, support feet is connected with by flange, and support feet triangularity arrangement.
Described securing member is bolt or screw.
Described support feet bottom is provided with travelling wheel.
The beneficial effects of the utility model are:
Compared with prior art, this utility model passes through to arrange zone of heating on reactor outer wall, and outside zone of heating Parcel heat-insulation layer realizes heat insulation function, to meet the requirement that needs are reacted at a certain temperature;Can allow heat transfer simultaneously To any required place, heating-up temperature is stable, and the thermal efficiency is high, is circulated cooling by arranging condensing tube, thus adjustment is anti- Should be temperature required, required with meeting reaction;Pass through to arrange scalable agitating device simultaneously, when using, can be adjusted by rotation Pole increases or reduces the length of whole shaft, to meet the use requirement of differing heights retort, not only makes retort Interior each position of reactor material be able to uniform stirring, be also greatly reduced use cost;Simultaneously between paddle Distance can be adjusted, thus reaching the uniform purpose of stirred autoclave material stirring, in addition, paddle is using arc outwardly Shape structure, can avoid material to produce accumulation on paddle, substantially increase stirring efficiency and mixing effect.
Brief description
Fig. 1 is structural representation of the present utility model;
Fig. 2 is the decomposing schematic representation of agitating device in this utility model.
In figure:1- motor, 2- bracing frame, 3- retort, 4- agitating device, 5- support feet, 6- shell, 7- zone of heating, 8- Heat-insulation layer, 9- condensing tube, 10- water inlet pipe, 11- water intaking valve, 12- drain pipe, 13- drain valve, 31- charging aperture A, 32- charging aperture B, 33- discharging opening, 34- tank body annulus ring flange, 41- shaft A, 42- adjusting rod, 43- shaft B, 44- securing member, 51- method Blue disk, 52- wheel out of shape, 61- housing annulus ring flange, 421- through hole, 431- mixing component, 4311- paddle, 4312- sleeve.
Specific embodiment
Further describe the technical solution of the utility model below in conjunction with the accompanying drawings, but claimed scope is not limited to Described.
As shown in Figure 1 and Figure 2, a kind of stirred reactor, including motor 1, retort 3 and be arranged on inside retort 3 Agitating device 4, described motor 1 is arranged on retort 3 top by bracing frame 2, and the deferent segment of motor 1 and agitating device 4 It is connected, described retort 3 top is respectively provided with charging aperture A31 and charging aperture B32 positioned at bracing frame 2 both sides, described retort 3 Bottom is additionally provided with discharging opening 33;On described retort 3 outer wall, housing 6, described retort 3 outer wall and shell are connected with by flange It is disposed with zone of heating 7 and heat-insulation layer 8 from the inside to the outside between body 6;It is disposed with condensation in the shape of a spiral on described retort 3 inwall Pipe 9, described condensing tube 9 two ends are respectively arranged with water inlet pipe 10 and drain pipe 12, and on water inlet pipe 10 and drain pipe 12 respectively It is provided with water intaking valve 11 and drain valve 13.This utility model passes through to arrange zone of heating on reactor outer wall, and outside zone of heating Side parcel heat-insulation layer realizes heat insulation function, to meet the requirement that needs are reacted at a certain temperature.It is provided with spiral simultaneously Shape condensing tube 9, can realize cooling to material in retort;And condensing tube 9 two ends are respectively arranged with water inlet pipe 10 and drain pipe 12, described water inlet pipe 10 is used for being connected with external water source with drain pipe 12, to realize circulating cooling, by water intaking valve 11 and draining Valve 13 controls into displacement.Charging aperture A31 is used for putting into dry material, and charging aperture B32 is used for putting into the liquid such as reactant liquor or solvent Material.Because discharging opening 33 is arranged on retort 3 bottom, it is easy to material emptying and cleaning retort 3.
Described agitating device 4 includes shaft A41 and shaft B43, the output of described shaft A41 upper end and motor 1 End is connected, and described shaft A41 lower end is connected with shaft B43 by adjusting rod 42, on described shaft B43 from the bottom to top extremely It is provided with one layer of mixing component 431 less, wherein, mixing component 431 includes sleeve 4312 and along sleeve 4312 circumferential directions Paddle 4311, described sleeve 4312 is sleeved on shaft B43, and is locked by securing member 44.Using the technical program, Paddle 4311 can be slided up and down in shaft B43 by sleeve 4312 and adjust into line height and spacing, realize paddle 4311 are stirred, so that the material in reactor is sufficiently stirred for, reaching good mixing effect in different depth;By It is respectively arranged with one end external screw thread in shaft A41 and shaft B43 to be connected with the female thread on adjusting rod 42, in processing stirring During axle A41 and shaft B43, the thread rotary orientation on shaft A41 and shaft B43 is contrary, and that is, the screw thread on shaft A41 is Left-hand thread, then the screw thread on shaft B43 is just right-hand thread, so, when using, can make to stir by rotation adjusting lever 42 Mix axle A41 and shaft B43 inside and outside movement vertically, and then increase or the length reducing whole shaft, to meet different height The use requirement of degree retort 3, not only makes the material in retort 3 be able to uniform stirring, is also greatly reduced use cost; In addition, paddle 4311, using arcuate structure outwardly, so can avoid material to produce accumulation on paddle 4311, greatly Improve greatly stirring efficiency and mixing effect.
At least two pieces of described paddle 4311 is along sleeve 4312 circumferential directions.So it is evenly arranged into quincunx knot Structure, further enhances mixing effect, improves stirring efficiency, accelerates material reaction speed.
The middle part of described adjusting rod 42 is provided with through hole 421.So, when adjusting, can adopt and through hole 421 diameter Carry out selecting adjusting rod 42 in the bars such as the round steel matching insertion through hole 421, time saving and energy saving.
The heater of the flat that described zone of heating 7 processes for Fe-based perovskite-like oxide.Good heat conductivity, thermal effect Rate is high, and heating is more uniform.In this way, it is possible to allow heat transfer arrive any required place, heating-up temperature is stable, uniformly, thermal effect Rate is high, increased the service life of reactor.
On described retort 3 outer wall, support feet 5 is connected with by flange 51, and support feet 5 triangularity arrangement.And support Foot 5 triangularity is arranged.Using triangular arrangement, good stability;Connected using flange and be arranged on reaction tank wall, be easy to tear open Dress, transport aspect.
Described securing member 44 is bolt or screw.It is easy to tighten and unclamp.
It is provided with two-layer mixing component 431 from the bottom to top on described shaft B43.Material stirring is made to put in place uniformly.
The width near shaft B43 one end for the described paddle 4311 is more than the width away from shaft B43 one end.In system When making, paddle 4311 is from inside to outside gradually increased, and so, in whipping process, the outside of paddle 4311 facilitates insertion into thing It is stirred in material, material can realize preferable upset outside paddle 4311 simultaneously, and then reach preferable stirring and anti- Answer effect.
Described support feet 5 bottom is provided with travelling wheel 52.It is easy to carry reactor, in actual applications, travelling wheel 52 is excellent First select universal wheel, required with meeting the steering in moving process.

Claims (10)

1. a kind of stirred reactor it is characterised in that:Including motor (1), retort (3) and be arranged in retort (3) The agitating device (4) in portion, described motor (1) is arranged on retort (3) top, and the deferent segment of motor (1) by bracing frame (2) It is connected with agitating device (4), described retort (3) top is respectively provided with charging aperture A (31) and charging positioned at bracing frame (2) both sides Mouth B (32), the bottom of described retort (3) is additionally provided with discharging opening (33);Connected by flange on described retort (3) outer wall There is housing (6), between described retort (3) outer wall and housing (6), be disposed with zone of heating (7) and heat-insulation layer from the inside to the outside (8);Condensing tube (9) is disposed with the shape of a spiral on described retort (3) inwall, described condensing tube (9) two ends be respectively arranged with into Water pipe (10) and drain pipe (12), and it is respectively arranged with water intaking valve (11) and drain valve on water inlet pipe (10) and drain pipe (12) (13).
2. stirred reactor as claimed in claim 1 it is characterised in that:Described agitating device (4) includes shaft A (41) and shaft B (43), described shaft A (41) upper end is connected with the outfan of motor (1), under described shaft A (41) End is connected with shaft B (43) by adjusting rod (42), and described shaft B (43) is stirred at least provided with one layer from the bottom to top Part (431), wherein, mixing component (431) includes sleeve (4312) and the paddle along sleeve (4312) circumferential directions (4311), described sleeve (4312) is sleeved on shaft B (43), and is locked by securing member (44).
3. stirred reactor as claimed in claim 1 it is characterised in that:Described housing (6) upper end is fixed with housing circle Ring flange disk (61), housing annulus ring flange (61) passes through bolt and the tank body annulus flange being fixed on retort (3) outer wall Disk (34) is connected.
4. stirred reactor as claimed in claim 2 it is characterised in that:Described paddle (4311) is outwardly Arcuate structure.
5. stirred reactor as claimed in claim 2 it is characterised in that:Described paddle (4311) is at least two pieces of edges Sleeve (4312) circumferential directions.
6. stirred reactor as claimed in claim 1 it is characterised in that:Described zone of heating (7) is closed for ferrum-chromium-aluminum electric heating The heater of the flat of metalworking.
7. stirred reactor as claimed in claim 1 it is characterised in that:Flange is passed through on described retort (3) outer wall (51) it is connected with support feet (5), and support feet (5) triangularity arrangement.
8. stirred reactor as claimed in claim 2 it is characterised in that:Described securing member (44) is bolt or screw.
9. stirred reactor as claimed in claim 1 it is characterised in that:Set from the bottom to top on described shaft B (43) It is equipped with two-layer mixing component (431).
10. stirred reactor as claimed in claim 7 it is characterised in that:Described support feet (5) bottom is provided with traveling Wheel (52).
CN201620816886.1U 2016-07-30 2016-07-30 Stirring formula reaction unit Active CN205925689U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620816886.1U CN205925689U (en) 2016-07-30 2016-07-30 Stirring formula reaction unit

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620816886.1U CN205925689U (en) 2016-07-30 2016-07-30 Stirring formula reaction unit

Publications (1)

Publication Number Publication Date
CN205925689U true CN205925689U (en) 2017-02-08

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620816886.1U Active CN205925689U (en) 2016-07-30 2016-07-30 Stirring formula reaction unit

Country Status (1)

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CN (1) CN205925689U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109173813A (en) * 2018-10-10 2019-01-11 南京正宽医药科技有限公司 Dosing agitating device in a kind of production of gel

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109173813A (en) * 2018-10-10 2019-01-11 南京正宽医药科技有限公司 Dosing agitating device in a kind of production of gel

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