CN106732259A - A kind of stirring means of reaction vessel - Google Patents
A kind of stirring means of reaction vessel Download PDFInfo
- Publication number
- CN106732259A CN106732259A CN201611144869.9A CN201611144869A CN106732259A CN 106732259 A CN106732259 A CN 106732259A CN 201611144869 A CN201611144869 A CN 201611144869A CN 106732259 A CN106732259 A CN 106732259A
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- China
- Prior art keywords
- reaction vessel
- stirring means
- little
- jet pump
- liquid
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Stirring will not be produced to wear and tear the invention discloses one kind, materials inside will not be polluted, agitation orientation is more abundant, and effect is more preferable, and low cost, the stirring means of the low reaction vessel of energy consumption.It is directly using the clean gas of the liquid in reaction vessel and outside as carrier, motive power is provided by jet pump, the clean gas of the liquid in reaction vessel and outside are injected into reaction vessel, make to form vortex in reaction vessel, by being vortexed the comprehensive material come in stirred reaction vessel；The clean gas of liquid and outside in described reaction vessel under the driving of jet pump, are cycling in and out reaction vessel interior by circulation loop.
Description
Technical field
The present invention relates to a kind of stirring means of reaction vessel, a kind of synthesis in Chemical Manufacture, dense is specifically referred to
The reactor of contracting, condensation, modified etc. or the stirring means of retort.
Background technology
Reactor is widely used in oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrifying,
The pressure vessel of the technical process such as hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.；Material
Matter typically has carbon manganese steel, stainless steel, zirconium, Ni-based（Kazakhstan, Monel, inconel）Alloy and other composites.Its structure one
As be made up of kettle, transmission device, agitating device, heater, cooling device, sealing device.Corresponding supporting auxiliary equipment：
Still, condenser, water knockout drum, collecting tank, filter etc..
Retort is then a kind of chemical reaction, physical reactions container, and being divided into has pressure vessel and non-pressure vessel.Retort is by pot
Body, pot cover, agitator, chuck, supporting and transmission device, gland seal device etc. are constituted, and material and perforate can be according to the techniques of user
It is required that formulating.Heat form has electrical heating, oil heating, gas heating, water to heat（Or cooling）, open firing etc..Chuck form point
For：Jacket type and outer half cast, chuck oil heating type are designed with guiding device.Whipped form typically have paddle, anchor formula, frame,
Ribbon formula, scraped wall etc..Rotating speed class high has dispersion impeller formula, turbine type, high shear formula, propeller formula, for client according to technique
Selection.Type of belt drive has common electric machine, fire-proof motor, electromagnetic adjustable speed motor, frequency converter etc., and heat exchanger has that cycloidal pin is wheeled, snail
Wheeled, planet electrodeless variable-speed formula.Axle envelope is common water cooling packing seal, the packing seal of combined type tetrafluoro, mechanical seal.Discharging
Form has ball valve, lower exhibition valve.
In two kinds of above-mentioned component parts of common reactant container, agitator is included.Further combined with accompanying drawing 1, no
By being reactor or retort, typically all include tank body 01 and agitator 02, described agitator 02 is if mechanical agitation
Device, then be to connect a poking bar extending into tank body 01 or stirring anchor by mechanical seal 03, then in tool sealing 03
Top reconnects a stirring motor 04 for offer stirring power.If magnetic stirring apparatus, then need to be put into tank body 01
, then be arranged on stirring motor 04 outside tank body by stirring magnetic bead, and the magnet that installation is connected with magnetic bead magnetic force on motor, passes through
Motor belt motor moving magnet rotates, and magnet drives stirring magnetic bead rotation to realize stirring again.
Because the reaction of chemical industry, synthesis, concentration, condensation, it is modified during need to be carried out in reactor or retort
Stirring, to reach the optimum efficiency of technological requirement.The stirring means for using at present, mainly above-mentioned mechanical agitation and magnetic force is stirred
Mix two kinds.The inventor of present patent application is having found that above two method has high energy consumption, easy to wear, contaminated material in practice,
Agitating device is internally rotated, and there is a dead angle in stirring orientation, and rotatable parts, seal are easily worn and produce pollution, nothing
Method reaches the weak points such as the clear production requirement of high purity material.
In sum, one kind is needed at present will not produce stirring to wear and tear, and will not pollute materials inside, and agitation orientation is more filled
Point, effect is more preferable, and low cost, the low new stirring means of energy consumption.
The content of the invention
The technical problem to be solved in the present invention is to provide one kind will not produce stirring to wear and tear, and will not pollute materials inside, stir
Dynamic orientation is more abundant, and effect is more preferable, and low cost, the stirring means of the low reaction vessel of energy consumption.
In order to solve the above technical problems, the technical scheme that the present invention is provided is：A kind of stirring means of reaction vessel, it is straight
The clean gas using the liquid in reaction vessel and outside are connect as carrier, motive power is provided by jet pump, reaction is held
The clean gas of liquid and outside in device are injected into reaction vessel, make to form vortex in reaction vessel, by the full side of vortex
The material that position is come in stirred reaction vessel；The clean gas of liquid and outside in described reaction vessel are existed by circulation loop
Under the driving of jet pump, reaction vessel interior is cycling in and out.
Preferably, described circulation loop be provided with the medium in loop can be heated or operation of being lowered the temperature temperature
Degree control device.
Preferably, described reaction vessel is provided with multiple for injecting injecting a little for liquids and gases, and each is penetrated
The corresponding pipeline of access point is provided with the electric control valve of control piper break-make.
Preferably, the material being additionally provided with described circulation loop for adding materials or changing materials inside is passed in and out and connect
Mouthful.
Preferably, the stir speed (S.S.) in reaction vessel is adjusted by the pump pressure of jet pump
Preferably, each inject at be provided with the electric rotary body that angle is injected for adjust automatically.
Preferably, upper, middle and lower three a little include in described is injected inject a little, be separately positioned on the top of reaction vessel, in
Portion and bottom；Each is injected and be a little also correspondingly arranged on an injection point.
After said structure, the present invention has the advantages that：
1st, original reactor is eliminated（Tank）Machinery（Magnetic force）Agitating device, reduces equipment manufacturing cost, reduces the abrasion of equipment,
The service life of extension device, improves the cleanliness factor of material.
2nd, by the jet pump device of exterior arrangement, liquid and air are constantly infused into reactor（Tank）It is interior, reaction pressure
Power can be adjusted and correct by being pumped.
3rd, liquids and gases can be recycled, can multi-point entrance, can be arbitrarily angled, reach stirring it is more abundant.
4th, liquids and gases can be heated and is lowered the temperature, can also be added new material.
5th, stir speed (S.S.) can be adjusted arbitrarily.
In sum, stirring will not be produced to wear and tear the invention provides one kind, materials inside will not be polluted, agitation orientation is more
Fully, effect is more preferable, and low cost, the stirring means of the low reaction vessel of energy consumption.
Brief description of the drawings
Fig. 1 is the structure schematic diagram of chemical reaction container in the prior art.
Fig. 2 be reaction vessel of the present invention stirring means in corresponding reaction vessel structure schematic diagram.
As shown in the figure：01st, tank body, 02, agitator, 03, mechanical seal, 04, stirring motor, 1, tank body, 2, jet pump, 3,
Circulation loop, 4, jet branch road.
Specific embodiment
The present invention is described in further detail below in conjunction with the accompanying drawings.
With reference to accompanying drawing 2, a kind of stirring means of reaction vessel, it is directly clean with outside using the liquid in reaction vessel
Net gas provides motive power as carrier by jet pump, and the clean gas of the liquid in reaction vessel and outside are injected into
In reaction vessel, make to form vortex in reaction vessel, by being vortexed the comprehensive material come in stirred reaction vessel；Described is anti-
Answer the clean gas of the liquid in container and outside to pass through circulation loop under the driving of jet pump, be cycling in and out in reaction vessel
Portion.
Preferably, described circulation loop be provided with the medium in loop can be heated or operation of being lowered the temperature temperature
Degree control device.
Preferably, described reaction vessel is provided with multiple for injecting injecting a little for liquids and gases, and each is penetrated
The corresponding pipeline of access point is provided with the electric control valve of control piper break-make.
Preferably, the material being additionally provided with described circulation loop for adding materials or changing materials inside is passed in and out and connect
Mouthful.
Preferably, the stir speed (S.S.) in reaction vessel is adjusted by the pump pressure of jet pump
Preferably, each inject at be provided with the electric rotary body that angle is injected for adjust automatically.
Preferably, upper, middle and lower three a little include in described is injected inject a little, be separately positioned on the top of reaction vessel, in
Portion and bottom；Each is injected and be a little also correspondingly arranged on an injection point.
After said structure, the present invention has the advantages that：
1st, original reactor is eliminated（Tank）Machinery（Magnetic force）Agitating device, reduces equipment manufacturing cost, reduces the abrasion of equipment,
The service life of extension device, improves the cleanliness factor of material.
2nd, by the jet pump device of exterior arrangement, liquid and air are constantly infused into reactor（Tank）It is interior, reaction pressure
Power can be adjusted and correct by being pumped.
3rd, liquids and gases can be recycled, can multi-point entrance, can be arbitrarily angled, reach stirring it is more abundant.
4th, liquids and gases can be heated and is lowered the temperature, can also be added new material.
5th, stir speed (S.S.) can be adjusted arbitrarily.
In sum, stirring will not be produced to wear and tear the invention provides one kind, materials inside will not be polluted, agitation orientation is more
Fully, effect is more preferable, and low cost, the stirring means of the low reaction vessel of energy consumption.
The present invention in the specific implementation, a kind of new reaction vessel of structure setting being referred in accompanying drawing 2, without
Mechanical agitation or magnetic stirring apparatus are set in reaction vessel.Tank body 1 and jet pump 2 are constituted into one by circulation loop 3 to follow
Ring, and main line is divided into multiple jet branch roads 4 into branch process is done on the pipeline of tank body 1 in jet pump 2, so can be with
Realize that multiple spot is injected, multi-angle is injected, solve the problems, such as to stir dead angle.While the pressure in order to balance turnover, each is injected a little
It is correspondingly arranged an injection point, the point position that can very easily control to inject and project by electric control valve.Described in addition
Temperature control equipment, preferably, being wound around outside the pipeline of circulation loop, Jie of the inside is heated by heating pipe
Matter, refrigeration is similarly in this way, so can preferably ensure the pure of medium in loop.It should be strongly noted that described
Liquid in reaction vessel refers to reaction solution, and it is to need to participate in reaction, and the clean gas of described outside are optional, tools
User can require to select plus be added without air or add corresponding reacting gas according to specific reaction during gymnastics is made.Existing skill
The patent on reactor or retort disclosed in art has a lot, and some of which is referred to vortex stirring, but this patent
The inventor of application is retrieved after technical scheme shaping, and just the result after retrieval is current by carefully studying discovery
Produce what the method for vortex was still realized by agitator in disclosed patent, realized rather than by jet pump, institute
There is essential distinction with present patent application.And the jet pump that also some patent applications are related in addition, but they are open
Jet pump Main Function be in order to expand the contact area between the gas in reaction vessel and liquid, be not used to provide
Stirring power, that is, used jet pump, but stirring still to be realized by mechanical stirring device.So present patent application is that possess
It is Promethean.
Above to the present invention and embodiments thereof be described, the description does not have restricted, shown in accompanying drawing also only
It is one of embodiments of the present invention, actual structure is not limited thereto.If all in all ordinary skill people of this area
Member is enlightened by it, similar to the technical scheme without designing for creativeness in the case where the invention objective is not departed from
Frame mode and embodiment, protection scope of the present invention all should be belonged to.
Claims (6)
1. a kind of stirring means of reaction vessel, it is characterised in that：It is directly clean with outside using the liquid in reaction vessel
Net gas provides motive power as carrier by jet pump, and the clean gas of the liquid in reaction vessel and outside are injected into
In reaction vessel, make to form vortex in reaction vessel, by being vortexed the comprehensive material come in stirred reaction vessel；Described is anti-
Answer the clean gas of the liquid in container and outside to pass through circulation loop under the driving of jet pump, be cycling in and out in reaction vessel
Portion.
2. stirring means of reaction vessel according to claim 1, it is characterised in that：Described circulation loop is provided with can
Medium in loop is heated or operation of being lowered the temperature temperature control equipment.
3. stirring means of reaction vessel according to claim 1, it is characterised in that：Described reaction vessel is provided with many
It is individual for injecting injecting a little for liquids and gases, and each injects the electrically-controlled valve that a little corresponding pipeline is provided with control piper break-make
Door.
4. stirring means of reaction vessel according to claim 1, it is characterised in that：It is additionally provided with described circulation loop
Material inlet and outlet connectors for adding materials or changing materials inside.
5. stirring means of reaction vessel according to claim 1, it is characterised in that：Stir speed (S.S.) in reaction vessel is led to
The pump pressure for crossing jet pump is adjusted
The stirring means of reaction vessel according to claim 3, it is characterised in that：Each inject at be provided with for
Adjust automatically injects the electric rotary body of angle.
6. stirring means of reaction vessel according to claim 6, it is characterised in that：Described injecting a little includes upper, middle and lower
Three are injected a little, are separately positioned on the upper, middle and lower of reaction vessel；Each is injected and be a little also correspondingly arranged on an injection
Point.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611144869.9A CN106732259A (en) | 2016-12-13 | 2016-12-13 | A kind of stirring means of reaction vessel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611144869.9A CN106732259A (en) | 2016-12-13 | 2016-12-13 | A kind of stirring means of reaction vessel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106732259A true CN106732259A (en) | 2017-05-31 |
Family
ID=58880659
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611144869.9A Pending CN106732259A (en) | 2016-12-13 | 2016-12-13 | A kind of stirring means of reaction vessel |
Country Status (1)
| Country | Link |
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| CN (1) | CN106732259A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108627657A (en) * | 2018-01-18 | 2018-10-09 | 重庆中元汇吉生物技术有限公司 | A kind of liquid path system, immune quantitative analyzer and its control method |
| CN108845154A (en) * | 2018-06-25 | 2018-11-20 | 重庆中元汇吉生物技术有限公司 | A kind of immune quantitative analyzer |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2487222A1 (en) * | 1980-07-23 | 1982-01-29 | Alemany Pierre | Anaerobic digester with pumped recycling mixing system - pref. re-injects surface crust bacteria into digester base to accelerate fermentation |
| KR100679876B1 (en) * | 2005-10-20 | 2007-02-07 | 이영우 | A gas liquefaction-reaction equipment |
| CN1962035A (en) * | 2006-10-30 | 2007-05-16 | 西安交通大学 | Spray cyclone bed type gas liquid solid tri-phase reactor |
| CN202478929U (en) * | 2012-01-16 | 2012-10-10 | 苏州睿枫新材料有限公司 | Stirring device for preparation kettle |
| CN103351043A (en) * | 2013-06-07 | 2013-10-16 | 西安建筑科技大学 | Vortex-type mixing sedimentation integrated reactor |
-
2016
- 2016-12-13 CN CN201611144869.9A patent/CN106732259A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2487222A1 (en) * | 1980-07-23 | 1982-01-29 | Alemany Pierre | Anaerobic digester with pumped recycling mixing system - pref. re-injects surface crust bacteria into digester base to accelerate fermentation |
| KR100679876B1 (en) * | 2005-10-20 | 2007-02-07 | 이영우 | A gas liquefaction-reaction equipment |
| CN1962035A (en) * | 2006-10-30 | 2007-05-16 | 西安交通大学 | Spray cyclone bed type gas liquid solid tri-phase reactor |
| CN202478929U (en) * | 2012-01-16 | 2012-10-10 | 苏州睿枫新材料有限公司 | Stirring device for preparation kettle |
| CN103351043A (en) * | 2013-06-07 | 2013-10-16 | 西安建筑科技大学 | Vortex-type mixing sedimentation integrated reactor |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108627657A (en) * | 2018-01-18 | 2018-10-09 | 重庆中元汇吉生物技术有限公司 | A kind of liquid path system, immune quantitative analyzer and its control method |
| CN108845154A (en) * | 2018-06-25 | 2018-11-20 | 重庆中元汇吉生物技术有限公司 | A kind of immune quantitative analyzer |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170531 |