CN209222104U - A kind of reaction kettle system with automatic temperature control function - Google Patents
A kind of reaction kettle system with automatic temperature control function Download PDFInfo
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- CN209222104U CN209222104U CN201821667956.7U CN201821667956U CN209222104U CN 209222104 U CN209222104 U CN 209222104U CN 201821667956 U CN201821667956 U CN 201821667956U CN 209222104 U CN209222104 U CN 209222104U
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- reaction kettle
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Abstract
The reaction kettle system with automatic temperature control function that the utility model discloses a kind of, including primary reaction kettle, deep reaction kettle and liquid storing barrel, the preliminary mixing of the progress of material and solution in primary reaction kettle, liquid pushing tube is then passed through to enter in deep reaction kettle, it is stirred in deep reaction kettle by the way that setting agitating paddle and arc scraper plate are comprehensive to the mixed solution further progress by initial reaction, deep reaction kettle hull outside spiral surrounding is equipped with heating wire, heat temperature raising quickly can be carried out to mixing liquid, and guarantee the uniformity of mixing liquid temperature, hull outside is additionally provided with water pipe, pass through the effect of cooling water in water pipe, quickly cool down to mixing liquid, realization is rapidly heated and is cooled down to mixing liquid temperature, product after reacted qualification enters liquid storing barrel through efferent duct and is stored.In the utility model reaction kettle system can be realized on-line continuous production, be rapidly heated with fast cooling, be stirred sufficiently.
Description
Technical field
The utility model relates to chemical equipment technical fields, and in particular to a kind of reaction kettle body with automatic temperature control function
System.
Background technique
Reaction kettle is widely used in the fields such as petroleum, chemical industry, rubber, pesticide, dyestuff, medicine, food, be for physics or
The container of chemical reaction, by the design of structure to container and parameter configuration, realize heating, evaporation, cooling that technique requires and
The mixed function of low high speed.
Existing reaction kettle generallys use electrically heated mode and is heated, and can only actively heat, be unable to active cooling.Instead
Answering kettle is usually to be cooled down after heating with natural way, and not only cooling is slow, production efficiency is low, and is not able to satisfy some needs
The production requirement of the product of fast cooling;Meanwhile in on-line continuous production process, needs to spend longer time, wait reaction
Kettle cooling is completed, and just be can be carried out the production of next group product, is affected the production efficiency of enterprise.
Utility model content
Aiming at the problems existing in the prior art, the utility model provide one kind can be realized on-line continuous production, quickly
Heating and fast cooling are stirred the reaction kettle system adequately with automatic temperature control function.
To solve the above-mentioned problems, the utility model uses following technical scheme:
A kind of reaction kettle system with automatic temperature control function, including primary reaction kettle, deep reaction kettle and liquid storing barrel, institute
It states primary reaction kettle lower end and offers liquid outlet, outlet tube is installed at the liquid outlet, the outlet tube is equipped with triple valve
Door, described three-way valve one end are connected with circulation pipe one end, and the circulation pipe other end is connected to primary reaction kettle top,
The three-way valve other end is connected to the first liquid pushing tube, and deep reaction kettle top is communicated with the second liquid pushing tube, and described
Rose Box is equipped between one liquid pushing tube and the second liquid pushing tube, deep reaction kettle lower end passes through efferent duct and the liquid storing barrel phase
Connection, the circulation pipe are equipped with circulating pump, and the liquid pushing tube is equipped with vacuum pump, and the efferent duct is equipped with the first valve,
Control device is equipped on the outside of the deep reaction kettle;
The deep reaction kettle includes shell, and the lateral surface of the shell and bottom are equipped with muff, the muff
Inside be equipped with the second heating wire and cooling tube, second heating wire and the cooling tube are spaced from each other, second heating wire and
The cooling tube is along the shell helically around shape, and second heating wire is electrically connected with control device, the cooling tube
On water inlet be connected by water pump with the water tank for being located at the hull outside, the water outlet on the cooling tube and the water
Case is connected, and second heating wire is electrically connected with the control device;
Second driving motor is installed, the output end of second driving motor is through described at the shell upper end center
Shell and the second rotary shaft are rotatablely connected, and second rotary shaft is located at the inside of the shell, in second rotary shaft
Lower part is equipped with multiple groups agitating paddle, and the agitating paddle is fixed in second rotary shaft by connecting shaft, is opened on the agitating paddle
Equipped with deflector hole, the lower end of the rotary shaft is equipped with arc scraper plate, and protrusion is towards the housing bottom on the arc scraper plate.
Further technical solution, the Rose Box include cabinet, and first liquid pushing tube is connected with the cabinet upper end
Logical, second liquid pushing tube is connected with the cabinet lower end, and the vacuum pump is set on second liquid pushing tube, the case
It is fixedly installed with arc filter plate in vivo, towards the cabinet upper end, the filter plate lower section is equipped with the protrusion of the filter plate
Vibrator, the cabinet two sides are equipped with rewinding pipe, and the rewinding pipe is located above the filter plate, the box inside wall and
Bottom is all provided with having heaters, and the heater is electrically connected with the control device.
It further has technical effect that, by the way that Rose Box is arranged on screen pipe, can be passed through in primary reaction kettle
Solution after crossing initial reaction removes unreacted large granular materials, passes through the drying of heater, enters rewinding Guan Zhongjin
Row recycling, is ground and is utilized again.
Further technical solution, is equipped with temperature sensor in the deep reaction still shell body, the temperature sensor with
The control device electrical connection.
It further has technical effect that, by the temperature in the accurate controlling depth reaction kettle of controller, and then realizes essence
Really control reaction process.
Compared with prior art, the utility model has the following beneficial effects:
The utility model forms a kind of novel reaction kettle system, material by setting primary reaction kettle and deep reaction kettle
With solution in primary reaction kettle be sufficiently mixed and initial reaction, then go through and carry out depth in deep reaction kettle
Reaction;By setting agitating paddle and arc scraper plate to complete by the mixed solution further progress of initial reaction in deep reaction kettle
Orientation is stirred, and promotes reaction efficiency, and deep reaction kettle hull outside spiral surrounding is equipped with heating wire, can be quickly right
Mixing liquid carries out heat temperature raising in deep reaction kettle, and guarantees the uniformity of mixing liquid temperature in reaction kettle, reacts still shell
External side is additionally provided with water pipe, by the effect of cooling water in water pipe, quickly cools down to mixing liquid in reaction kettle, real
Mixing liquid temperature is rapidly heated and is cooled down in existing deep reaction kettle;Product after reacted qualification enters directly into liquid storage
Bucket is stored, and the on-line continuous production of product is realized.
Detailed description of the invention
The utility model is described in further detail with specific embodiment with reference to the accompanying drawing.
Fig. 1 is the primary structure schematic diagram of the utility model embodiment 1;
Fig. 2 is the cross-sectional view of primary reaction kettle in the utility model embodiment 1;
Fig. 3 is the cross-sectional view of deep reaction kettle in the utility model embodiment 1;
Fig. 4 is the top view of deep reaction kettle in the utility model embodiment 1;
Fig. 5 is the primary structure schematic diagram of the utility model embodiment 2;
Fig. 6 is the cross-sectional view of Rose Box in the utility model embodiment 2;
Wherein, specific appended drawing reference is as follows: primary reaction kettle 1, autoclave body 2, the first driving motor 3, and the first rotary shaft 4 is stirred
Mix bar 5, U-shaped scraper plate 6, cleaning brush 7, feed hopper 8, weight analyzer 9, charging baffle 10, adjusting screw rod 11, inlet tube 12, liquid
Fluid meter 13, the second valve 14, inspection liquid pipe 15, third valve 16, muff 17, the first heating wire 18, deep reaction kettle 19,
Shell 20, the second heating wire 21, cooling tube 22, the second driving motor 23, the second rotary shaft 24, agitating paddle 25, connecting shaft 26 are led
Discharge orifice 27, arc scraper plate 28, liquid storing barrel 29, outlet tube 30, three-way valve 31, circulation pipe 32, circulating pump 33, liquid pushing tube 34, the
One liquid pushing tube 35, the second liquid pushing tube 36, vacuum pump 37, Rose Box 38, cabinet 39, arc filter plate 40, vibrator 41, rewinding pipe
42, heater 43, efferent duct 44, the first valve 45, control device 46.
Specific embodiment
Embodiment 1
Referring to figs. 1 to Fig. 4, the present embodiment provides a kind of reaction kettle systems, including primary reaction kettle 1, deep reaction kettle 19
With liquid storing barrel 29,1 lower end of primary reaction kettle offers liquid outlet, and outlet tube 30 is equipped at liquid outlet, and outlet tube 30 is equipped with
Three-way valve 31,31 one end of three-way valve are connected with 32 one end of circulation pipe, and 32 other end of circulation pipe is connected to primary reaction kettle 1
Top, 31 other end of three-way valve are connected to 34 one end of liquid pushing tube, and 34 other end of liquid pushing tube is connected to 19 top of deep reaction kettle, deep
Degree 19 lower end of reaction kettle is connected by efferent duct 44 with liquid storing barrel 29, and circulation pipe 32 is equipped with circulating pump 33, on liquid pushing tube 34
Equipped with vacuum pump 37, efferent duct 44 is equipped with the first valve 45, is equipped with control device 46 on the outside of deep reaction kettle 19.
Primary reaction kettle 1 includes autoclave body 2, is equipped with the first driving motor 3, the first driving motor 3 at 2 upper end center of autoclave body
Output end through autoclave body 2 and the rotation connection of the first rotary shaft 4, the first rotary shaft 4 is located at the inside of autoclave body 2, the first rotary shaft
4 middle and lower part is equipped with multiple groups stirring rod 5, and the lower end of the first rotary shaft 4 is equipped with U-shaped scraper plate 6, U-shaped 6 two sides of scraper plate and bottom outer wall
Multiple cleaning brush 7 are equipped with, cleaning brush 7 fits with 2 inner wall of autoclave body.The right side of 2 upper end of autoclave body is equipped with feed hopper 8, feed hopper 8
Bottom is equipped with weight analyzer 9, and the lower section of feed hopper 8 is equipped with charging baffle 10, and charging 10 one end of baffle, which is articulated with, is located at charging
Struggle against 8 sides 2 upper end of autoclave body inner sidewall on, charging 10 other end of baffle inclination extends at stirring rod 5, on 2 side wall of autoclave body
Equipped with screw thread, adjusting screw rod 11 passes through screw thread and is connected with charging 10 side of baffle.2 one upper lateral part of autoclave body is equipped with inlet tube 12,
Liquid meter 13 and the second valve 14 are successively arranged on inlet tube 12,2 lower part side of autoclave body is equipped with inspection liquid pipe 15, examines liquid pipe 15
It is equipped with third valve 16.2 outside of autoclave body and bottom are equipped with muff 17, and the first heating wire 18 is equipped in muff 17, the
One heating wire 18 is electrically connected with control device 46.
Deep reaction kettle 19 includes shell 20, and the lateral surface of shell 20 and bottom are equipped with muff 17, in muff 17
Equipped with the second heating wire 21 and cooling tube 22, the second heating wire 21 and cooling tube 22 are spaced from each other, the second heating wire 21 and cooling
Pipe 22 is along shell 20 helically around shape, and the second heating wire 21 is electrically connected with control device 46, the water inlet on cooling tube 22
It is connected by water pump with the water tank for being located at 20 outside of shell, the water outlet on cooling tube 22 is connected with water tank, the second electric heating
Silk 21 is electrically connected with control device 46;Second driving motor 23 is installed at 20 upper end center of shell, the second driving motor 23
Output end is rotatablely connected through shell 20 and the second rotary shaft 24, and the second rotary shaft 24 is located at the inside of shell 20, the second rotation
The middle and lower part of axis 24 is equipped with multiple groups agitating paddle 25, and agitating paddle 25 is fixed in the second rotary shaft 24 by connecting shaft 26, agitating paddle
Offer deflector hole 27 on 25, the lower end of rotary shaft is equipped with arc scraper plate 28, and protrusion is towards 20 bottom of shell on arc scraper plate 28
Portion.Temperature sensor is equipped in primary reaction kettle 1 and deep reaction kettle 19, temperature sensor is electrically connected with control device 46.
Embodiment 2
With reference to Fig. 5 and Fig. 6, the present embodiment provides a kind of reaction kettle system, the basic phases of feature of embodiment 2 and embodiment 1
Together, main distinguishing feature is, liquid pushing tube 34 includes the first liquid pushing tube 35 and the second liquid pushing tube 36, the first liquid pushing tube 35 and the
Rose Box 38 is equipped between two liquid pushing tubes 36, Rose Box 38 includes cabinet 39, and the first liquid pushing tube 35 is connected with 39 upper end of cabinet,
Second liquid pushing tube 36 is connected with 39 lower end of cabinet, and vacuum pump 37 is set on the second liquid pushing tube 36, is fixedly mounted in cabinet 39
There is arc filter plate 40, protrusion is equipped with vibrator 41,39 two sides of cabinet towards 39 upper end of cabinet, filter plate lower section on filter plate
It is equipped with rewinding pipe 42, rewinding pipe 42 is located above filter plate, and 39 inner sidewall of cabinet and bottom are all provided with having heaters 43, heats
Device 43 is electrically connected with control device 46.
Use above specific case is illustrated the utility model, is merely used to help understand the utility model, and
Not to limit the utility model.Think of for those skilled in the art of the present invention, according to the utility model
Think, several simple deductions, deformation or replacement can also be made.
Claims (3)
1. a kind of reaction kettle system with automatic temperature control function, which is characterized in that including primary reaction kettle, deep reaction kettle and
Liquid storing barrel, primary reaction kettle lower end offer liquid outlet, and outlet tube is equipped at the liquid outlet, is set on the outlet tube
There is three-way valve, described three-way valve one end is connected with circulation pipe one end, and the circulation pipe other end connection is described primary anti-
Kettle top is answered, the three-way valve other end is connected to the first liquid pushing tube, and deep reaction kettle top is communicated with the second liquor charging
Pipe, is equipped with Rose Box between first liquid pushing tube and the second liquid pushing tube, deep reaction kettle lower end passes through efferent duct and institute
It states liquid storing barrel to be connected, the circulation pipe is equipped with circulating pump, and the liquid pushing tube is equipped with vacuum pump, and the efferent duct is equipped with
First valve, the deep reaction kettle outside are equipped with control device;
The deep reaction kettle includes shell, and the lateral surface of the shell and bottom are equipped with muff, is set in the muff
There are the second heating wire and cooling tube, second heating wire and the cooling tube are spaced from each other, second heating wire and described
Cooling tube is along the shell helically around shape, and second heating wire is electrically connected with control device, on the cooling tube
Water inlet is connected by water pump with the water tank for being located at the hull outside, the water outlet on the cooling tube and the water tank phase
Connection, second heating wire are electrically connected with the control device;
Second driving motor is installed, the output end of second driving motor runs through the shell at the shell upper end center
It is rotatablely connected with the second rotary shaft, second rotary shaft is located at the inside of the shell, the middle and lower part of second rotary shaft
Equipped with multiple groups agitating paddle, the agitating paddle is fixed in second rotary shaft by connecting shaft, is offered on the agitating paddle
Deflector hole, the lower end of the rotary shaft are equipped with arc scraper plate, and protrusion is towards the housing bottom on the arc scraper plate.
2. the reaction kettle system according to claim 1 with automatic temperature control function, which is characterized in that the filtering luggage
Cabinet is included, first liquid pushing tube is connected with the cabinet upper end, and second liquid pushing tube is connected with the cabinet lower end,
The vacuum pump is set on second liquid pushing tube, and arc filter plate is fixedly installed in the cabinet, the filter plate
Protrusion is equipped with vibrator towards the cabinet upper end, the filter plate lower section, and the cabinet two sides are equipped with rewinding pipe, the receipts
Expects pipe is located above the filter plate, and the box inside wall and bottom are all provided with having heaters, the heater and the control
Device electrical connection.
3. the reaction kettle system according to claim 1 with automatic temperature control function, which is characterized in that the deep reaction
Temperature sensor is equipped in still shell body, the temperature sensor is electrically connected with the control device.
Priority Applications (1)
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CN201821667956.7U CN209222104U (en) | 2018-10-15 | 2018-10-15 | A kind of reaction kettle system with automatic temperature control function |
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CN201821667956.7U CN209222104U (en) | 2018-10-15 | 2018-10-15 | A kind of reaction kettle system with automatic temperature control function |
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CN201821667956.7U Expired - Fee Related CN209222104U (en) | 2018-10-15 | 2018-10-15 | A kind of reaction kettle system with automatic temperature control function |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110624491A (en) * | 2019-10-30 | 2019-12-31 | 新疆农业科学院农作物品种资源研究所 | A agitated vessel for preparing seed coating agent |
CN113318679A (en) * | 2021-05-28 | 2021-08-31 | 重庆化工职业学院 | Circulation reaction kettle |
CN113634213A (en) * | 2021-08-10 | 2021-11-12 | 安徽广信农化股份有限公司 | Preparation process of sulfonyl isocyanate with high conversion rate |
CN113983757A (en) * | 2021-12-23 | 2022-01-28 | 常州铭赛机器人科技股份有限公司 | Constant temperature module and stock preparation barrel with same |
CN114870440A (en) * | 2022-06-15 | 2022-08-09 | 徐州隆仕达新材料科技研究院有限公司 | Defoaming agent for water-based adhesive |
CN117427585A (en) * | 2023-12-21 | 2024-01-23 | 技源集团股份有限公司 | Reaction device for producing HMB-Ca |
-
2018
- 2018-10-15 CN CN201821667956.7U patent/CN209222104U/en not_active Expired - Fee Related
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110624491A (en) * | 2019-10-30 | 2019-12-31 | 新疆农业科学院农作物品种资源研究所 | A agitated vessel for preparing seed coating agent |
CN113318679A (en) * | 2021-05-28 | 2021-08-31 | 重庆化工职业学院 | Circulation reaction kettle |
CN113634213A (en) * | 2021-08-10 | 2021-11-12 | 安徽广信农化股份有限公司 | Preparation process of sulfonyl isocyanate with high conversion rate |
CN113983757A (en) * | 2021-12-23 | 2022-01-28 | 常州铭赛机器人科技股份有限公司 | Constant temperature module and stock preparation barrel with same |
CN114870440A (en) * | 2022-06-15 | 2022-08-09 | 徐州隆仕达新材料科技研究院有限公司 | Defoaming agent for water-based adhesive |
CN117427585A (en) * | 2023-12-21 | 2024-01-23 | 技源集团股份有限公司 | Reaction device for producing HMB-Ca |
CN117427585B (en) * | 2023-12-21 | 2024-02-27 | 技源集团股份有限公司 | Reaction device for producing HMB-Ca |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190809 Termination date: 20211015 |
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CF01 | Termination of patent right due to non-payment of annual fee |