CN205786054U - Quadruple safeguard protection High Temperature High Pressure digestion system - Google Patents

Quadruple safeguard protection High Temperature High Pressure digestion system Download PDF

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Publication number
CN205786054U
CN205786054U CN201620563909.2U CN201620563909U CN205786054U CN 205786054 U CN205786054 U CN 205786054U CN 201620563909 U CN201620563909 U CN 201620563909U CN 205786054 U CN205786054 U CN 205786054U
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CN
China
Prior art keywords
colorimetric pool
pipeline
high temperature
colorimetric
polytetrafluoro
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620563909.2U
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Chinese (zh)
Inventor
冯中宝
徐生龙
赵峰
李军
孙潮
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong Sirui Environmental Equipment Technology Co Ltd
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Shandong Sirui Environmental Equipment Technology Co Ltd
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Priority to CN201620563909.2U priority Critical patent/CN205786054U/en
Application granted granted Critical
Publication of CN205786054U publication Critical patent/CN205786054U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of quadruple safeguard protection High Temperature High Pressure digestion system, it relates to High Temperature High Pressure and clears up technical field.Lower electromagnetic valve, solenoid is respectively by lower polytetrafluoro pipeline, upper polytetrafluoro pipeline is connected with colorimetric pool, two pipe ends of lower polytetrafluoro pipeline are fixed on lower electromagnetic valve by pipe joint respectively, on the lower end of colorimetric pool, two pipe ends of upper polytetrafluoro pipeline are fixed on the upper end of colorimetric pool respectively by pipe joint, on solenoid, pipe joint and lower polytetrafluoro pipeline, it is mounted on clip on the pipeline that upper polytetrafluoro pipeline connects, colorimetric pool is fixed in colorimetric pool mounting seat by mounting blocks under colorimetric pool, the upper end of colorimetric pool is provided with colorimetric pool compact heap, colorimetric pool compact heap matches with rustless steel holddown spring and housing screw, Temperature sampler is installed on colorimetric pool.This utility model realizes High Temperature High Pressure and clears up test, it is ensured that colorimetric pool will not cause blast because of high temperature, and safety is high, reliable and stable.

Description

Quadruple safeguard protection High Temperature High Pressure digestion system
Technical field
The utility model relates to High Temperature High Pressure and clear up technical field, be specifically related to quadruple safeguard protection High Temperature High Pressure and disappear Solution system.
Background technology
It is that one can decompose indissoluble physical means that High Temperature High Pressure is cleared up, can be used for atomic absorption spectrum, environment measuring etc. from Molten sample pretreatment in the analysis such as sub-transmitting, it can also be used to the synthetic reaction of low dose, is also with strong acid or highly basic in tank body And high temperature high pressure enclosed environment reaches the purpose of rapid-digestion indissoluble material;Colorimetric is to use spectrophotography test material A kind of method of content, is usually used in the instrument detection of on-line monitoring.
Owing to the reagent cleared up in test process is often for concentrated acid or concentrated base, as a example by COD in digestion process, then colorimetric Mixed liquor in pond is the mixed liquor of 50% concentrated sulphuric acid, and the digestion condition of COD is more than 165 DEG C, and the pressure in digestion pool can reach 4.3 atmospheric pressure, if safeguard protection do not in place, the most once temperature controls to lose efficacy, it will explode, and owing to clearing up In the concentrated sulphuric acid that reagent is High Temperature High Pressure, the most often cause the irremediable loss of instrument, if safety devices are not in place, May threaten to personal safety.
In order to solve the problems referred to above, designing that a kind of novel quadruple safeguard protection High Temperature High Pressure digestion system has the most very much must Want.
Utility model content
For not enough present on prior art, this utility model purpose is to be to provide a kind of quadruple safeguard protection high temperature High-pressure digestion system, simple in construction, reasonable in design, it is achieved High Temperature High Pressure clears up test, it is ensured that colorimetric pool will not be led because of high temperature Causing blast, safety is high, reliable and stable, it is easy to promote the use of.
To achieve these goals, this utility model is to realize by the following technical solutions: quadruple safeguard protection is high Temperature high-pressure digestion system, including under clip, pipe joint, the lower electromagnetic valve of high-temperature high-pressure corrosion resisting, lower polytetrafluoro pipeline, colorimetric pool Mounting blocks, colorimetric pool mounting seat, colorimetric pool, Temperature sampler, colorimetric pool compact heap, holddown spring, housing screw, upper polytetrafluoro Pipeline and the solenoid of corrosion-resistant usual pressure, lower electromagnetic valve, solenoid are respectively by lower polytetrafluoro pipeline, upper polytetrafluoro Pipeline is connected with colorimetric pool, and two pipe ends of lower polytetrafluoro pipeline are fixed on lower electromagnetic valve, colorimetric pool by pipe joint respectively On lower end, two pipe ends of upper polytetrafluoro pipeline are fixed on the upper end of colorimetric pool, solenoid by pipe joint respectively, and pipe connects Being mounted on clip on the pipeline that head is connected with lower polytetrafluoro pipeline, upper polytetrafluoro pipeline, colorimetric pool is by installing under colorimetric pool Block is fixed in colorimetric pool mounting seat, and the upper end of colorimetric pool is provided with colorimetric pool compact heap, colorimetric pool compact heap and rustless steel pressure Tight spring and housing screw match, and colorimetric pool is provided with Temperature sampler.
As preferably, the upper port of described colorimetric pool, lower port are smooth port sealing structure, in order to avoid leaking gas, leaking, leaking Acid, upper port, lower port are respectively arranged with o-ring, lower o-ring, and upper o-ring, lower o-ring all use fluorubber ring, protect Card can permanently effective operation under high temperature and high pressure environment.
As preferably, described Temperature sampler uses Pt100 Temperature sampler, Temperature sampler and PLC acquisition module Coupling, PLC is heated by PID temperature control realization, exception, system automatic alarm once occurs.
As preferably, described colorimetric pool is quartz glass colorimetric pool, and colorimetric pool is welded with multiple spherical protuberances shape Semicircular ring, semicircular ring is also made for quartz glass, and semicircular ring is wound with heater strip, in order to heater strip can preferably be attached to high temperature On high-pressure digestion colorimetric device.
As preferably, under described colorimetric pool, mounting blocks, colorimetric pool compact heap all use politef to make, to ensure The safety of system and usability.
The beneficial effects of the utility model: the design structure of quadruple safeguard protection ensure that colorimetric pool will not be led because of high temperature The blast caused, safety is high, good stability, and reliable and practical, and service life is longer.
Accompanying drawing explanation
This utility model is described in detail below in conjunction with the accompanying drawings with detailed description of the invention;
Fig. 1 is structural representation of the present utility model.
Detailed description of the invention
For the technological means making this utility model realize, creation characteristic, reach purpose and be easy to understand with effect, below In conjunction with detailed description of the invention, this utility model is expanded on further.
With reference to Fig. 1, this detailed description of the invention by the following technical solutions: quadruple safeguard protection High Temperature High Pressure digestion system, Including mounting blocks 5, ratio under clip 1, pipe joint 2, the lower electromagnetic valve 3 of high-temperature high-pressure corrosion resisting, lower polytetrafluoro pipeline 4, colorimetric pool Color pond mounting seat 6, colorimetric pool 7, Temperature sampler 8, colorimetric pool compact heap 9, holddown spring 10, housing screw 11, upper polytetrafluoro The solenoid 13 of pipeline 12 and corrosion-resistant usual pressure, lower electromagnetic valve 3, solenoid 13 respectively by lower polytetrafluoro pipeline 4, Upper polytetrafluoro pipeline 12 is connected with colorimetric pool 7, and two pipe ends of lower polytetrafluoro pipeline 4 are fixed on lower electricity by pipe joint 2 respectively Magnet valve 3, colorimetric pool 7 lower end on, two pipe ends of upper polytetrafluoro pipeline 12 are fixed on colorimetric pool 7 by pipe joint 2 respectively On upper end, solenoid 13, the pipeline that pipe joint 2 is connected with lower polytetrafluoro pipeline 4, upper polytetrafluoro pipeline 12 is mounted on card Hoop 1, colorimetric pool 7 is fixed in colorimetric pool mounting seat 6 by mounting blocks 5 under colorimetric pool, and the upper end of colorimetric pool 7 is provided with colorimetric pool Compact heap 9, colorimetric pool compact heap 9 matches with holddown spring 10 and housing screw 11, colorimetric pool 7 is provided with Temperature sampler 8。
It should be noted that the upper port of described colorimetric pool 7, lower port are smooth port sealing structure, in order to avoid gas leakage, leakage Water, leakage acid, upper port, lower port are respectively arranged with o-ring 15, lower o-ring 14, and upper o-ring 15, lower o-ring 14 are all adopted Use fluorubber ring, it is ensured that can permanently effective operation under high temperature and high pressure environment.
It should be noted that described colorimetric pool 7 uses quartz glass, there is light transmission strong, it is possible to achieve 190nm- The light of 1000nm passes through, and has and can repeatedly heat and the feature such as high-temperature high-pressure corrosion resisting, and acid and alkali-resistance can be with resistance to 200 degree 98% Concentrated sulphuric acid, it is ensured that add sulphuric acid and reagent mixing post-heating and do not burst to 200 degree;It is welded with multiple spherical prominent on colorimetric pool 7 Playing the semicircular ring of shape, semicircular ring is also made for quartz glass, and semicircular ring is wound with heater strip, in order to heater strip can preferably paste Clear up on colorimetric device in High Temperature High Pressure.
It should be noted that mounting blocks 5 under described colorimetric pool, colorimetric pool compact heap 9 all use politef to make, To ensure safety and the usability of system.
Additionally, described colorimetric pool mounting seat 6 uses the structure of integration, save the set-up time in a large number, simplify peace Dress step, reduces the deviation caused because disparate modules assembles.
This detailed description of the invention has quadruple safety protection function: wherein, and ground floor protection is Temperature sampler 8, temperature Harvester 8 uses Pt100 Temperature sampler, Temperature sampler 8 to couple with PLC acquisition module, and PLC controls real by PID temperature Now heating, in heating and digestion process, once system is heated beyond the regular hour, and system can automatic alarm.
Second layer protection is holddown spring 10, and holddown spring 10 is high-strength stainless steel spring, this spring and housing screw 11 coordinate, and well coordinate realizing pressure with the pressure of colorimetric pool, to reach the purpose of safeguard protection, when housing screw 11 is twisted During to bottom, the pressure of the holddown spring 10 calculated according to Hooke's law is higher than the pressure of 180 DEG C less than colorimetric pool temperature, If i.e. the heating-up temperature in colorimetric pool 7 is more than 180 DEG C, holddown spring 10 can automatically open up pressure release.
Third layer protection is the solenoid 13 of corrosion-resistant usual pressure, and this electromagnetic valve customizes according to demand, i.e. colorimetric pool 7 Temperature more than 178 DEG C when, solenoid 13 is backed down by air pressure automatically, thus realizes self-relieving purpose.
4th layer of protection for clip 1, when the temperature of colorimetric pool 7 more than 200 DEG C when, the pressure conduction of whole system arrives Pipeline, then thrust is higher than the kilocalorie power of clip 1 design, and pipeline Automatic-falling discharges pressure, quick-fried to ensure that system does not haves Fried.
This detailed description of the invention High Temperature High Pressure in on-line computing model test process clears up test, not only can clear up but also can For colorimetric, unique quadruple protection structure so that during clearing up, once occur that temperature control is out of control, also have its excess-three Individual safe relief passage, this ensure that the blast that colorimetric pool will not cause because of high temperature, protects instrument and equipment, ensures person peace Entirely, there is wide market application foreground.
Of the present utility model ultimate principle and principal character and of the present utility model advantage have more than been shown and described.One's own profession Skilled person will appreciate that of industry, this utility model is not restricted to the described embodiments, described in above-described embodiment and description Principle of the present utility model is simply described, on the premise of without departing from this utility model spirit and scope, this utility model is also Have various changes and modifications, in the range of these changes and improvements both fall within claimed this utility model.This utility model Claimed scope is defined by appending claims and equivalent thereof.

Claims (5)

1. quadruple safeguard protection High Temperature High Pressure digestion system, it is characterised in that include clip (1), pipe joint (2), High Temperature High Pressure Mounting blocks (5), colorimetric pool mounting seat (6), colorimetric pool under corrosion resistant lower electromagnetic valve (3), lower polytetrafluoro pipeline (4), colorimetric pool (7), Temperature sampler (8), colorimetric pool compact heap (9), holddown spring (10), housing screw (11), upper polytetrafluoro pipeline (12) With the solenoid (13) of corrosion-resistant usual pressure, lower electromagnetic valve (3), solenoid (13) are respectively by lower polytetrafluoro pipeline (4), upper polytetrafluoro pipeline (12) be connected with colorimetric pool (7), two pipe ends of lower polytetrafluoro pipeline (4) pass through pipe joint respectively (2) being fixed on the lower end of lower electromagnetic valve (3), colorimetric pool (7), two pipe ends of upper polytetrafluoro pipeline (12) are connect by pipe respectively Head (2) is fixed on the upper end of colorimetric pool (7), solenoid (13), pipe joint (2) and lower polytetrafluoro pipeline (4), upper polytetrafluoro Being mounted on clip (1) on the pipeline that pipeline (12) connects, colorimetric pool (7) is fixed on colorimetric by mounting blocks (5) under colorimetric pool In pond mounting seat (6), the upper end of colorimetric pool (7) is provided with colorimetric pool compact heap (9), colorimetric pool compact heap (9) and rustless steel pressure Tight spring (10) and housing screw (11) match, and colorimetric pool (7) is provided with Temperature sampler (8).
Quadruple safeguard protection High Temperature High Pressure digestion system the most according to claim 1, it is characterised in that described colorimetric pool (7) upper port, lower port are smooth port sealing structure, and upper port, lower port are respectively arranged with o-ring (15), lower O Type ring (14), upper o-ring (15), lower o-ring (14) all use fluorubber ring.
Quadruple safeguard protection High Temperature High Pressure digestion system the most according to claim 1, it is characterised in that described temperature is adopted Storage (8) uses Pt100 Temperature sampler, and Temperature sampler (8) couples with PLC acquisition module.
Quadruple safeguard protection High Temperature High Pressure digestion system the most according to claim 1, it is characterised in that described colorimetric pool (7) it is quartz glass colorimetric pool, colorimetric pool (7) is welded with the semicircular ring of multiple spherical protuberances shape, semicircular ring is wound with and adds Heated filament.
Quadruple safeguard protection High Temperature High Pressure digestion system the most according to claim 1, it is characterised in that described colorimetric pool Lower mounting blocks (5) is politef mounting blocks, and colorimetric pool compact heap (9) is politef compact heap.
CN201620563909.2U 2016-06-13 2016-06-13 Quadruple safeguard protection High Temperature High Pressure digestion system Expired - Fee Related CN205786054U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620563909.2U CN205786054U (en) 2016-06-13 2016-06-13 Quadruple safeguard protection High Temperature High Pressure digestion system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620563909.2U CN205786054U (en) 2016-06-13 2016-06-13 Quadruple safeguard protection High Temperature High Pressure digestion system

Publications (1)

Publication Number Publication Date
CN205786054U true CN205786054U (en) 2016-12-07

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111323547A (en) * 2020-04-09 2020-06-23 国家电网有限公司 GIS air chamber decomposition object detection device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111323547A (en) * 2020-04-09 2020-06-23 国家电网有限公司 GIS air chamber decomposition object detection device

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161207

Termination date: 20190613