CN205759821U - A kind of crystallization apparatus - Google Patents

A kind of crystallization apparatus Download PDF

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Publication number
CN205759821U
CN205759821U CN201620094132.XU CN201620094132U CN205759821U CN 205759821 U CN205759821 U CN 205759821U CN 201620094132 U CN201620094132 U CN 201620094132U CN 205759821 U CN205759821 U CN 205759821U
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CN
China
Prior art keywords
chamber
vaporization chamber
separation chamber
vaporization
crystallization apparatus
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620094132.XU
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Chinese (zh)
Inventor
沈建钢
曾青峰
冯顶文
郑金锋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Shengfu Chemical Co Ltd
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Jiangxi Shengfu Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangxi Shengfu Chemical Co Ltd filed Critical Jiangxi Shengfu Chemical Co Ltd
Priority to CN201620094132.XU priority Critical patent/CN205759821U/en
Application granted granted Critical
Publication of CN205759821U publication Critical patent/CN205759821U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of crystallization apparatus, including vaporization chamber, circulation pipe and separation chamber, circulation pipe one end is connected with vaporization chamber, the other end is connected with separation chamber, connect on circulation pipe and have heating chamber and circulating pump, the top of heating chamber and vaporization chamber is respectively equipped with solar energy heating plate and scrapes brilliant device, is provided with seed crystal holder outside separation chamber, and seed crystal holder is connected with separation chamber by connecting tube;Scraping brilliant device and include rotating shaft and the connecting rod being arranged in vaporization chamber, rotating shaft lower end is connected with connecting rod, the two ends of connecting rod be provided with contact with vaporization chamber inwall scrape crystalline substance plate.The beneficial effects of the utility model: arranged after scraping brilliant device by the top of vaporization chamber, can effectively prevent the inwall of vaporization chamber from crystal fouling condition occurring, by arranging seed crystal holder outside separation chamber and connecting seed crystal holder and the connecting tube of separation chamber, control to add crystal seed quantity, the crystal grain produced in making separation chamber is uniform, and the anti-caking performance of crystal is strong.

Description

A kind of crystallization apparatus
Technical field
This utility model relates to crystallization technique field, it particularly relates to a kind of crystallization apparatus.
Background technology
The process that crystal is formed in the solution is referred to as crystallization.The method of crystallization typically has 2 kinds: one is evaporation solvent method, It is applicable to temperature to the dissolubility little material of impact, and " evaporating brine " in coastal area be exactly this method of utilization, and another kind is Cooling down hot saturated solution method, this method is applicable to temperature and raises, the material that dissolubility also increases.Evaporation solvent, makes solution by insatiable hunger With become saturated, continue evaporation, superfluous solute will separate out in crystal, is evaporative crystallization.
The patent disclosure of Application No. 201520611294.1 has gone out a kind of solar heating evaporation crystallizer, including evaporation Room, separation chamber, circulation pipe, circulating pump, heating chamber, described vaporization chamber bottom is located in separation chamber, and described circulation pipe connects Heating chamber, separation chamber and vaporization chamber, described circulating pump is located on circulation pipe, and described bottom, separation chamber is provided with discharging opening, institute The vaporization chamber top stated is provided with vapor outlet port, and described heating chamber is rectangular structure, and described heating chamber top is provided with the sun Energy heating plate, described evaporation chamber top is provided with defecator.This solar heating evaporation crystallizer in use, steams The inwall sending out room there will be the situation of fouling, and cleaning inconvenience after time length, additionally, due to product moisture content is high, in separation chamber Glomerocryst many time easily lump, crystalline particle is little.
For the problem in correlation technique, effective solution is the most not yet proposed.
Utility model content
The purpose of this utility model is to provide a kind of crystallization apparatus, to overcome currently available technology above shortcomings.
For realizing above-mentioned technical purpose, the technical solution of the utility model is achieved in that
A kind of crystallization apparatus, including vaporization chamber and circulation pipe, be arranged on vaporization chamber lower end and be connected with vaporization chamber point From room, described circulation pipe one end is connected with vaporization chamber, and the other end is connected with separation chamber, and described circulation pipe connects heating Room and circulating pump, described heating chamber top is provided with solar energy heating plate, and the top of described vaporization chamber is provided with scrapes brilliant device, described point Be provided with the seed crystal holder that can add crystal seed from outdoor, described seed crystal holder is connected with the internal cavities of separation chamber by connecting tube Logical;Described scrape brilliant device include rotating shaft and the connecting rod being arranged in vaporization chamber, described rotating shaft lower end extend into vaporization chamber interior and Be connected with the connecting rod in vaporization chamber, the two ends of described connecting rod be provided with contact with vaporization chamber inwall scrape brilliant plate.
Further, described connecting tube is provided with control valve.
Further, described separation chamber is provided with inclined plane, and is provided with visual window in this inclined plane.
Further, the top of described vaporization chamber is eccentrically provided with vapor outlet line, and this vapor outlet line one end extend into steaming Send out indoor and connection has defecator.
Further, scrape brilliant device described in and be located at the center, top of separation chamber.
Further, the bottom of described separation chamber is provided with discharging opening, and this discharge outlet is provided with blow-off valve.
The beneficial effects of the utility model: arranged by the top of vaporization chamber after scraping brilliant device, it is possible to effectively prevent from steaming There is crystal fouling condition, by arranging seed crystal holder outside separation chamber and connecting seed crystal holder and separation chamber in the inwall sending out room Connecting tube, control to add crystal seed quantity, make the crystal grain that produces in separation chamber uniformly, the anti-caking performance of crystal is strong.
Accompanying drawing explanation
In order to be illustrated more clearly that this utility model embodiment or technical scheme of the prior art, below will be to embodiment The accompanying drawing used required in is briefly described, it should be apparent that, the accompanying drawing in describing below is the most of the present utility model Some embodiments, for those of ordinary skill in the art, on the premise of not paying creative work, it is also possible to according to this A little accompanying drawings obtain other accompanying drawing.
Fig. 1 is the structural representation according to the crystallization apparatus described in this utility model embodiment.
In figure:
1, vaporization chamber;2, circulation pipe;3, separation chamber;4, heating chamber;5, circulating pump;6, solar energy heating plate;7, crystal seed holds Device;8, connecting tube;9, rotating shaft;10, connecting rod;11, brilliant plate is scraped;12, control valve;13, inclined plane;14, visual window;15, steam Outlet;16, defecator;17, discharging opening;18, blow-off valve.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is carried out Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of this utility model rather than whole Embodiment.Based on the embodiment in this utility model, all other embodiments that those of ordinary skill in the art are obtained, all belong to Scope in this utility model protection.
As it is shown in figure 1, according to a kind of crystallization apparatus described in embodiment of the present utility model, including vaporization chamber 1 and circulation Pipe 2, is arranged on vaporization chamber 1 lower end and the separation chamber 3 being connected with vaporization chamber 1, and described circulation pipe 2 one end is connected with vaporization chamber 1 Logical, the other end is connected with separation chamber 3, and described circulation pipe 2 connects heating chamber 4 and circulating pump 5, described heating chamber 4 top Being provided with solar energy heating plate 6, the top of described vaporization chamber 1 is provided with scrapes brilliant device, and outside being provided with in described separation chamber 3 can add crystal seed Seed crystal holder 7, described seed crystal holder 7 is connected by the internal cavities of connecting tube 8 with separation chamber 3;Described scrape brilliant device bag Include rotating shaft 9 and the connecting rod 10 being arranged in vaporization chamber 1, in described rotating shaft 9 lower end extend into vaporization chamber 1 and with in vaporization chamber 1 Connecting rod 10 be connected, the two ends of described connecting rod 10 be provided with contact with vaporization chamber 1 inwall scrape brilliant plate 11.
Described connecting tube 8 is provided with control valve 12, and then can effectively control addition.
Described separation chamber 3 is provided with inclined plane 13, and is provided with visual window 14 in this inclined plane 13, convenient observation separation chamber Crystallization situation in 3.
The top of described vaporization chamber 1 is eccentrically provided with vapor outlet line 15, and this vapor outlet line 15 one end extend into vaporization chamber 1 Interior and connection has defecator 16.
Described crystalline substance device of scraping is located at the center, top of separation chamber 3.
The bottom of described separation chamber 3 is provided with at discharging opening 17, and this discharging opening 17 and is provided with blow-off valve 18.
Understand technique scheme of the present utility model for convenience, below by way of new to this practicality in specifically used mode The technique scheme of type is described in detail.
When specifically used, operationally, described rotating shaft 9 rotates described vaporization chamber 1, thus is driven by connecting rod 10 again Described crystalline substance plate 11 of scraping rotates, and can effectively prevent the inwall of described vaporization chamber 1 from crystal fouling occur, simultaneously by described crystal seed Container 7 adds crystal seed in described separation chamber 3, and the crystal grain produced in described separation chamber 3 is uniform.
In sum, by means of technique scheme of the present utility model, arranged by the top of vaporization chamber 1 and scrape brilliant device After, it is possible to effectively prevent the inwall of vaporization chamber 1 from crystal fouling condition occurring, by arranging seed crystal holder 7 outside separation chamber 3 With the connecting tube 8 connecting seed crystal holder 7 and separation chamber 3, control to add crystal seed quantity, the crystal grain produced in making separation chamber 3 Uniformly, the anti-caking performance of crystal is strong.
The foregoing is only preferred embodiment of the present utility model, not in order to limit this utility model, all at this Within the spirit of utility model and principle, any modification, equivalent substitution and improvement etc. made, should be included in this utility model Protection domain within.

Claims (6)

1. a crystallization apparatus, including vaporization chamber (1) and circulation pipe (2), be arranged on vaporization chamber (1) lower end and with vaporization chamber (1) The separation chamber (3) being connected, described circulation pipe (2) one end is connected with vaporization chamber (1), and the other end is connected with separation chamber (3), The upper connection of described circulation pipe (2) has heating chamber (4) and circulating pump (5), and described heating chamber (4) top is provided with solar energy heating plate (6), it is characterised in that the top of described vaporization chamber (1) is provided with scrapes brilliant device, and described separation chamber (3) outside being provided with can add crystalline substance The seed crystal holder (7) planted, described seed crystal holder (7) is connected by the internal cavities of connecting tube (8) with separation chamber (3);Described Scraping brilliant device and include rotating shaft (9) and the connecting rod (10) being arranged in vaporization chamber (1), described rotating shaft (9) lower end extend into evaporation In room (1) and being connected with the connecting rod (10) in vaporization chamber (1), the two ends of described connecting rod (10) are provided with and vaporization chamber (1) What inwall contacted scrapes brilliant plate (11).
Crystallization apparatus the most according to claim 1, it is characterised in that described connecting tube (8) is provided with control valve (12).
Crystallization apparatus the most according to claim 1, it is characterised in that described separation chamber (3) are provided with inclined plane (13), and This inclined plane (13) is provided with visual window (14).
Crystallization apparatus the most according to claim 1, it is characterised in that the top of described vaporization chamber (1) is eccentrically provided with steam Outlet (15), this vapor outlet line (15) one end extend in vaporization chamber (1) and connects defecator (16).
Crystallization apparatus the most according to claim 1, it is characterised in that described in scrape brilliant device and be located at the top of separation chamber (3) Center.
Crystallization apparatus the most according to claim 1, it is characterised in that the bottom of described separation chamber (3) is provided with discharging opening , and this discharging opening (17) place is provided with blow-off valve (18) (17).
CN201620094132.XU 2016-01-30 2016-01-30 A kind of crystallization apparatus Expired - Fee Related CN205759821U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620094132.XU CN205759821U (en) 2016-01-30 2016-01-30 A kind of crystallization apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620094132.XU CN205759821U (en) 2016-01-30 2016-01-30 A kind of crystallization apparatus

Publications (1)

Publication Number Publication Date
CN205759821U true CN205759821U (en) 2016-12-07

Family

ID=57413843

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620094132.XU Expired - Fee Related CN205759821U (en) 2016-01-30 2016-01-30 A kind of crystallization apparatus

Country Status (1)

Country Link
CN (1) CN205759821U (en)

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161207

Termination date: 20180130