CN205627872U - Saponin ring -opening reaction kettle device - Google Patents
Saponin ring -opening reaction kettle device Download PDFInfo
- Publication number
- CN205627872U CN205627872U CN201620447497.6U CN201620447497U CN205627872U CN 205627872 U CN205627872 U CN 205627872U CN 201620447497 U CN201620447497 U CN 201620447497U CN 205627872 U CN205627872 U CN 205627872U
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- CN
- China
- Prior art keywords
- reactor
- saponin
- reation kettle
- wall
- controller
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
The utility model discloses a saponin ring -opening reaction kettle device, the control unit comprises a reaction vessel, reation kettle's inner chamber bottom is equipped with temperature sensor, reation kettle's inner chamber top central point puts and is equipped with the axis of rotation, the motor passes through the rotor and links to each other with the axis of rotation, be equipped with the puddler on the outer wall of axis of rotation, reation kettle's bottom is equipped with the backup pad, the bottom of backup pad is equipped with the support frame, the left side of support frame is equipped with the vacuum pump, the top of vacuum pump is equipped with pipeline, pipeline runs through reation kettle's outer wall. This saponin ring -opening reaction kettle device can put into reation kettle to the material through the feed inlet, and passing through liquids charge -in pipeline can drop into reation kettle to the liquid of reaction, can detect whether reach the vacuum in the reation kettle through the vacuum test ware, and the air bleed in reation kettle goes out through the vacuum pump, becomes vacuum reation kettle device with reation kettle, boiling point lowering when making the reaction, effectively energy -conservation.
Description
Technical field
This utility model relates to reactor technical field, and a kind of reactor for Saponin open loop fills
Put.
Background technology
Steroidal compounds is the important natural organic-compound of class being widely present in animal and plant body, plants
Class is various, the most all has important physiological action, and the steroid drugs that success has been developed is not only widely used in be controlled
Treat rheumatism, cardiovascular diseases, cancer, dermatosis, endocrine disturbance, male prostatic hyperplasia, old age
Property disease, and in family planning and to produce the aspect such as immunosuppressant be also indispensable, it is three big
A most important class, China's kind in major hormone drug type prostaglandin, peptide hormone, steroid hormone
Planting abundant natural plants Dioscorea zingiberensis, Folium Agaves Sisalanae and Dioscorea nipponica Mak. Ningpo Yam Rhizome is to produce coming of steroid hormone class medicine basic material
Source, plant Saponin mainly has three major types, i.e. diosgenin, tigogenin, hecogenin, is to produce steroid
The optimal basic material of body hormonal medicaments, the steroid hormone medicine of more than 2/3rds is with soap in the world
Element makees what basic material produced, so being synthesized dehydropregnenolone acetate, monoene alcohol ketone acetic acid by Saponin
The important intermediate of the synthesizing steroid hormone medicines such as ester, tool is of great significance, in order to improve money
The availability of source property native compound steroidal and affluent resources chemical content, we are synthesized alkene by Saponin at research
The technique of alcohol acetate also improves industrialization efficiency, the such as patent of Patent No. 201420690259.9,
Including reactor main body, reacting kettle jacketing, reactor body exterior is provided with reacting kettle jacketing, and reactor presss from both sides
Set is built with conduction oil, and as electrical heating medium, reactor main body includes cylinder body, discharge nozzle, though
So it is heated rapidly, and ladder-elevating temperature can be controlled, but uneven when material and liquid mixing.
Utility model content
The purpose of this utility model is to provide a kind of reactor device for Saponin open loop, on solving
State the problem proposed in background technology.
For achieving the above object, this utility model provides following technical scheme: a kind of for Saponin open loop
Reactor device, including reactor, the outer wall of described reactor is provided with controller, described controller bag
Including control panel and display, the right side of described control panel is provided with display, the left side of described reactor
Outer wall upper end is provided with charging aperture, and the outer right wall upper end of described reactor is provided with liquid feedstock pipeline, described
Charging aperture is all connected with lid by connecting pin with liquid feedstock pipeline, the lower end of described liquid feedstock pipeline
Being provided with discharging opening, the top of described reactor is provided with motor, and described controller is electrically connected with motor, institute
The inner side stating reactor is provided with resistive heater, and described controller is electrically connected with resistive heater, described
The inner chamber bottom of reactor is provided with temperature sensor, and described controller is electrically connected with temperature sensor, institute
The internal chamber wall stating reactor is provided with vacuum detector, and described controller is electrically connected with vacuum detector,
The inner chamber top dead center position of described reactor is provided with rotary shaft, and described motor passes through rotor and rotary shaft phase
Even, the outer wall of described rotary shaft is provided with puddler, and the bottom of described reactor is provided with gripper shoe, described
The bottom of gripper shoe is provided with bracing frame, and support frame as described above runs through gripper shoe and is connected with reactor, described support
The left side of frame is provided with vacuum pump, and described controller is electrically connected with vacuum pump, and the top of described vacuum pump sets
Conveyance conduit, described conveyance conduit is had to run through the outer wall of reactor.
Preferably, the left and right sides of described reactor is equipped with protective plate.
Preferably, the bottom of support frame as described above is provided with protective base.
Preferably, the bottom of described motor is provided with cushion.
Preferably, the outer wall of described puddler is provided with ultrasonic vibrator, described controller and ultrasound wave
Vibrator is electrically connected with.
Preferably, the inner side of described lid is provided with sealing ring.
Compared with prior art, the beneficial effects of the utility model are: this is used for the reactor of Saponin open loop
Device, can put into reactor material by charging aperture, can be reaction by liquid feedstock pipeline
Liquid puts in reactor, by lid, charging aperture and liquid feedstock pipeline is sealed, thus reactor
Reach the state sealed, whether reach vacuum in reactor can being detected by vacuum detector, by very
Empty pump emits the air in reactor, reactor becomes vacuum response kettle device, when making reaction
Boiling point reduce, it is possible to the most energy-conservation, rotated by driven by motor rotary shaft, thus rotary shaft drive stir
Mix bar to rotate, make the material in reactor stir uniformly, can be added to reactor by resistive heater
Heat, can sense the temperature in reactor by temperature sensor, and the conversion ratio making Saponin open loop is high, instead
Shorten between Ying Shi, Quality advance.
Accompanying drawing explanation
Fig. 1 is this utility model structural representation；
Fig. 2 is reactor sectional structure schematic diagram of the present utility model.
In figure: 1, reactor, 2, controller, 201, control panel, 202, display, 3, discharging
Mouthful, 4, gripper shoe, 5, protective base, 6, bracing frame, 7, vacuum pump, 8, conveyance conduit, 9,
Charging aperture, 10, lid, 11, cushion, 12, motor, 13, sealing ring, 14, liquid feed pipe
Road, 15, protective plate, 16, resistive heater, 17, vacuum detector, 18, rotary shaft, 19, super
Sonic wave vibrator, 20, puddler, 21, temperature sensor.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, to the technology in this utility model embodiment
Scheme is clearly and completely described, it is clear that described embodiment is only this utility model one
Divide embodiment rather than whole embodiments.Based on the embodiment in this utility model, this area is common
The every other embodiment that technical staff is obtained under not making creative work premise, broadly falls into this
The scope of utility model protection.
Fig. 1-2, a kind of technical scheme of this utility model offer: a kind of reaction for Saponin open loop are provided
Kettle device, including reactor 1, the outer wall of described reactor 1 is provided with controller 2, described controller 2
Including control panel 201 and display 202, the right side of described control panel 201 is provided with display 202,
The outer wall upper end, left side of described reactor 1 is provided with charging aperture 9, and the outer right wall upper end of described reactor 1 sets
Having liquid feedstock pipeline 14, described charging aperture 9 and liquid feedstock pipeline 14 are all by connecting pin and lid
10 are connected, and the inner side of described lid 10 is provided with sealing ring 13, can be with charging aperture 9 He by sealing ring 10
Liquid feedstock pipeline 14 is tighter with the connection of lid 10, and the lower end of described liquid feedstock pipeline 14 is provided with
Discharging opening 3, makes the top of described reactor 1 be provided with motor 12, and described controller 2 is electrical with motor 12
Connecting, the bottom of described motor 12 is provided with cushion 10, can make minimizing motor 12 by cushion 10
Vibration, the inner side of described reactor 1 is provided with resistive heater 16, described controller 2 with add thermal resistance
Silk 16 is electrically connected with, and the inner chamber bottom of described reactor 1 is provided with temperature sensor 21, described controller 2
Being electrically connected with temperature sensor 21, the internal chamber wall of described reactor 1 is provided with vacuum detector 17, institute
Stating controller 2 to be electrically connected with vacuum detector 17, the left and right sides of described reactor 1 is equipped with protection
Plate 15, the outer wall being possible to prevent reactor 1 by protective plate 15 is overheated, scald staff, described instead
The inner chamber top dead center position answering still 1 is provided with rotary shaft 18, and described motor 12 is by rotor and rotary shaft
18 are connected, and the outer wall of described rotary shaft 18 is provided with puddler 20, and the outer wall of described puddler 20 sets
Having ultrasonic vibrator 19, described controller 2 is electrically connected with ultrasonic vibrator 19, passes through ultrasound wave
Vibrator 19 can make material stirring evenly, and the bottom of described reactor 1 is provided with gripper shoe 4, institute
The bottom stating gripper shoe 4 is provided with bracing frame 6, and support frame as described above 6 runs through gripper shoe 4 and is connected with reactor 1,
The bottom of support frame as described above 6 is provided with protective base 5, bracing frame 6 can be made more stable by protective base 5
Support reactor 1, the left side of support frame as described above 6 is provided with vacuum pump 7, described controller 2 and vacuum pump
7 are electrically connected with, and the top of described vacuum pump 7 is provided with conveyance conduit 8, and described conveyance conduit 8 runs through reaction
The outer wall of still 1.
During use, material is put in reactor 1, by liquid feedstock pipeline 14 by charging aperture 9
The liquid of reaction can be put in reactor 1, by 10 charging apertures 9 of lid and liquid feedstock pipeline
14 seal, thus reactor 1 reaches the state of sealing, can detect reaction by vacuum detector 17
Whether reach vacuum in still 1, control the air in 7 reactors 1 of vacuum pump by controller 2 and discharge
Go out, reactor 1 is become vacuum response still 1 device, make boiling point during reaction reduce, it is possible to effectively
Energy-conservation, drive rotary shaft 18 to rotate by motor 12, thus rotary shaft 18 drives puddler 20 to rotate,
Make the material in reactor 1 stir uniformly, heat to reactor 1 by resistive heater 16,
The temperature in reactor 1 can be sensed by temperature sensor 21.
Embodiment the most of the present utility model, for the ordinary skill people of this area
For Yuan, it is possible to understand that can be real to these in the case of without departing from principle of the present utility model and spirit
Executing example to carry out multiple change, revise, replace and modification, scope of the present utility model is by claims
And equivalent limits.
Claims (6)
1. for the reactor device of Saponin open loop, including reactor, it is characterised in that: described instead
The outer wall answering still is provided with controller, and described controller includes control panel and display, described operation control surface
The right side of plate is provided with display, and the outer wall upper end, left side of described reactor is provided with charging aperture, described reactor
Outer right wall upper end be provided with liquid feedstock pipeline, described charging aperture and liquid feedstock pipeline all by connect
Pin is connected with lid, and the lower end of described liquid feedstock pipeline is provided with discharging opening, and the top of described reactor sets
Having motor, described controller to be electrically connected with motor, the inner side of described reactor is provided with resistive heater,
Described controller is electrically connected with resistive heater, and the inner chamber bottom of described reactor is provided with temperature sensor,
Described controller is electrically connected with temperature sensor, and the internal chamber wall of described reactor is provided with vacuum detector,
Described controller is electrically connected with vacuum detector, and the inner chamber top dead center position of described reactor is provided with and turns
Moving axis, described motor is connected with rotary shaft by rotor, and the outer wall of described rotary shaft is provided with puddler,
The bottom of described reactor is provided with gripper shoe, and the bottom of described gripper shoe is provided with bracing frame, support frame as described above
Running through gripper shoe to be connected with reactor, the left side of support frame as described above is provided with vacuum pump, and described controller is with true
Empty pump is electrically connected with, and the top of described vacuum pump is provided with conveyance conduit, and described conveyance conduit runs through reactor
Outer wall.
A kind of reactor device for Saponin open loop the most according to claim 1, it is characterised in that:
The left and right sides of described reactor is equipped with protective plate.
A kind of reactor device for Saponin open loop the most according to claim 1, it is characterised in that:
The bottom of support frame as described above is provided with protective base.
A kind of reactor device for Saponin open loop the most according to claim 1, it is characterised in that:
The bottom of described motor is provided with cushion.
A kind of reactor device for Saponin open loop the most according to claim 1, it is characterised in that:
The outer wall of described puddler is provided with ultrasonic vibrator, and described controller electrically connects with ultrasonic vibrator
Connect.
A kind of reactor device for Saponin open loop the most according to claim 1, it is characterised in that:
The inner side of described lid is provided with sealing ring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620447497.6U CN205627872U (en) | 2016-05-17 | 2016-05-17 | Saponin ring -opening reaction kettle device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620447497.6U CN205627872U (en) | 2016-05-17 | 2016-05-17 | Saponin ring -opening reaction kettle device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205627872U true CN205627872U (en) | 2016-10-12 |
Family
ID=57057100
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620447497.6U Expired - Fee Related CN205627872U (en) | 2016-05-17 | 2016-05-17 | Saponin ring -opening reaction kettle device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205627872U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108508935A (en) * | 2017-05-18 | 2018-09-07 | 太仓东诚塑胶有限公司 | Intelligent work temperature regulating device |
| CN108912208A (en) * | 2018-06-20 | 2018-11-30 | 南京肽业生物科技有限公司 | A kind of adjustable Solid-phase synthesis peptides device of temperature |
-
2016
- 2016-05-17 CN CN201620447497.6U patent/CN205627872U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108508935A (en) * | 2017-05-18 | 2018-09-07 | 太仓东诚塑胶有限公司 | Intelligent work temperature regulating device |
| CN108912208A (en) * | 2018-06-20 | 2018-11-30 | 南京肽业生物科技有限公司 | A kind of adjustable Solid-phase synthesis peptides device of temperature |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161012 Termination date: 20170517 |