CN205590711U - But apparatus for producing of biological enzyme is retrieved to magnetism suitable for industrialization is used - Google Patents
But apparatus for producing of biological enzyme is retrieved to magnetism suitable for industrialization is used Download PDFInfo
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- CN205590711U CN205590711U CN201620441873.0U CN201620441873U CN205590711U CN 205590711 U CN205590711 U CN 205590711U CN 201620441873 U CN201620441873 U CN 201620441873U CN 205590711 U CN205590711 U CN 205590711U
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- service sink
- pipeline
- separating still
- reactor
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Abstract
The utility model discloses a but apparatus for producing of biological enzyme is retrieved to magnetism suitable for industrialization is used, the control unit comprises a reaction vessel, cauldron body upper portion is equipped with feed inlet, retrieval and utilization biological enzyme solution entry, and there is the export of mixed liquid the lower part, and the export links to each other with the separation cauldron, and the lower part of separation cauldron has the pipeline to pass through the plastic pump to link to each other with reation kettle, and another export simultaneously links to each other through plastic pump and clean water basin. All there is a powerful electro -magnet lower part of separation cauldron and clean water basin, but produces strong magnetism after the circular telegram and retrieve the biological enzyme catalyst to the magnetism that obtains and carry out magnetic force and retrieve, reaches quickly separating's purpose, makes catalyst and liquid separation quickening processing. Linking to each other with the separation cauldron of pipeline and plastic pump is passed through on the upper portion of clean water basin. The utility model discloses a but the device can be used for magnetic force to retrieve the industrial production of catalyst itself, but also can be used to use in the industry other industrial production devices of magnetic force recovery, repeatedly usable's catalyst.
Description
Technical field
This utility model belongs to Catalyst Production technical field, be specifically related to a kind of be applicable to industrial applications can magnetic recovery raw
The process units of thing enzyme.
Background technology
Enzyme, as biocatalyzer, has the distinguishing features such as selectivity is high, catalytic condition is gentle, pollution-free, has been developed wide
General it is applied to the industries such as food processing, medicine, weaving and fine chemistry industry.The use of enzyme is typically under free state with weak solution
Form and substrate carry out catalytic reaction, be difficult to after react reclaim enzyme, the most preferably use in tank reactor, throw in batches
Put, relatively costly.Native enzyme poor stability simultaneously, easy in inactivation, it is impossible to reuse, and the isolated and purified difficulty of product, make
It is difficult to large-scale application in Industrial Catalysis.In recent years, improve the stability of enzyme by immobilization and reuse number of times
Become the focus of research.Being combined with some insoluble macromolecular carrier by enzyme, form immobilized enzyme, its advantage is the company of may be constructed
Continuous operation, can use in stirred reactor, fixed bed reactors or the fluidized-bed reactor of flowing continuously.After immobilization often
Can improve the stability of enzyme, some occasion also can improve vigor.But, the recycling of supported biological enzyme agent is still
Face the problem how separated from reaction system, may often be such that and operate along with the unit such as filtering or centrifugal, cause the damage of enzyme
Losing and even inactivate, regeneration effect causes anxiety.
Nano magnetic material, as preferable enzyme carrier, has the performance not available for conventional material so that its potential application
Extremely advantageous, for nano magnetic material and the immobilized application aspect research work of enzyme oneself through being no longer limited to single
Section and single research method, but the comprehensive utilization of multidisciplinary and multiple research method.By surface-functionalized to magnetic particle,
Making enzyme the most immobilized on magnetic carrier with enzyme generation chemical coupling effect after functionalization, magnetic carrier is efficient with it
Magnetic action, it is simple to reclaim after a procedure.Although have at present can the small-sized preparation facilities of magnetic recovery enzyme, but due to life
Thing enzyme is the bioactive substance such as protein or polypeptide, poor stability, easy in inactivation, thus this device be limited only within laboratory or
The preparation of a small amount of enzyme, there is presently no and be applicable to industrialized production or reclaim the device of enzyme.
Utility model content
The purpose of this utility model is contemplated to solve the problems referred to above, it is provided that a kind of be applicable to industrial applications can magnetic recovery raw
The process units of thing enzyme, can effectively prepare can magnetic recovery immobilized biological enzyme agent.
To achieve these goals, this utility model adopts the following technical scheme that
A kind of be applicable to industrial applications can the process units of magnetic recovery enzyme, including politef reactor, separation
Still and service sink,
Described politef reactor top arranges feed(raw material)inlet and the first pipeline, and described politef reactor is by described
First pipeline is connected with described separating still sidewall, and described politef reactor bottom is by second pipe with separating still top even
Connect, inside described politef reactor, agitator is set；
Arranging electric magnet bottom described separating still, described separating still bottom is connected with described service sink top by the 4th pipeline, institute
The top stating separating still is connected with the sidewall of service sink by the 3rd pipeline；
Described service sink top arranges clear water entrance, and described service sink upper portion side wall arranges wastewater outlet, and described service sink bottom sets
Put products export, electric magnet is set bottom described service sink, in described service sink, agitator is set；
Valve is all set on described first, second, third and fourth pipeline, described first and third, four pipelines all arrange plastic pump.
Preferably: described service sink bottom is arranged products export and is connected with pan tank by the 5th pipeline.
Preferably: the top of described separating still arranges upper cover, cover on described and there is the hole that second and third pipeline passes through.
Preferably: described pipeline is high-performance PVC (polyvinyl chloride) pipe.
Preferably: the shell of described reactor is supported on support.
Preferably: described service sink is square, the top of described service sink arranges upper cover, described on cover and there is the 4th pipeline pass through
Hole and clear water entrance.
Preferably: described reactor, separating still and service sink use polytetrafluoroethylmaterial material, advantage: effectively prevent magnetic bio enzyme
The attachment of catalyst, increases the fluency of conveying.
Separating still and clear water reserviors top, with cover plate, prevent from spattering outside liquid and other foreign matter entrance inside.
Above-mentioned device is produce can application in magnetic recovery material.
A kind of based on said apparatus industrialized production can the method for magnetic recovery enzyme,
(1) finished product magnetic carrier and coupling agent are joined in reactor, add enzyme solution, reacted by stirring；
(2) after having reacted, open the valve on the second pipe of reactor, make reacted mixing liquid enter separating still；
(3) by bottom described reactor Magnet be energized, make the magnetic bio enzyme in mixed liquor be attracted, make magnetic bio enzyme with
Solution separating, the liquid after separation pumps into reactor by the plastic pump on described first pipeline, the magnetic bio enzyme of isolated
Service sink is pumped into by the pump on the 4th pipeline；
(4) in service sink, clear water is pumped into, stirring and washing, pumped into distinguishing water in the middle part of service sink point by the pump on the 4th pipeline
In still, the magnetic bio enzyme catalyst in separating still is made to be transferred into clear water reserviors completely；
(5) being energized by the Magnet bottom described service sink, the waste water after cleaning is discharged.
Preferably: the magnetic bio enzyme after described method also includes (6) cleaning has pump to squeeze into pan tank.
The beneficial effects of the utility model:
What process units of the present utility model may be used for industrialized production can the catalyst that reclaims of magnetic force and carrier material large-scale
Device, it is possible to achieve Kg even tonne other production, can realize can reclaiming fast separating of catalyst, tool by magnetic force efficiently
There is a simple in construction, small investment, easy to maintenance, it is ensured that to run well for a long time.Can efficiently be prepared on a large scale magnetic bio enzyme
Catalyst.When industrialized production, immobilized after enzymatic solution can apply mechanically, it is achieved circulation reduces waste, so having very well
Economy.
The pump that this utility model is used is all plastic pump, and the part passed through at material is all made up of polytetrafluoroethylplastic plastic.Subtract
Few superincumbent adhesion of magnetic bio enzyme catalyst.
The bottom of service sink also is provided with a strong electromagnet, and the convenient magnetic separation to the magnetic bio enzyme in cleaning process reclaims,
Reduce the loss in cleaning process.
Accompanying drawing explanation
Fig. 1 is the structural representation of this utility model process units；
Wherein, 1. reactor, 2. separating still, 3. electric magnet, 4. the first pipeline, 5. second pipe, 6. clear water reserviors, 7. the 4th pipeline,
8. the 3rd pipeline, 9. clear water entrance, 10. wastewater outlet, 11. the 5th pipelines, 12. products exports, 13. agitators.
Detailed description of the invention
The utility model is described in further detail with embodiment below in conjunction with the accompanying drawings.
As it is shown in figure 1, a kind of be applicable to industrial applications can the process units of magnetic recovery enzyme, including politef
Reactor 1, separating still 2 and service sink 6, described politef reactor 1 top arranges feed(raw material)inlet and the first pipeline 4,
Described politef reactor 1 is connected with described separating still 2 sidewall by described first pipeline 4, and described politef is anti-
Answering still 1 bottom to be connected with separating still 2 top by second pipe 5, described politef reactor 1 is internal arranges agitator
13；
Arranging electric magnet 3 bottom described separating still 2, described separating still 2 bottom is pushed up with described service sink 6 by the 4th pipeline 7
Portion connects, and the top of described separating still 2 is connected with the sidewall of service sink 6 by the 3rd pipeline 8；
Described service sink 6 top arranges clear water entrance 9, and described service sink 6 upper portion side wall arranges wastewater outlet 10, described cleaning
Bottom, pond 6 arranges products export 12, arranges electric magnet 3, arrange agitator 13 in described service sink 6 bottom described service sink 6；
Valve is all set on described first, second, third and fourth pipeline, described first and third, four pipelines all arrange plastic pump.
Described service sink 6 bottom is arranged products export 12 and is connected with pan tank by the 5th pipeline 11.
The top of described separating still 2 arranges upper cover, described on cover there is the hole that second and third pipeline passes through.
Described pipeline is high-performance PVC (polyvinyl chloride) pipe.
The shell of described reactor is supported on support.
Described service sink 6 is square, and the top of described service sink 6 arranges upper cover, described on cover and there is the 4th pipeline 7 pass through
Hole and clear water entrance 9.
Described reactor 1, separating still 2 and service sink 6 use polytetrafluoroethylmaterial material.
The work process of said apparatus is as follows:
During use, finished product magnetic carrier is dissolved in buffer solution, prepares certain density coupling agent, and certain density biology
Enzyme is sent in reactor 1 by feed(raw material)inlet, starts agitator 13 and starts reaction.The reaction regular hour, reacted mixing
Liquid is entered in separating still in 2 by second pipe 5.Open the power supply of electric magnet 3 bottom separating still 2, make electric magnet 3
Energizing magnetic, makes the magnetic bio enzyme catalyst in mixing liquid and unreacted enzyme solution separating, the life after separation
Thing enzymatic solution is squeezed in reactor 1 by plastic pump, the adsorbed biological enzyme agent in bottom after stopping electric magnet 3 energising,
Squeezed in clear water reserviors 6 by plastic pump.In separating still 2, the magnetic bio enzyme catalyst of isolated cleans in clear water reserviors 6,
Being sent in separating still 2 by part clear water by plastic pump, cleaning part remains in the magnetic bio enzyme catalysis in separating still 2 simultaneously
Agent, cleans and makes for three times magnetic bio enzyme catalyst all proceed in service sink 6, after cleaning, open the electromagnetism bottom service sink 6
The power supply of ferrum 3, makes electric magnet 3 produce strong magnetic, attracts the biological enzyme agent obtained.Supernatant is beaten by plastic pump
Return in separating still 2, turnover.Bottom magnetic bio enzyme catalyst after the magnetic removing electric magnet 3 by being pumped into pan tank,
Carry out subsequent treatment and obtain finished product.
Although detailed description of the invention of the present utility model is described by the above-mentioned accompanying drawing that combines, but not this utility model is protected
The restriction of scope, one of ordinary skill in the art should be understood that on the basis of the technical solution of the utility model, art technology
Personnel need not to pay various amendments or deformation that creative work can make still within protection domain of the present utility model.
Claims (7)
1. be applicable to industrial applications can the process units of magnetic recovery enzyme, it is characterized in that: include politef
Reactor, separating still and service sink；Described politef reactor top arranges feed(raw material)inlet and the first pipeline, and described poly-four
Fluorothene reactor is connected with described separating still sidewall by described first pipeline, and described politef reactor bottom passes through the
Two pipelines are connected with separating still top, arrange agitator inside described politef reactor；Bottom described separating still, electricity is set
Magnet, described separating still bottom is connected with described service sink top by the 4th pipeline, and the top of described separating still is by the 3rd pipe
Road is connected with the sidewall of service sink；Described service sink top arranges clear water entrance, and described service sink upper portion side wall arranges wastewater outlet,
Described service sink bottom arranges products export, arranges electric magnet, arrange agitator in described service sink bottom described service sink；Institute
State and valve is all set on first, second, third and fourth pipeline, described first and third, four pipelines all arrange plastic pump.
2. device as claimed in claim 1, is characterized in that: described service sink bottom arrange products export by the 5th pipeline with
Pan tank connects.
3. device as claimed in claim 1, is characterized in that: the top of described separating still arranges upper cover, described on cover and have
The hole that second and third pipeline passes through.
4. device as claimed in claim 1, is characterized in that: the shell of described reactor is supported on support.
5. device as claimed in claim 1, is characterized in that: described service sink is square, and the top of described service sink is arranged
Lid, described on cover there is hole and the clear water entrance that the 4th pipeline passes through.
6. device as claimed in claim 1, is characterized in that: described reactor, separating still and service sink use politef
Material.
7. device as claimed in claim 1, is characterized in that: described pipeline is high-performance PVC (polyvinyl chloride) pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620441873.0U CN205590711U (en) | 2016-05-13 | 2016-05-13 | But apparatus for producing of biological enzyme is retrieved to magnetism suitable for industrialization is used |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620441873.0U CN205590711U (en) | 2016-05-13 | 2016-05-13 | But apparatus for producing of biological enzyme is retrieved to magnetism suitable for industrialization is used |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205590711U true CN205590711U (en) | 2016-09-21 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620441873.0U Expired - Fee Related CN205590711U (en) | 2016-05-13 | 2016-05-13 | But apparatus for producing of biological enzyme is retrieved to magnetism suitable for industrialization is used |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105861307A (en) * | 2016-05-13 | 2016-08-17 | 山东师范大学 | Production device of magnetically-recyclable biological enzymes suitable for industrialized application |
-
2016
- 2016-05-13 CN CN201620441873.0U patent/CN205590711U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105861307A (en) * | 2016-05-13 | 2016-08-17 | 山东师范大学 | Production device of magnetically-recyclable biological enzymes suitable for industrialized application |
| CN105861307B (en) * | 2016-05-13 | 2018-08-28 | 山东师范大学 | Suitable for industrial applications can magnetic recovery biological enzyme process units |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160921 Termination date: 20170513 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |