CN205287636U - Recovery unit of volatile solvent - Google Patents
Recovery unit of volatile solvent Download PDFInfo
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- CN205287636U CN205287636U CN201521003354.8U CN201521003354U CN205287636U CN 205287636 U CN205287636 U CN 205287636U CN 201521003354 U CN201521003354 U CN 201521003354U CN 205287636 U CN205287636 U CN 205287636U
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- vaporizer
- retracting device
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- alembic
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Abstract
The utility model discloses a recovery unit of volatile solvent belongs to the chemical industry equipment field. This recovery unit includes evaporimeter, heating pipe, condensation water source, circulating pipe, retort, condenser pipe, honeycomb duct, closed waste liquid collecting barrel. Wherein, the evaporimeter is built -in to be filled with heating medium, and the heating pipe setting is in the evaporimeter for heat heating medium, the retort is placed among the heating medium in the evaporimeter. The condenser pipe comprises inner core pipe and water -cooled tube, the import of inner core pipe and the side pipe sealing connection of retort, the export of inner core pipe and the imported sealing connection of honeycomb duct, the export and the closed waste liquid collecting barrel sealing connection of honeycomb duct. Simultaneously, water -cooled tube, circulating pipe, condensation water source are connected in order, form the condensation unit. The utility model discloses a recovery unit, it is whole to the ground evaporation of organic solvent closed with retrieve, rather than in directly discharging the atmosphere, effectively guaranteed the volatile solvent and can have been retrieved safely, its easy operation, recovery efficiency height.
Description
Technical field
This utility model relates to field of chemical equipment, particularly to the retracting device of a kind of volatile solvent.
Background technology
In organic chemical industry's laboratory, such as, in oilfield chemistry laboratory, volatile organic solvent is generally adopted to carry out various experimentation, and after experiment terminates, shown in the disposal options of volatile organic solvent is generally as follows: reaction residual solvent is placed in uncovered reaction bulb, then utilize oil bath or water-bath that this reaction bulb is heated in fume hood, make that volatile organic solvent is uncovered to be evaporated. Above-mentioned method of disposal can referring to " in SY/T7550-2012 crude oil wax, colloid, asphalt content algoscopy ".
But, utilizing aforesaid operations, volatile organic solvent is disposed, not only need to use rubber pipette bulb constantly to purge reaction bottleneck, complex operation, and the organic solvent being evaporated will be directly discharged in air, easily causing environmental pollution, also easily sucked by operator simultaneously, infringement operator's is healthy.
In order to solve as above problem, it is necessary to provide a kind of device that volatile solvent is reclaimed, this device can not only make volatile organic solvent be reclaimed safely, rather than it is directly discharged in air, and use this device to reclaim organic solvent, and simple to operate, there is higher organic efficiency.
Utility model content
This utility model embodiment technical problem to be solved is in that, it is provided that a kind of retracting device that can reclaim volatile organic solvent safely and efficiently. Concrete technical scheme is as follows:
A kind of retracting device of volatile solvent, described retracting device includes vaporizer, adds heat pipe, condensation water, circulating water pipe, alembic, condensing tube, mozzle, closed waste collection bucket;
Be filled with heating medium in described vaporizer, described in add heat pipe and be arranged in described vaporizer, for the described thermal medium that adds is heated, described alembic is placed on and adds in thermal medium in described vaporizer,
Described condensing tube is made up of inner core tube and water cooling tube, the side pipe of the import of described inner core tube and described alembic is tightly connected, the outlet of described inner core tube is connected with the inlet seal of described mozzle, and the outlet of described mozzle and described closed waste collection bucket are tightly connected;Described water cooling tube, described circulating water pipe, described condensation water are sequentially connected with, to form condensing unit.
Further, described retracting device also includes temperature control and display, hygrosensor;
Described hygrosensor is arranged on described heating media interior, is used for adding described in measuring the temperature of thermal medium;
Described temperature controls and display is arranged on described vaporizer outer wall, add heat pipe with described simultaneously and described hygrosensor electrically connects, for receiving and show the temperature data measured by described hygrosensor, according to the control of described temperature data, add the heating-up temperature of heat pipe simultaneously.
As preferably, being provided with hold-down support in described vaporizer, it is used for placing described alembic.
As preferably, described vaporizer is cuboid structure, is arranged below lift supporting leg at two ends, described vaporizer left and right, for regulating the height of described vaporizer.
As preferably, the number of described alembic and described condensing tube is at least one;
The described water cooling tube of all described condensing tubes is communicated with each other by multiple described circulating water pipes, to share described condensation water;
The import of the described inner core tube of each described condensing tube connects an independent described alembic respectively, and confluxed by described mozzle in the exit of described inner core tube, and it is tightly connected by the described mozzle after confluxing and described closed waste collection bucket.
As preferably, described condensing tube is serpentine condenser.
As preferably, by using the caulking gum head with central through hole to realize being tightly connected between the import of described inner core tube and the side pipe of described alembic, and realizing being tightly connected between outlet and the described closed waste collection bucket of described mozzle.
Specifically, as preferably, being additionally provided with circulating pump in described vaporizer, described in being used for circulating, add thermal medium.
The technical scheme that this utility model embodiment provides has the benefit that
The retracting device of the volatile solvent that this utility model embodiment provides, by using vaporizer at a suitable temperature the liquid containing organic solvent in alembic to be heated, condensation in making organic solvent volatilization form steam and enter the inner core tube of condensing tube, is entered in closed waste collection bucket by mozzle after one-tenth liquid to be condensed and reclaims. Visible, that this utility model embodiment provides retracting device, to organic solvent by whole process is evaporated and reclaims, rather than being directly discharged in air with carrying out closed, and being effectively ensured volatile solvent can be reclaimed safely, and can recycle. And, utilize this retracting device to reclaim volatile organic solvent, simple to operate, and there is higher organic efficiency.
Accompanying drawing explanation
In order to be illustrated more clearly that the technical scheme in this utility model embodiment, below the accompanying drawing used required during embodiment is described is briefly described, apparently, accompanying drawing in the following describes is only embodiments more of the present utility model, for those of ordinary skill in the art, under the premise not paying creative work, it is also possible to obtain other accompanying drawing according to these accompanying drawings.
Fig. 1 is retracting device first structural representation of the volatile solvent that this utility model embodiment provides;
Fig. 2 is retracting device second structural representation of the volatile solvent that the another embodiment of this utility model provides.
Accompanying drawing labelling represents respectively:
1 vaporizer,
2 add heat pipe,
3 condensation waters,
4 circulating water pipes,
5 alembics,
6 condensing tubes,
7 mozzles,
8 closed waste collection buckets,
9 temperature control and display,
10 hold-down supports,
11 caulking gum heads,
12 lift supporting legs.
Detailed description of the invention
For making the purpose of this utility model, technical scheme and advantage clearly, below in conjunction with accompanying drawing, this utility model embodiment is described in further detail.
As shown in accompanying drawing 1 and accompanying drawing 2, this utility model embodiment provides the retracting device of a kind of volatile solvent, and this retracting device includes vaporizer 1, adds heat pipe 2, condensation water 3, circulating water pipe 4, alembic 5, condensing tube 6, mozzle 7, closed waste collection bucket 8. Wherein, being filled with heating medium in vaporizer 1, add heat pipe 2 and be arranged in vaporizer 1, for being heated adding thermal medium, alembic 5 is placed on adding in thermal medium in vaporizer 1.
Condensing tube 6 is made up of inner core tube and water cooling tube, and the side pipe of the import of inner core tube and alembic 5 is tightly connected, and the outlet of inner core tube is connected with the inlet seal of mozzle 7, and the outlet of mozzle 7 and closed waste collection bucket 8 are tightly connected. Meanwhile, water cooling tube, circulating water pipe 4, condensation water 3 are sequentially connected with, to form condensing unit.
The retracting device of the volatile solvent that this utility model embodiment provides, by using vaporizer 1 at a suitable temperature the liquid containing organic solvent in alembic 5 to be heated, condensation in making organic solvent volatilization form steam and enter the inner core tube of condensing tube 6, is entered in closed waste collection bucket 8 by mozzle 7 after one-tenth liquid to be condensed and reclaims. Visible, that this utility model embodiment provides retracting device, to organic solvent by whole process is evaporated and reclaims, rather than being directly discharged in air with carrying out closed, and being effectively ensured volatile solvent can be reclaimed safely, and can recycle. And, utilize this retracting device to reclaim volatile organic solvent, simple to operate, and there is higher organic efficiency.
It is understandable that, in the retracting device that this utility model embodiment provides, by making water cooling tube, circulating water pipe 4, condensation water 3 be sequentially connected with, to ensure to realize circulating chilled water in the annular space between the inner core tube and water cooling tube of condensing tube 6, so that the organic vapor of volatilization is condensed into liquid.
Further, in order to improve the operability of this retracting device, reducing manpower output, as shown in Figure 2, the retracting device that this utility model embodiment provides also includes temperature control and display 9, hygrosensor. Wherein, hygrosensor is arranged on heating media interior, for measuring the temperature adding thermal medium; Temperature controls and display 9 is arranged on vaporizer 1 outer wall, simultaneously with add heat pipe 2 and hygrosensor electrically connect, for the temperature data received and measured by displays temperature detector, add the heating-up temperature of heat pipe 2 according to temperature data control simultaneously. By as set above, to realize the controllability of this retracting device heating system, it is ensured that the temperature adding thermal medium in vaporizer 1 is in the volatilization point of organic solvent all the time. Further, in this vaporizer 1, it is additionally provided with circulating pump, for circulating-heating medium, so that the Temperature Distribution adding thermal medium is more uniform, and then ensures that multiple alembics 5 are heated evenly and temperature is identical when using multiple alembic 5.
Further, this utility model embodiment is provided with hold-down support 10 in vaporizer 1, is used for placing alembic 5, so that the bottle portion of alembic 5 is fully and stably inserted adds thermal medium, for instance water or in oil. For example, the support arm on this hold-down support 10 sidewall that can to include annular bracing ring relative with being arranged on this annular bracing ring, and the end of two support arms is separately fixed on the sidewall of vaporizer 1.
Specifically, in the retracting device that this utility model embodiment provides, vaporizer 1, in cuboid structure, is arranged below lift supporting leg 12 at vaporizer about 1 two ends, for regulating the height of vaporizer 1, ensure that condensed organic solvent flows in closed waste collection bucket 8 smoothly.
As preferably, in order to improve the organic efficiency of organic solvent, it is possible to arrange at least one alembic 5 and condensing tube 6, and the number of alembic 5 and condensing tube 6 is one to one. Such as alembic 5 and condensing tube 6 can be 2,3,4,5 or more. Specifically, the water cooling tube of all condensing tubes 6 is communicated with each other by multiple circulating water pipes 4, with shared condensation water 3; The import of the inner core tube of each condensing tube 6 connects an independent alembic 5 respectively, and is confluxed by mozzle 7 in the exit of inner core tube, and is tightly connected with closed waste collection bucket 8 by the mozzle 7 after confluxing. On this basis, in order to ensure condensation degree, the condensing tube 6 in this utility model embodiment is preferably serpentine condenser 6.
Specifically, in the retracting device that this utility model embodiment provides, the connection between all parts should be seal, to ensure that organic solvent will not leak in air. Specifically, this relation of being tightly connected can use elastic hose, the caulking gum head 11 with central through hole realizes. As preferably, this utility model embodiment is by making in the central through hole that the side pipe of alembic 5 stretches into caulking gum head 11, and make caulking gum head 11 fill in the inner core tube of condensing tube 6, realize being tightly connected between the import of inner core tube and the side pipe of alembic 5, and by making in the central through hole that the outlet of mozzle 7 extend into caulking gum head 11, and make caulking gum head 11 fill in closed waste collection bucket 8, realize being tightly connected between the outlet of mozzle 7 and closed waste collection bucket 8.
The foregoing is only preferred embodiment of the present utility model; not in order to limit protection domain of the present utility model; all within spirit of the present utility model and principle, any amendment of making, equivalent replacement, improvement etc., should be included within protection domain of the present utility model.
Claims (8)
1. the retracting device of a volatile solvent, it is characterised in that described retracting device includes vaporizer, adds heat pipe, condensation water, circulating water pipe, alembic, condensing tube, mozzle, closed waste collection bucket;
Be filled with heating medium in described vaporizer, described in add heat pipe and be arranged in described vaporizer, for the described thermal medium that adds is heated, what described alembic was placed on described vaporizer adds in thermal medium;
Described condensing tube is made up of inner core tube and water cooling tube, the side pipe of the import of described inner core tube and described alembic is tightly connected, the outlet of described inner core tube is connected with the inlet seal of described mozzle, and the outlet of described mozzle and described closed waste collection bucket are tightly connected; Described water cooling tube, described circulating water pipe, described condensation water are sequentially connected with, to form condensing unit.
2. retracting device according to claim 1, it is characterised in that described retracting device also includes temperature control and display, hygrosensor;
Described hygrosensor is arranged on described heating media interior, is used for adding described in measuring the temperature of thermal medium;
Described temperature controls and display is arranged on described vaporizer outer wall, add heat pipe with described simultaneously and described hygrosensor electrically connects, for receiving and show the temperature data measured by described hygrosensor, according to the control of described temperature data, add the heating-up temperature of heat pipe simultaneously.
3. retracting device according to claim 2, it is characterised in that be provided with hold-down support in described vaporizer, is used for placing described alembic.
4. retracting device according to claim 3, it is characterised in that described vaporizer is cuboid structure, is arranged below lift supporting leg at two ends, described vaporizer left and right, for regulating the height of described vaporizer.
5. retracting device according to claim 1, it is characterised in that the number of described alembic and described condensing tube is at least one;
The described water cooling tube of all described condensing tubes is communicated with each other by multiple described circulating water pipes, to share described condensation water;
The import of the described inner core tube of each described condensing tube connects an independent described alembic respectively, and confluxed by described mozzle in the exit of described inner core tube, and it is tightly connected by the described mozzle after confluxing and described closed waste collection bucket.
6. retracting device according to claim 1, it is characterised in that described condensing tube is serpentine condenser.
7. retracting device according to claim 1, it is characterized in that, by using the caulking gum head with central through hole to realize being tightly connected between the import of described inner core tube and the side pipe of described alembic, and realize being tightly connected between outlet and the described closed waste collection bucket of described mozzle.
8. retracting device according to claim 1, it is characterised in that be additionally provided with circulating pump in described vaporizer, adds thermal medium described in being used for circulating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201521003354.8U CN205287636U (en) | 2015-12-07 | 2015-12-07 | Recovery unit of volatile solvent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201521003354.8U CN205287636U (en) | 2015-12-07 | 2015-12-07 | Recovery unit of volatile solvent |
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| Publication Number | Publication Date |
|---|---|
| CN205287636U true CN205287636U (en) | 2016-06-08 |
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| CN201521003354.8U Active CN205287636U (en) | 2015-12-07 | 2015-12-07 | Recovery unit of volatile solvent |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106125775A (en) * | 2016-07-05 | 2016-11-16 | 中国核动力研究设计院 | Based on devices and methods therefor steam flow being evaporated, measure and controlling |
| CN106110697A (en) * | 2016-08-23 | 2016-11-16 | 成都慧信实验设备有限公司 | Box electrothermic retorting device |
| CN106125776A (en) * | 2016-07-05 | 2016-11-16 | 中国核动力研究设计院 | Devices and methods therefor steam flow being evaporated, measure and automatically controlling |
| CN109060580A (en) * | 2018-06-14 | 2018-12-21 | 超威电源有限公司 | A kind of sour saturation degree test method of battery separator suction |
| CN109833488A (en) * | 2019-03-06 | 2019-06-04 | 吴克足 | A kind of biology,drug and chemical industry factory heating device |
| CN112782026A (en) * | 2021-01-19 | 2021-05-11 | 四川科路泰交通科技有限公司 | Novel cyclic analysis appearance of pitch content among bituminous mixture |
| CN116022900A (en) * | 2023-03-30 | 2023-04-28 | 沧州医学高等专科学校 | Laboratory waste liquid treatment device and method |
-
2015
- 2015-12-07 CN CN201521003354.8U patent/CN205287636U/en active Active
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106125775A (en) * | 2016-07-05 | 2016-11-16 | 中国核动力研究设计院 | Based on devices and methods therefor steam flow being evaporated, measure and controlling |
| CN106125776A (en) * | 2016-07-05 | 2016-11-16 | 中国核动力研究设计院 | Devices and methods therefor steam flow being evaporated, measure and automatically controlling |
| CN106125776B (en) * | 2016-07-05 | 2018-10-30 | 中国核动力研究设计院 | The method that steam flow is evaporated, measure and is automatically controlled |
| CN106125775B (en) * | 2016-07-05 | 2018-12-04 | 中国核动力研究设计院 | Based on the method for being evaporated, measuring and controlling to steam flow |
| CN106110697A (en) * | 2016-08-23 | 2016-11-16 | 成都慧信实验设备有限公司 | Box electrothermic retorting device |
| CN109060580A (en) * | 2018-06-14 | 2018-12-21 | 超威电源有限公司 | A kind of sour saturation degree test method of battery separator suction |
| CN109060580B (en) * | 2018-06-14 | 2020-12-15 | 超威电源集团有限公司 | Method for testing acid absorption saturation of storage battery separator |
| CN109833488A (en) * | 2019-03-06 | 2019-06-04 | 吴克足 | A kind of biology,drug and chemical industry factory heating device |
| CN109833488B (en) * | 2019-03-06 | 2021-03-09 | 鹤壁市人民医院 | Heating device for biological medicine chemical plant |
| CN112782026A (en) * | 2021-01-19 | 2021-05-11 | 四川科路泰交通科技有限公司 | Novel cyclic analysis appearance of pitch content among bituminous mixture |
| CN116022900A (en) * | 2023-03-30 | 2023-04-28 | 沧州医学高等专科学校 | Laboratory waste liquid treatment device and method |
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