CN203935633U - A kind of novel organic solvent recovery device - Google Patents
A kind of novel organic solvent recovery device Download PDFInfo
- Publication number
- CN203935633U CN203935633U CN201420367246.8U CN201420367246U CN203935633U CN 203935633 U CN203935633 U CN 203935633U CN 201420367246 U CN201420367246 U CN 201420367246U CN 203935633 U CN203935633 U CN 203935633U
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- CN
- China
- Prior art keywords
- condenser pipe
- organic solvent
- still
- recovery device
- solvent recovery
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000003960 organic solvent Substances 0.000 title claims abstract description 28
- 238000011084 recovery Methods 0.000 title claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims abstract description 11
- 238000009833 condensation Methods 0.000 claims abstract description 6
- 230000005494 condensation Effects 0.000 claims abstract description 6
- 238000005485 electric heating Methods 0.000 claims description 6
- WYTGDNHDOZPMIW-RCBQFDQVSA-N alstonine Natural products C1=CC2=C3C=CC=CC3=NC2=C2N1C[C@H]1[C@H](C)OC=C(C(=O)OC)[C@H]1C2 WYTGDNHDOZPMIW-RCBQFDQVSA-N 0.000 claims description 3
- 239000012530 fluid Substances 0.000 abstract description 11
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 238000004064 recycling Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 238000002390 rotary evaporation Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model relates to a kind of novel organic solvent recovery device, comprises reaction vessel, and reaction vessel comprises reative cell, equalized temperature chamber, filling opening, bottleneck and arm; Still, the lower end of still is connected with bottleneck; Condenser pipe, comprises the first condenser pipe and the second condenser pipe that are connected, and the lower end of the second condenser pipe is connected with arm, and the upper end of the first condenser pipe is connected with still; Receiving flask; Heater.In the utility model, organic solvent to be recycled adds in reative cell, conductive fluid adds equalized temperature indoor, heater heating conductive fluid, conductive fluid is heated and is heated up and heat evenly imported in the organic solvent of reative cell, organic solvent is heated to vaporize and enters still, exports to receiving flask reclaim after the first condensing tube condensation by the first liquid outlet; The second condenser pipe reuses the condensed water of the first condenser pipe, using water wisely, more environmental protection.
Description
Technical field
The utility model relates to a kind of retracting device, relates in particular to a kind of novel organic solvent recovery device.
Background technology
In the laboratories such as chemistry, environment, biochemistry, organic solvent extracts the solvent of use as synthetic agent, synthetic medium, natural organic-compound, need recycling use.In existing laboratory, conventional Rotary Evaporators, distilling apparatus, fractionating device reclaim, and distillation, that device is built in fractionation is more loaded down with trivial details, waste time and energy; Rotary evaporation need to be supported by pumped vacuum systems, more difficult.
Utility model content
The purpose of this utility model is to overcome the defect that prior art exists, and a kind of novel organic solvent recovery device is provided.
The technical scheme that realizes the utility model object is: a kind of novel organic solvent recovery device, comprising:
Reaction vessel, reaction vessel is shell type cucurbit, described shell type cucurbit comprises reative cell, equalized temperature chamber, filling opening, bottleneck and arm, described reative cell is arranged at described equalized temperature chamber interior, described filling opening, bottleneck are connected with described reative cell, and described arm is connected with described equalized temperature chamber;
Still, the lower end of described still is connected with described bottleneck;
Condenser pipe, comprise the first condenser pipe and the second condenser pipe that are connected, described the first condenser pipe upper end is connected with described still, described the first condenser pipe lower end is provided with the first liquid outlet, on the lower sides of described the first condenser pipe, be also provided with the first water inlet, the lower end of described the second condenser pipe is connected with described arm, is provided with the second delivery port in the upper portion side wall of described the second condenser pipe;
Receiving flask, be arranged at described the first condenser pipe below and with the corresponding setting of described the first liquid outlet;
Heater, is connected with described equalized temperature chamber.
Further, described the first condenser pipe is serpentine condenser, and described the second condenser pipe is spherical condensation tube.
Further, described still is flow guiding type still.
Further, be also provided with thermometer, described thermometer runs through the upper end that is arranged at described still.
Further, be also provided with lifting platform, described receiving flask is arranged on described lifting platform.
Further, described heater is electric heating cover, and described electric heating cover is coated on the outer surface of described equalized temperature chamber.
Further, be also provided with for containing the dropping funel of organic solvent to be recycled, described dropping funel is connected with described filling opening.
The utlity model has positive effect: in the utility model, organic solvent to be recycled adds in reative cell, conductive fluid adds equalized temperature indoor, heater heating conductive fluid, conductive fluid is heated and is heated up and heat evenly imported in the organic solvent of reative cell, organic solvent is heated to vaporize and enters still, then after the first condensing tube condensation, by the first liquid outlet, exports to receiving flask and reclaims; On the other hand, condensed water enters the first condenser pipe from the first water inlet, then enters the second condenser pipe, finally from the second delivery port, derives, and maintains the balance of conductive fluid, and the second condenser pipe reuses the condensed water of the first condenser pipe, using water wisely, more environmental protection.
Accompanying drawing explanation
For content of the present utility model is more easily expressly understood, according to specific embodiment also by reference to the accompanying drawings, the utility model is described in further detail below, wherein:
Fig. 1 is the structural representation of the utility model the first embodiment;
Fig. 2 is the structural representation of the utility model the first embodiment.
Wherein: 1, heater, 2, reaction vessel, 3, dropping funel, 4, still, the 5, first delivery port, 6, thermometer, the 7, second condenser pipe, the 8, first condenser pipe, the 9, first liquid outlet, the 10, first water inlet, 11, receiving flask, 12, lifting platform.
The specific embodiment
As shown in Figure 1, as the first preferred embodiment, present embodiment provides a kind of novel organic solvent recovery device, comprising:
Reaction vessel 2, reaction vessel 2 is shell type cucurbit, and shell type cucurbit comprises reative cell, equalized temperature chamber, filling opening, bottleneck and arm, and reative cell is arranged at equalized temperature chamber interior, and filling opening, bottleneck are connected with reative cell, and arm is connected with equalized temperature chamber;
Still 4, the lower end of still 4 is connected with bottleneck;
Condenser pipe, comprise the first condenser pipe 8 and the second condenser pipe 7 that are connected, the first condenser pipe 8 upper ends are connected with still 4, the first condenser pipe 8 lower ends are provided with the first liquid outlet 9, on the lower sides of the first condenser pipe 8, be also provided with the first water inlet 10, the lower end of the second condenser pipe 7 is connected with arm, is provided with the second delivery port 5 in the upper portion side wall of the second condenser pipe 7;
Receiving flask 11, be arranged at the first condenser pipe 8 below and with the corresponding setting of the first liquid outlet 10;
Heater 1, is connected with equalized temperature chamber.
In present embodiment, organic solvent to be recycled adds in reative cell, conductive fluid adds equalized temperature indoor, heater 1 heating conductive fluid, conductive fluid is heated and is heated up and heat evenly imported in the organic solvent of reative cell, organic solvent is heated to vaporize and enters still, then after the first condenser pipe 8 condensations, by the first liquid outlet 9, exports to receiving flask 11 and reclaims; On the other hand, condensed water enters the first condenser pipe 8 from the first water inlet 10, then enters the second condenser pipe 7, finally from the second delivery port 5, derive, maintain the balance of conductive fluid, the condensed water of second condenser pipe 7 recycling the first condenser pipes 8, using water wisely, more environmental protection.
As shown in Figure 2, as the first preferred embodiment, the first condenser pipe 8 that present embodiment provides is serpentine condenser, the second condenser pipe 7 is spherical condensation tube, still 4 is flow guiding type still, and heater 1 is electric heating cover, and electric heating cover is coated on the outer surface of equalized temperature chamber.
Present embodiment is also provided with thermometer 6, and thermometer 6 runs through the upper end that is arranged at still 4, the temperature that thermometer monitoring organic solvent fractionates out.
Present embodiment is also provided with lifting platform 12, and receiving flask 11 is arranged on lifting platform 12, and lifting platform 12 is controlled the distance of receiving flask 11 and the first liquid outlet 9.
Present embodiment is also provided with for containing the dropping funel 3 of organic solvent to be recycled, and dropping funel 3 is connected with filling opening.
Above-described specific embodiment; the purpose of this utility model, technical scheme and beneficial effect are further described; institute is understood that; the foregoing is only specific embodiment of the utility model; be not limited to the utility model; all within spirit of the present utility model and principle, any modification of making, be equal to replacement, improvement etc., within all should being included in protection domain of the present utility model.
Claims (7)
1. a novel organic solvent recovery device, is characterized in that, comprising:
Reaction vessel, described reaction vessel is shell type cucurbit, described shell type cucurbit comprises reative cell, equalized temperature chamber, filling opening, bottleneck and arm, described reative cell is arranged at described equalized temperature chamber interior, described filling opening, described bottleneck are connected with described reative cell, and described arm is connected with described equalized temperature chamber;
Still, the lower end of described still is connected with described bottleneck;
Condenser pipe, comprise the first condenser pipe and the second condenser pipe that are connected, the upper end of described the first condenser pipe is connected with described still, the lower end of described the first condenser pipe is provided with the first liquid outlet, on the lower sides of described the first condenser pipe, be also provided with the first water inlet, the lower end of described the second condenser pipe is connected with described arm, is provided with the second delivery port in the upper portion side wall of described the second condenser pipe;
Receiving flask, be arranged at described the first condenser pipe below and with the corresponding setting of described the first liquid outlet;
Heater, it is connected with described equalized temperature chamber.
2. novel organic solvent recovery device according to claim 1, is characterized in that, described the first condenser pipe is serpentine condenser, and described the second condenser pipe is spherical condensation tube.
3. novel organic solvent recovery device according to claim 1, is characterized in that, described still is flow guiding type still.
4. novel organic solvent recovery device according to claim 1, is characterized in that, is also provided with thermometer, and described thermometer runs through the upper end that is arranged at described still.
5. novel organic solvent recovery device according to claim 1, is characterized in that, is also provided with lifting platform, and described receiving flask is arranged on described lifting platform.
6. novel organic solvent recovery device according to claim 1, is characterized in that, described heater is electric heating cover, and described electric heating cover is coated on the outer surface of described equalized temperature chamber.
7. novel organic solvent recovery device according to claim 1, is characterized in that, is also provided with for containing the dropping funel of organic solvent to be recycled, and described dropping funel is connected with described filling opening.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420367246.8U CN203935633U (en) | 2014-07-03 | 2014-07-03 | A kind of novel organic solvent recovery device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420367246.8U CN203935633U (en) | 2014-07-03 | 2014-07-03 | A kind of novel organic solvent recovery device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203935633U true CN203935633U (en) | 2014-11-12 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420367246.8U Expired - Fee Related CN203935633U (en) | 2014-07-03 | 2014-07-03 | A kind of novel organic solvent recovery device |
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| Country | Link |
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| CN (1) | CN203935633U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104771923A (en) * | 2015-03-16 | 2015-07-15 | 泰州市华晨仪器有限公司 | Water quality positive-pressure distillation instrument |
| CN105381622A (en) * | 2015-10-16 | 2016-03-09 | 哈尔滨理工大学 | Continuous reduced pressure distillation apparatus and method for refining branched fatty acyl chloride by using apparatus thereof |
| CN107114821A (en) * | 2017-07-07 | 2017-09-01 | 重庆中烟工业有限责任公司 | The apparatus and method that a kind of hot trapping prepares smoke spices |
| CN110006774A (en) * | 2018-01-04 | 2019-07-12 | 中电电气(上海)太阳能科技有限公司 | A kind of cross linking degree tester of recyclable dimethylbenzene and its application |
-
2014
- 2014-07-03 CN CN201420367246.8U patent/CN203935633U/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104771923A (en) * | 2015-03-16 | 2015-07-15 | 泰州市华晨仪器有限公司 | Water quality positive-pressure distillation instrument |
| CN104771923B (en) * | 2015-03-16 | 2016-09-07 | 泰州市华晨仪器有限公司 | A kind of water quality malleation distillation apparatus |
| CN105381622A (en) * | 2015-10-16 | 2016-03-09 | 哈尔滨理工大学 | Continuous reduced pressure distillation apparatus and method for refining branched fatty acyl chloride by using apparatus thereof |
| CN105381622B (en) * | 2015-10-16 | 2017-08-18 | 哈尔滨理工大学 | The method that Branched fatty acyl chlorides is refined using continuous vacuum distillation apparatus |
| CN107114821A (en) * | 2017-07-07 | 2017-09-01 | 重庆中烟工业有限责任公司 | The apparatus and method that a kind of hot trapping prepares smoke spices |
| CN107114821B (en) * | 2017-07-07 | 2019-03-19 | 重庆中烟工业有限责任公司 | A kind of device and method of hot trapping preparation smoke fragrance |
| CN110006774A (en) * | 2018-01-04 | 2019-07-12 | 中电电气(上海)太阳能科技有限公司 | A kind of cross linking degree tester of recyclable dimethylbenzene and its application |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141112 Termination date: 20150703 |
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| EXPY | Termination of patent right or utility model |