CN106125775A - Based on devices and methods therefor steam flow being evaporated, measure and controlling - Google Patents

Based on devices and methods therefor steam flow being evaporated, measure and controlling Download PDF

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Publication number
CN106125775A
CN106125775A CN201610519491.XA CN201610519491A CN106125775A CN 106125775 A CN106125775 A CN 106125775A CN 201610519491 A CN201610519491 A CN 201610519491A CN 106125775 A CN106125775 A CN 106125775A
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China
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flow
evaporation
container
steam flow
steam
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CN201610519491.XA
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CN106125775B (en
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李统业
张良
潘小强
杨静
唐明国
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Nuclear Power Institute of China
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Nuclear Power Institute of China
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    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05DSYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D7/00Control of flow
    • G05D7/06Control of flow characterised by the use of electric means

Abstract

The invention discloses one to be evaporated based on to steam flow, metering and the device controlled, add and hot tank is provided with container for evaporation, add and weighing apparatus and display system are installed in hot tank, weighing apparatus is connected with container for evaporation and display system simultaneously, container for evaporation connects jet chimney, jet chimney is internal with container for evaporation to be connected, and it is provided with stop valve on jet chimney, and stop valve can cut off the jet chimney of correspondence, jet chimney is provided with control valve, control valve can cut off jet chimney, add and in hot tank, be provided with hands handle, handle connects bindiny mechanism, and bindiny mechanism is connected with control valve.By balance weight method, steam flow is measured, steam flow is controlled by the aperture utilizing Non-follow control control valve, there is good reliability, use the metering that temperature is high, be applicable to less steam flow and advantage steam flow can being controlled, it is possible to form effective supplementing for existing steam-flow meter.

Description

Based on devices and methods therefor steam flow being evaporated, measure and controlling
Technical field
The invention belongs to the metering of flow and control technical field, being specifically related to one and steam based on to steam flow The devices and methods therefor send out, measuring and controlling.
Background technology
The metering of steam flow is one crucial technology of chemical field, currently mainly uses vortex-shedding meter or differential pressure stream Gauge carries out the metering of steam flow.After having evaporated, the deposit that high-temperature steam cooling produces can block and corrode effusion meter, Therefore measuring accuracy is gradually reduced, and easily causes the inefficacy of effusion meter.Steam-flow meter use temperature typically below 350 DEG C, The evaporating temperature steam more than 350 DEG C can not be measured, and be not suitable for the metering of less steam flow.It addition, steam stream The metering being mainly used in steam flow of gauge, typically without the control function of steam flow, it is therefore desirable to find new steam stream The metering of amount and control method.
Document 1, the Chinese patent of Patent No. 201410047972.6, disclose the steam vortex street of a kind of measuring multiple parameters Effusion meter, swirl generating body is arranged in the endoporus that pipe table body measured by band, measures the outside of pipe table body at band and is positioned at vortex and sends out The vertical open pores just below of raw body install described in flow transducer, band measure pipe table body be arranged above support barrel mast, Described support barrel mast covers flow transducer, and described flow integrator is arranged on the end, upper end supporting barrel mast.The present invention The parameter that can measure steam is many, broad quantum, and the precision of measurement steam is high, the pressure loss is little, and multiple sensors is based on integration Design, flowmeter structure is compact, the advantage such as reliability height, low cost of manufacture, working service convenience, life of product length, have employed Resistant to elevated temperatures flow transducer and temperature sensor so that the steam vortex flowmeter of this measuring multiple parameters can measure saturated steaming Vapour can measure again the superheated steam of higher temperature.
Document 2, the Chinese patent of Patent No. 03820649.8 relates to a kind of method, wherein utilizes bluff body (20) at stream Body produces vortex, and determines the repetition rate producing vortex.The repetition rate determined for calculating flow measurement (XV), It represents volume flow or flow velocity.Additionally, two measurement point (M1, the M2) records being separated from each other in the flowing direction act on stream Two pressure p 1 and p2 of body.In these pressure, at least one is at least with repetition rate periodically-varied.Pressure p 1 He of record P2 is used for generating pressure measuring value (Xp), and its representative at least partly acts on one section of average time period in the flowing direction Average dynamic pressure.Pressure measuring value (Xp) and flow measurement (XV) are for determining the mass flow measurement (Xm) of fluid.
Document 3, the Chinese patent of Patent No. 200710133653.7 relates to a kind of effusion meter, is specially a kind of split type Vortex-shedding meter.It is made up of with digital signal processing module sensor, conditioning circuit module, three kinds of sensors and modulate circuit Module is placed in the tested scene of high temperature, and digital signal processing module is under normal temperature environment, between module by shielded cable even Connect, transmit signal with the form of differential signal.It solve prior art and may not apply to the technical problem of hot environment, permissible It is applied to hot environment and needs the special occasions of split type instrument, there is good capacity of resisting disturbance and reliability.
Document 4, the Chinese patent of Patent No. 201320110735.0 relates to one and is applicable to industrial automation instrument neck The flowmeter in territory, especially relates to a kind of steam-flow meter, and it includes interior wimble device, interior wimble device is combined with successively cold Condenser, difference become assembly and buckling assembly, and interior wimble device is from the V-arrangement inner cone measured with on pipe, the support measured in pipe, support Body forms;This utility model structure is unique, facilitate user installation, height accurate to flow measurement of steam, scene can show many seed ginsengs Count and have 485 communication interfaces, be easy to user transmission, gather and manage.
Document 5, the Chinese patent of Patent No. 200910011212.9 relates to heavy crude heat extraction steam and drives steam injection well high temperature height The thick oil thermal extraction saturated steam flow metering method of pressure saturated vapor one-well metering, is to pass through thick oil thermal extraction saturated steam Effusion meter realizes, and this effusion meter is made up of pressure transducer, display, differential pressure variator, V-type cone, temperature sensor: pressure Force transducer is threadeded with metering pipeline, display and pressure transducer, differential pressure transmitter, temperature sensor screw thread, and V-type is bored Body is welded to connect with differential pressure transmitter;The method is to be connected with manifold and steam injection well screw thread by thick oil thermal extraction saturated steam effusion meter Connect, produce differential pressure at V-type cone two ends when steam passes through this effusion meter, it is achieved that the accurate measurement to saturated vapor flow velocity, With differential pressure variator, flow velocity is converted into flow signal send into calculating system and show steam one-well metering at any time.The method solves The problem that can not measure single well flow in prior art.The present invention can be used for heavy crude heat extraction steam drive steam injection well High Temperature High Pressure satisfy With in steam one-well metering.
Document 6, Patent No. 200820068517.4 discloses a kind of integrated pressure-differential type steam flow meter, including throttling Device, the ring flange in throttling arrangement is arranged on measurement pipe, is provided with orifice plate, is respectively placed in the pressure of orifice plate both sides in measuring pipe Pipe extend in high pressure room and the low pressure room of equalizing reservoir, and equalizing reservoir is connected by pressure guiding pipe and three valve groups, three valve groups It is connected with differential pressure meter.The pressure room part of pressure guiding pipe, three valve groups and differential pressure meter is under the liquid level of equalizing reservoir, and has Downward inclination angle.In this utility model, the equipment such as throttling arrangement, pressure pipe, equalizing reservoir and differential pressure meter is integrated, Decrease the workload of on-the-spot processing and fabricating, facilitate in-site installation, improve work efficiency, reduce the skill of in-site installation personnel Energy;After integration, it is ensured that the reliability of device, improve the quality of product
Document 7, the Chinese patent of Patent No. 201220685281.5 discloses the differential pressure type of a kind of intelligent measure steam flow Effusion meter and pressure tester, it include throttling element, connecting pipe, its also include differential pressure transmitter or intelligent flow-integrating instrument, described Differential pressure transmitter or intelligent flow-integrating instrument be connected with the positive and negative pressure chamber of throttling element respectively, wherein with plemum by connecting pipe The connecting pipe connected is plemum conduit, and the pilot being connected with negative pressure chamber is negative pressure chamber's conduit, and described plemum conduit is with negative More than one group serpentine pipe, a diameter of 1mm~40mm of described serpentine pipe, serpentine pipe and horizontal plane angle it is respectively provided with on pressure chamber conduit It is 0~45 DEG C, described plemum conduit and negative pressure chamber's conduit further respectively has a switch valve or is provided with three valve groups It is simultaneously connected with plemum conduit and negative pressure chamber's conduit, serpentine pipe and differential pressure transmitter or intelligent flow on described plemum conduit The pipeline that integrating instrument connects is additionally provided with pressure transducer.This utility model fills connecting pipe, compact conformation, volume without anti-icing fluid Little.
Document 8, the Chinese patent of Patent No. 201320155941.3 discloses a kind of condensation weighing method steam-flow meter Amount standard set-up, including vacuum tank, temperature transmitter, pressure transmitter, effusion meter, manual ball valve, pneumatic ball valve, pneumatic butterfly Valve, pneumatic control valve, direct-operated regulator, meter-clamping apparatus, electronic scale, condenser, cooling tower, water pump, each parts are by pipeline even Connect.Vapour source is by after vacuum tank, and pressure regulation enters calibrating pipeline, by tested effusion meter, enters condenser, by accredited steaming The steam of steam flow gauge all condenses, and condensed water is carried out Weighing, the condensate quality weighed with pass through steam The quality of steam of effusion meter compares, and completes the calibrating to steam-flow meter, improves automaticity, and temperature, pressure can Control, can examine and determine multiple caliber effusion meter, and the accuracy of measuring is reliable, and calibrating efficiency is high, plays certain effect for national energy-saving consumption reduction.
Document 9, nineteen eighty-three 03 periodical delivered Guangzhou Nitrogenous Fertilizer Factory and succeeded in developing a kind of steam flow caliberating device, can be to work Industry steam-flow meter carries out verification and demarcates.It uses timing weight method in kind, and steam is first condensed into water, then water is weighed with Determine steam flow.This device is made up of vapour source, condenser, timer, weighing utensil and various monitoring instrument.Small investment, Energy consumption is low, the more reduction of cumulative flow.
Document 10, within 2009,02 phase periodical discloses the analysis on Uncertainty of steam real stream calibrating vortex-shedding meter, flux of vortex street Count by a large amount of, be widely used in the metering of steam flow, the calibrating of vortex-shedding meter is currently mainly used and replaces with air Steam is examined and determine as calibrating medium, inevitably has a certain impact verification result.Article is based on condensation weighing method Vortex-shedding meter is examined and determine by steam flow assay device, and is analyzed result, gives and fixs real the failing to be sold at auction of steam Uncertainty evaluation method and result.
Document 11, the Chinese patent of Patent No. 201210564802.6 discloses a kind of for dynamic gas flow analysis Weight-loss method detection of gas flow rate method.It uses following detecting step: set up the Dynamic link library of electronic balance and computer, starts Gas generator and beginning timing and weighing, the volumetric flow of gas of unit of account time, obtain flow-time curve figure, inspection Survey data process&analysis.It utilizes the Dynamic link library of electronic balance and computer, the gaseous mass of real-time detected gas generator Flow, utilizes the weighing software of computer to complete to detect accordingly process, including: balance type selecting and configuration, the conversion of volume flow, inspection Survey the setting of duration, the drafting of flow-time curve figure, data process&analysis.It is widely used in all kinds of middle-size and small-size gas The detection of gas flow rate of generator, it is also possible to the gas flow for quality change corresponding with the time dynamically detects.The present invention has There are simple to operate, detection safety, and the advantage that the high and on-the-spot adaptability of accuracy of detection is good.
Document 12, the Chinese patent of Patent No. 201110147057.0 discloses a kind of mass flow based on weight method Meter, including container, the top of container is provided with water inlet, and bottom is provided with outlet, and the bottom of container is provided with LOAD CELLS, container The lower section of interior water inlet is provided with water conservancy diversion and anti-impact device.When can reduce flow dynamics measurement, hydraulic shock power symmetry retransmits The measurement error that sensor causes, and the bigger impurity in drainage can be crossed by this device, solve line clogging and water circulation system Unite a most smooth difficult problem.
Document 13, the United States Patent (USP) of Patent No. US20060464514 discloses A fabric treatment appliance comprises a steam generator having a chamber configured to hold Water, a supply conduit configured to transport water to the steam generator Chamber, a weight sensor outputting a signal responsive to the weight of the Steam generator, and a controller coupled to the weight sensor and configured to control a flow of water through the supply conduit based on the signal from the weight sensor. The disclosure provides methods of water supply control that can employ the weight sensor。
Document 14, the Chinese patent of Patent No. 200510131200.1 discloses a kind of weightless effusion meter and weight-loss method stream Amount controller.It solving flow detection device structure used during existing industrial automation produces complicated, cost is high, easy loss etc. Problem, has simple in construction, has antiseptic power, measures accurately, the advantages such as control mode is flexible.Its structure is: a kind of weightless Method effusion meter and weight-loss method flow controller, it has power supply, also includes sensor, and sensor will measure the gravimetric value signal of gained Amplified device and digitizer send into microprocessor after being converted to digital signal;Microprocessor is defeated after processing signal Go out;This control signal can also pass through interface circuit and upper machine communication, weight and flow value is transferred on host computer, it is simple to The monitoring management of host computer, the gravimetric value recorded is simultaneously fed in memorizer, it is simple to process query in the future;Weight and flow value Can be shown by display, microprocessor arranges parameter also by key device.
Document 15, the Chinese patent of Patent No. 201010120967.5 discloses the dynamic weighing of a kind of high-viscosity fluid System and method, the scale body outfan of this system is connected with weight display instrument and weighing controller simultaneously, this Weighing control The output control terminal of device is connected with high-viscosity fluid barrel pump by converter, and this high-viscosity fluid barrel pump is high viscous by being inserted into High-viscosity fluid is pumped into scale body by the pump rod in property fluid charging basket;The method uses high-viscosity fluid barrel pump by high-viscosity fluid pump Getting in scale body, weighing-up wave is fed back in weighing controller by scale body, and weighing controller is the poorest according to controlling parameter employing Value penalty method and to measure minimum stream mensuration and by the pump speed of Frequency Converter Control high-viscosity fluid barrel pump.The present invention is reasonable in design, Achieve and high-viscosity fluid is dynamically precisely weighed function, it is ensured that weighing precision and speed of weighing, meet high viscosity The requirement being dynamically precisely weighed of fluid, has feature easy to use, applied widely simultaneously.
Document 16, it is high that the Chinese patent of Patent No. CN 200710147395 discloses a kind of detection control accuracy, available Flow controller in deep-etching liquid.Employing is weighed and weightless two ways measures flow.Output takes step type electric to hold The method of row device control flow realizes the continuous-stable of fluid flow and controls, flow pulse free composition.Use weightless self-correction Algorithm is tracked curve amendment, can realize flow accumulation error and level off to zero.The present invention mainly by buffer barrel, weighing bucket, enters, Tapping electromagnetic valve and weight display, intelligent controller and step type electric actuator valve composition.Weighing bucket when adding liquid level be by Buffer barrel tapping completes.When weighing bucket liquid level rises, YE valve outlet port flow increases, and stepping YE valve is wanted Progressively go back to pass.When weighing bucket liquid level declines, valve is progressively opened, to keep flow constant.Go round and begin again.Stepping YE Valve returns pass speed and to open speed the most equal with weighing bucket liquid weight climbing speed and the flat root of fall off rate, makes flow-control Become a stable straight line.
The metering method of document 1~7 pairs of steam flows is described, and mainly has vortex street and the two kinds of steam of differential pressure Effusion meter, for the metering of big flow steam, and the function controlled without steam flow.
Document 8,9,10 utilizes weight method to weigh condensed steam, for the mark to steam-flow meter accuracy Fixed, it is impossible to as steam-flow meter, only as the caliberating device of steam-flow meter.Document 11 utilizes weight method to gas flow Measure, but without heating system, and without the function automatically controlled, be not suitable for automatically controlling of steam flow.Document 12, 13 utilize weight method measure the flow of the liquid such as water or control, but this system is in open environment, and nothing The function that steam flow controls.Document 14,15,16 utilizes weight method to count the flow of deep-etching liquid, high-viscosity fluid Amount, and there is the automatic control function of flow, but this system is in open environment, is not suitable for the flow of high-temperature steam Metering and control.
To sum up narrate, so above-mentioned literature research purpose differs with scheme.
Summary of the invention
The technical problem to be solved is the poor reliability of existing steam-flow meter existence, uses temperature low, no It is applicable to the metering of less steam flow and cannot be carried out flow-control, it is therefore intended that providing one to carry out based on to steam flow Evaporation, the devices and methods therefor measuring and controlling, measured steam flow by balance weight method, utilize hand-operated valve to steaming Steam flow amount is controlled, have good reliability, use that temperature is high, be applicable to less steam flow metering and can be to steam stream The advantage that amount is controlled, it is possible to form effective supplementing for existing steam-flow meter, solves existing steam-flow meter and exists Poor reliability, use that temperature is low, be not suitable for the metering of less steam flow and cannot be carried out the problem of flow-control.
The present invention is achieved through the following technical solutions:
Based on device steam flow being evaporated, measure and controlling, add hot tank including inner hollow, described in add in hot tank It is provided with container for evaporation, adds and weighing apparatus and display system are installed in hot tank, and weighing apparatus with container for evaporation and display is simultaneously System connects, and container for evaporation connects jet chimney, and one end of jet chimney is internal with container for evaporation to be connected, and on jet chimney It is provided with stop valve, and stop valve can cut off the jet chimney of correspondence, is provided with control valve, control valve energy on jet chimney Enough cutting off jet chimney, control valve is arranged on and adds in hot tank, adds and is provided with handle in hot tank, and handle connects bindiny mechanism, and Bindiny mechanism is connected with control valve.Existing existence utilizes the method that balance weight method carries out flow measurement, but is not suitable for steaming The metering of steam flow amount, and without the function of flow-control.This patent is called method in the following text by balance and is weighed container for evaporation, passes through Weightlessness in the unit of account time obtains the steam flow of steam.Manually the aperture of application valve body makes steam flow close to meter Draw and control flow, reach the metering of steam flow and the purpose of control.The sensor of this control method is electronic balance, not with Steam directly contacts, and steam will not produce corrosion to electronic balance and then affect precision, does not the most have what control accuracy declined Problem, stability is high.Balance of weighing is adding outside hot tank, is connected with container for evaporation by an one metal wire, not by evaporating temperature Impact, therefore evaporating temperature is higher.The method utilizes balance to call method in the following text and weighs evaporator, and pipeline connection utilizes metal wave Stricture of vagina flexible pipe, reduces the connection pipeline STRESS VARIATION impact on measurement result accuracy, it is possible to meet the precision of low discharge metering Requirement.
Weighing apparatus is electronic balance.In evaporation process, the weight of container for evaporation can be changed output extremely by electronic balance Display system, electronic balance has bottom scale hook, and range should be more than container for evaporation and the weight summation of evaporated material.My god Flat need have data-interface, it is possible to input weight data to display system.
Jet chimney is corrugated tube and metal hard tube, and corrugated tube connects with container for evaporation inside, metal hard tube and ripple Stricture of vagina pipe connects away from one end of container for evaporation.Measurement error mostlys come from the STRESS VARIATION connecting pipeline in evaporation process, steams Sending out and be connected with corrugated flexible hose between tank with metal hard tube, the internal stress of corrugated flexible hose is the least, due to evaporator position ripple The corrugated flexible hose STRESS VARIATION moved and cause is less, even if also therefore being able to the change of the weight to evaporator with the presence of corrugated flexible hose Carry out precise.In order to prevent steam corrosion corrugated flexible hose from causing steam to leak, corrugated flexible hose regularly replaces.
Based on method steam flow being evaporated, measure and controlling, evaporated material after weighing is placed on evaporation and holds In device and seal, being placed on by container for evaporation and add in hot tank, weighing apparatus is arranged on heating box top, and container for evaporation is by gold Belonging to silk and be connected so that container for evaporation is unsettled with weighing apparatus bottom suspension hook, container for evaporation is connected with metal hard tube by corrugated tube, The range of weighing apparatus is more than container for evaporation and the weight summation of evaporated material, after using protection gas to empty container for evaporation, opens Display system, arranges time interval dt reading weighing apparatus display numerical value, in dm is dt according to actual needs by display system The difference of weighing apparatus display numerical value, display system can show the numerical value i.e. steam flow of dm/dt.Start and add hot tank to evaporation appearance Device, control valve heat, and set according to the character of evaporated material and add heater temperature, and in the starting stage, steam flow does not reaches Plan controls flow, and along with the rising of evaporated material temperature, steam flow is gradually increased, when the flow of evaporated material is i.e. up to Plan controls flow, and the aperture of Non-follow control control valve makes steam flow control flow close to plan, if steam flow is the lowest Control flow in plan, then heighten the aperture of Non-follow control control valve, until steam flow is close to setting flow value, if steam stream Measure and control flow apparently higher than plan, then turn down the aperture of Non-follow control control valve, until steam flow controls stream close to plan Amount, after evaporation process reaches the scheduled time or evaporated material evaporates substantially, will add heat container front and back end stop valve and close, pass Fall heating system, cool down.By balance weight method, steam flow is measured, utilize control valve that steam flow is carried out Control, there is good reliability, use temperature height, be applicable to the metering of less steam flow and steam flow can be controlled Advantage, be mainly used in the evaporation of the steam flow that existing steam-flow meter can not complete, measure and control.Manually control The aperture of valve body makes steam flow control flow close to plan, it is achieved the purpose that steam flow controls.The biography of this control method Sensor is electronic balance, does not directly contact with steam, and steam will not produce corrosion to electronic balance and then affect precision, the most not There is the problem that control accuracy declines, stability is high.The electronic balance weighed is outside container for evaporation adds hot tank, by a metal Silk is connected with container for evaporation, is not affected by evaporating temperature, and therefore evaporating temperature is higher.The method utilizes balance to call method in the following text to steaming Sending out tank to weigh, pipeline connection utilizes corrugated flexible hose, reduces the connection pipeline STRESS VARIATION shadow to measurement result accuracy Ring, it is possible to meet the required precision of low discharge metering.
The present invention compared with prior art, has such advantages as and beneficial effect:
(1) by the evaporator in evaporation process being weighed and weightlessness in the unit of account time obtains the steam stream of steam Amount, the method blocks or corrodes effusion meter after not cooled down by steam to be affected, reliable and stable;
(2) the use temperature of this device is high, it is possible to realize the flow of 800 DEG C of steam is measured and controlled;
(3) this device utilizes balance to call method in the following text only to weigh evaporator, and pipeline connects and utilizes metal bellow, reduces Connect the impact on measurement result accuracy of the pipeline STRESS VARIATION, it is adaptable to the metering of less steam flow;
(4) aperture of this device manually application valve body thus control the steam flow of steam, the control of steam flow can be realized System.
Accompanying drawing explanation
Accompanying drawing described herein is used for providing being further appreciated by the embodiment of the present invention, constitutes of the application Point, it is not intended that the restriction to the embodiment of the present invention.In the accompanying drawings:
Fig. 1 is present configuration schematic diagram;
Fig. 2 is the flow-control experimental result schematic diagram of embodiment 1;
Fig. 3 is the flow-control experimental result schematic diagram of embodiment 2.
The parts title of labelling and correspondence in accompanying drawing:
1-adds hot tank, 2-container for evaporation, 3-stop valve, 4-corrugated tube, 5-display system, 6-electronic balance, 7-handle, and 8-connects Mechanism, 9-control valve, 10-metal hard tube.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearer, below in conjunction with embodiment and accompanying drawing, to this Invention is described in further detail, and the exemplary embodiment of the present invention and explanation thereof are only used for explaining the present invention, do not make For limitation of the invention.
Embodiment 1:
As shown in Figure 1 and Figure 2, to NbCl5The evaporation of steam flow, measure and control, by the NbCl of 200g5Powder loads evaporation In container 2, being placed on electronic balance 6 and weigh after then being sealed by container for evaporation 2, gross weight is 9829.08g.By close The container for evaporation 2 being honored as a queen is arranged on and adds in hot tank 1, and electronic balance 6 shows that weight is 9846.33g.Use protection gas that evaporation is held After device emptying, opening display system 5 and show flow value, steam flow dm/dt time interval is 5s, NbCl5Effusion meter Draw and control as 0.10g/s.Startup adds hot tank 1 and heats container for evaporation 2, control valve 9, and be provided with container for evaporation adds hot tank Temperature be set in 270 DEG C, the temperature adding hot tank being provided with control valve is set in 270 DEG C.Container for evaporation in evaporation process Weight change and steam flow be not as in figure 2 it is shown, in the starting stage, steam flow reaches setting flow, along with evaporated material temperature The rising of degree, steam flow is gradually increased, and works as NbCl5When flow is i.e. up to 0.10g/s, utilize opening of Non-follow control control valve Degree transfers in row NbCl5The control of flow;When steam flow is significantly lower than 0.10g/s, suitably heighten the aperture of control valve until steaming Steam flow amount is close to 0.10g/s;When steam flow is apparently higher than 0.10g/s, suitably turn down the aperture of control valve, until steam flow Close to 0.10g/s.After evaporation a period of time, NbCl5Substantially use up, NbCl5Flow-reduction, will add heat container front and back end stop valve Close, now stop container for evaporation and control valve are heated.The display weight of last balance is 9667.86g, whole evaporation process The weightlessness of middle on-line weighing is 178.51g.Completely after cooling, container for evaporation is dismantled, is then placed within balance weighing, Gross weight is 9653.02g, NbCl in whole evaporation process5Actual weightlessness be 176.06g, weightless basic with on-line weighing Unanimously, the steam flow that online weighing is described is accurately.As seen from Figure 2, at NbCl5The Non-follow control process of steam flow In, steam flow has a certain degree of fluctuation, but flowed fluctuation range-controllable, say and utilize this device can carry out NbCl5Stream The control of amount.
Embodiment 2:
As shown in Figure 1, Figure 3, to TiCl4The evaporation of steam flow, measure and control, by the TiCl of 500g4Load container for evaporation In, it being placed on electronic balance after then container for evaporation being sealed and weigh, gross weight is 10131.08g.After sealing Container for evaporation is arranged on and adds in hot tank, and electronic balance display weight is 10147.11g.Use protection gas that container for evaporation is emptied After, to open display system and flow value is shown, steam flow dm/dt time interval is 10s, TiCl4Flow plan controls For 0.15g/s.Startup adds hot tank and heats container for evaporation, control valve, and the temperature adding hot tank being provided with container for evaporation sets Being scheduled on 160 DEG C, the temperature adding hot tank being provided with control valve is set in 160 DEG C.The weight change of container for evaporation in evaporation process And steam flow is not as it is shown on figure 3, in the starting stage, steam flow reaches setting flow, along with the rising of evaporated material temperature, Steam flow is gradually increased, and works as TiCl4When flow reaches 0.15g/s, hand control valve is utilized to carry out TiCl4The control of flow.As Really steam flow is significantly lower than 0.15g/s, suitably heightens the aperture of control valve, until steam flow is close to 0.15g/s.If steamed Steam flow amount, apparently higher than 0.15g/s, suitably turns down the aperture of control valve, until steam flow is close to 0.15g/s.Evaporation 60min After, heat container front and back end stop valve will be added and close, and turn off heating system, cool down.Now the display weight of balance is 9811.52g, in whole evaporation process, the weightlessness of on-line weighing is 335.59g.Completely after cooling, container for evaporation is dismantled, then Being placed on balance and weigh, gross weight is 9792.14g, TiCl in whole evaporation process4Actual weightlessness be 338.94g, Basically identical with the weightlessness of on-line weighing, illustrate that the steam flow of online weighing is accurately.As seen from Figure 3, at TiCl4Steam During the Non-follow control of steam flow amount, steam flow has a certain degree of fluctuation, but flowed fluctuation range-controllable, say and utilize this Device can carry out TiCl4The control of flow.
Call method in the following text by balance container for evaporation is weighed, obtained the steaming of steam by the weightlessness in the unit of account time Steam flow amount, manually adjust control valve aperture control steam flow close to flow set flow, reach steam flow control Purpose.The present invention is applicable to steam flow control accuracy and automaticity less demanding, however it is necessary that steam flow becomes The place that change can quickly respond.
Above-described detailed description of the invention, has been carried out the purpose of the present invention, technical scheme and beneficial effect further Describe in detail, be it should be understood that the detailed description of the invention that the foregoing is only the present invention, be not intended to limit the present invention Protection domain, all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. done, all should comprise Within protection scope of the present invention.

Claims (4)

1. based on device steam flow being evaporated, measure and controlling, it is characterised in that include inner hollow adds hot tank (1), described in add hot tank (1) be provided with container for evaporation (2), add and weighing apparatus and display system (5) be installed in hot tank (1), and Weighing apparatus is connected with container for evaporation (2) and display system (5) simultaneously, and container for evaporation (2) connects jet chimney, jet chimney One end and container for evaporation (2) are internal to be connected, and is provided with stop valve (3) on jet chimney, and stop valve (3) can cut off right The jet chimney answered, is provided with control valve (9) on jet chimney, and the aperture of control valve (9) can adjust, and adds in hot tank (1) Being provided with handle (7), handle (7) connects bindiny mechanism (8), and bindiny mechanism (8) is connected with control valve (9).
It is the most according to claim 1 based on device steam flow being evaporated, measure and controlling, it is characterised in that Described weighing apparatus is electronic balance (6).
It is the most according to claim 1 based on device steam flow being evaporated, measure and controlling, it is characterised in that Described jet chimney is corrugated tube (4) and metal hard tube (10), and corrugated tube (4) connects with container for evaporation (2) inside, metal Hard tube (10) is connected away from one end of container for evaporation (2) with corrugated tube (4).
4. based on method steam flow being evaporated, measure and controlling, it is characterised in that: the material after weighing is placed on In container for evaporation (2) and seal, being placed on by container for evaporation (2) and add in hot tank (1), weighing apparatus is arranged on and adds hot tank (1) Top, container for evaporation (2) is connected so that container for evaporation (2) is unsettled by tinsel with weighing apparatus bottom suspension hook, container for evaporation (2) being connected with metal hard tube (7) by corrugated tube (4), the range of weighing apparatus is more than container for evaporation (2) and the weight of evaporated material Summation, after using protection gas to empty container for evaporation (2), opens display system (5), passes through display system according to actual needs (5) arranging and read time interval dt of weighing apparatus display numerical value, dm is the difference of weighing apparatus display numerical value, display system in dt (5) can show that the numerical value i.e. steam flow of dm/dt, startup add hot tank (1) and add container for evaporation (2), control valve (9) Heat, sets according to the character of evaporated material and adds hot tank (1) temperature, and in the starting stage, the steam flow plan of not reaching controls flow, Along with the rising of evaporated material temperature, steam flow is gradually increased, and controls flow when the flow of evaporated material is i.e. up to plan, The aperture of Non-follow control control valve (9) makes steam flow control flow close to plan, if steam flow controls significantly lower than plan Flow, then heighten the aperture of Non-follow control control valve (9), until steam flow is close to setting flow value, if steam flow is obvious Control flow higher than plan, then turn down the aperture of Non-follow control control valve (9), until steam flow controls flow close to plan, After evaporation process reaches the scheduled time or evaporated material evaporates substantially, heat container front and back end stop valve (3) will be added and close, close Fall heating system, cool down.
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