CN205182700U - System of recycling is retrieved to alcohol - Google Patents
System of recycling is retrieved to alcohol Download PDFInfo
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- CN205182700U CN205182700U CN201520899873.0U CN201520899873U CN205182700U CN 205182700 U CN205182700 U CN 205182700U CN 201520899873 U CN201520899873 U CN 201520899873U CN 205182700 U CN205182700 U CN 205182700U
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Abstract
The utility model relates to a glycyrrhizinic acid monoammonium salt production facility technical field provides a system of recycling is retrieved to alcohol, system of recycling is retrieved to alcohol is including setting up gas recovery pipeline on the drying -machine in, and cauldron and rectifying column, in feed through with alkalization centrifugal filter and acidizing centrifugal filter's liquid outlet respectively with the import of cauldron, in with the export of cauldron with the liquid import intercommunication of rectifying column, the gas recovery pipeline with the gas feed intercommunication of rectifying column, the liquid import of rectifying column is located the upper portion of rectifying column, the gas feed and the liquid outlet of rectifying column are located the lower part of rectifying column. The utility model provides the recycle of high ethanol as the solvent is rateed, has reduced manufacturing cost.
Description
Technical field
The utility model relates to mono-ammonium glycyrrhizinate production equipment technical field, is specially a kind of alcohol recycle reutilization system.
Background technology
Mono-ammonium glycyrrhizinate belongs to Triterpenes triterpenes, and molecular weight is 839.97, is white or pale yellow crystals type powder, has special sweet taste.Find that mono-ammonium glycyrrhizinate has anti-hepatotoxicity, hormone-like activity, prevents cirrhosis etc. after deliberation.Mono-ammonium glycyrrhizinate not only has significant curative effect to respiratory diseases such as tracheitis, bronchitis, cough, asthma, and also has good result for the treatment of to infection of digestive canal, hepatitis B, canker sore, gastric ulcer etc.There is stronger detoxicating functions for multiple toxin as diphtheria toxin, tetanus toxin and snake venom etc., also there is the effect of similar cortex hormone of aadrenaline simultaneously.Chinese medicine has body Mutiple Targets, multiple organ, and multisystem produces the advantage of comprehensive function.Ammonium glycyrrhizinate has now been widely used in medicine, health products, food service industry.
At present, generally adopt neutral alcohol as solvent extraction in mono-ammonium glycyrrhizinate industrial production, but solvent recovering rate is lower, is generally only 40% ~ 50%, wasting of resources situation is obvious.Above-mentioned reason is caused to mainly contain 2 points: the first, insufficient to alkalization, acidifying and refining solvent recovery used of purifying; The second, the product after ammonium glycyrrhizinate salt refining is centrifugal is directly dried, and the ethanol steamed in drying course all emits, do not reclaim, this not only causes the waste of etoh solvent, and discarded alcohol gas also constitutes a threat to safety in production, there is larger potential safety hazard.
Utility model content
Technical problem to be solved in the utility model is: provide a kind of alcohol recycle reutilization system, to improve the ethanol recovery utilization rate as solvent, reduces production cost.
For solving the problems of the technologies described above, the utility model provides following technical scheme:
A kind of alcohol recycle reutilization system, described alcohol recycle reutilization system comprise the gas withdrawal line be arranged on dryer, in and still and rectifying column, be communicated with the liquid outlet of acidifying centrifugal filter with alkalization centrifugal filter respectively with the import of still in described, be communicated with the liquid-inlet of the outlet of still with described rectifying column in described, described gas withdrawal line is communicated with the gas feed of described rectifying column, the liquid-inlet of described rectifying column is positioned at the top of described rectifying column, and the gas feed of described rectifying column and liquid outlet are positioned at the bottom of described rectifying column.
Preferably, the liquid outlet of mono-ammonium glycyrrhizinate production system purification centrifugal filter is communicated with described rectifying column liquid-inlet.
Preferably, described mono-ammonium glycyrrhizinate production system comprises leaching tower, alkalization still, described alkalization centrifugal filter, acidifying still, described acidifying centrifugal filter, decolorization and purification still, plate filter, described purification centrifugal filter, described dryer, pulverizer and packing machine from front to back successively.
Preferably, the liquid outlet of described rectifying column is connected with the liquid-inlet of described leaching tower.
After have employed technique scheme, the beneficial effects of the utility model are: because described alcohol recycle reutilization system comprises the gas withdrawal line be arranged on dryer, in and still and rectifying column, be communicated with the liquid outlet of acidifying centrifugal filter with alkalization centrifugal filter respectively with the import of still in described, be communicated with the liquid-inlet of the outlet of still with described rectifying column in described, described gas withdrawal line is communicated with the gas feed of described rectifying column, the liquid-inlet of described rectifying column is positioned at the top of described rectifying column, the gas feed of described rectifying column and liquid outlet are positioned at the bottom of described rectifying column, therefore, this recycling system is not only to alkalization, in acidifying and drying course, alcohol solvent used has carried out omnibearing recovery, and adopt rectifying column equipment, simultaneously to gas, liquid ethanol reclaims, substantially increase organic efficiency and recovering effect.In addition, from alkalization centrifugal filter alkaline ethanol solvent out and from acidifying centrifugal filter acidic ethanol solvent out and in first carrying out in still and, then enter in rectifying column and reclaim, also further increase the ethanol rate of recovery.Through measuring and calculating, during the utility model makes mono-ammonium glycyrrhizinate produce, alcohol recycle utilization rate reaches 70% ~ 80%, greatly reduces production cost.
Accompanying drawing explanation
Fig. 1 is the utility model detailed description of the invention stereoscopic mechanism schematic diagram;
Wherein, 1, leaching tower; 2, alkalize centrifugal filter; 3, acidifying centrifugal filter; 4, purification centrifugal filter; 5, dryer; 6, gas withdrawal line; 7, in and still; 8, rectifying column.
detailed description of the invention;
Below in conjunction with accompanying drawing, detailed description of the invention of the present utility model is elaborated.
embodiment 1
A kind of alcohol recycle reutilization system being applied to mono-ammonium glycyrrhizinate and producing as shown in Figure 1.Mono-ammonium glycyrrhizinate production system comprises leaching tower 1, alkalization still, alkalization centrifugal filter 2, acidifying still, acidifying centrifugal filter 3, decolorization and purification still, plate filter, purification centrifugal filter 4, dryer 5, pulverizer and packing machine from front to back successively.
Alcohol recycle reutilization system comprise the gas withdrawal line 6 be arranged on dryer, in and still 7 and rectifying column 8, in be communicated with the liquid outlet of acidifying centrifugal filter 3 with alkalization centrifugal filter 2 respectively with the import of still 7, in be communicated with the liquid-inlet of rectifying column 8 with the outlet of still 7, gas withdrawal line 6 is communicated with the gas feed of rectifying column 8, the liquid-inlet of rectifying column 8 is positioned at the top of rectifying column, and the gas feed of rectifying column 8 and liquid outlet are positioned at the bottom of rectifying column 8.The liquid outlet of purification centrifugal filter 4 is communicated with rectifying column 8 liquid-inlet.The liquid outlet of rectifying column 8 is connected with the liquid-inlet of leaching tower 1.
The utility model has carried out disposable recovery to alcohol solvent used in alkalization, acidifying, refining purification and drying course, and adopts rectifying column equipment, reclaims simultaneously, substantially increase organic efficiency and recovering effect to gas, liquid ethanol.In addition, from alkalization centrifugal filter alkaline ethanol solvent out and from acidifying centrifugal filter acidic ethanol solvent out and in first carrying out in still and, then enter in rectifying column and reclaim, also further increase the ethanol rate of recovery.Through measuring and calculating, during the utility model makes mono-ammonium glycyrrhizinate produce, alcohol recycle utilization rate reaches 70% ~ 80%, greatly reduces production cost.
The utility model is not limited to above-mentioned concrete embodiment, and those of ordinary skill in the art is from above-mentioned design, and without performing creative labour, done all conversion, all drop within protection domain of the present utility model.
Claims (4)
1. an alcohol recycle reutilization system, it is characterized in that: described alcohol recycle reutilization system comprises the gas withdrawal line be arranged on dryer, in and still and rectifying column, be communicated with the liquid outlet of acidifying centrifugal filter with alkalization centrifugal filter respectively with the import of still in described, be communicated with the liquid-inlet of the outlet of still with described rectifying column in described, described gas withdrawal line is communicated with the gas feed of described rectifying column, the liquid-inlet of described rectifying column is positioned at the top of described rectifying column, the gas feed of described rectifying column and liquid outlet are positioned at the bottom of described rectifying column.
2. a kind of alcohol recycle reutilization system as claimed in claim 1, is characterized in that: the liquid outlet of mono-ammonium glycyrrhizinate production system purification centrifugal filter is communicated with described rectifying column liquid-inlet.
3. a kind of alcohol recycle reutilization system as claimed in claim 2, is characterized in that: described mono-ammonium glycyrrhizinate production system comprises leaching tower, alkalization still, described alkalization centrifugal filter, acidifying still, described acidifying centrifugal filter, decolorization and purification still, plate filter, described purification centrifugal filter, described dryer, pulverizer and packing machine from front to back successively.
4. a kind of alcohol recycle reutilization system as claimed in claim 3, is characterized in that: the liquid outlet of described rectifying column is connected with the liquid-inlet of described leaching tower.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520899873.0U CN205182700U (en) | 2015-11-12 | 2015-11-12 | System of recycling is retrieved to alcohol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520899873.0U CN205182700U (en) | 2015-11-12 | 2015-11-12 | System of recycling is retrieved to alcohol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205182700U true CN205182700U (en) | 2016-04-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201520899873.0U Active CN205182700U (en) | 2015-11-12 | 2015-11-12 | System of recycling is retrieved to alcohol |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106083526A (en) * | 2016-06-01 | 2016-11-09 | 金河生物科技股份有限公司 | Ethanol reclaims the system and method for Automated condtrol |
| CN111116431A (en) * | 2019-12-31 | 2020-05-08 | 中船重工（邯郸）派瑞特种气体有限公司 | Device and method for recovering trifluoromethanesulfonic acid from trifluoromethanesulfonic acid-containing wastewater |
| WO2022122027A1 (en) | 2020-12-11 | 2022-06-16 | 安徽金禾实业股份有限公司 | Device for alcohol distillation decoloring and purification and method for purification in maltol production |
-
2015
- 2015-11-12 CN CN201520899873.0U patent/CN205182700U/en active Active
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106083526A (en) * | 2016-06-01 | 2016-11-09 | 金河生物科技股份有限公司 | Ethanol reclaims the system and method for Automated condtrol |
| CN106083526B (en) * | 2016-06-01 | 2018-06-19 | 金河生物科技股份有限公司 | Ethyl alcohol recycles the system and method for automation control |
| CN111116431A (en) * | 2019-12-31 | 2020-05-08 | 中船重工（邯郸）派瑞特种气体有限公司 | Device and method for recovering trifluoromethanesulfonic acid from trifluoromethanesulfonic acid-containing wastewater |
| CN111116431B (en) * | 2019-12-31 | 2022-08-05 | 中船(邯郸)派瑞特种气体股份有限公司 | Device and method for recovering trifluoromethanesulfonic acid from trifluoromethanesulfonic acid-containing wastewater |
| WO2022122027A1 (en) | 2020-12-11 | 2022-06-16 | 安徽金禾实业股份有限公司 | Device for alcohol distillation decoloring and purification and method for purification in maltol production |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
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Address after: 831200 office building, No. three, No. 1, light industrial zone, Hutubi County Industrial Park, Changji Hui Autonomous Prefecture, the Xinjiang Uygur Autonomous Region, Patentee after: Xinjiang Kaimeijia Biotechnology Co.,Ltd. Address before: 831200 office building, No. three, No. 1, light industrial zone, Hutubi County Industrial Park, Changji Hui Autonomous Prefecture, the Xinjiang Uygur Autonomous Region, Patentee before: HUTUBI MEIJIA BIOTECHNOLOGY Co.,Ltd. |