CN205046080U - Solar energy silicon chip cutting antiquated sand thick liquid recovery processing device - Google Patents

Solar energy silicon chip cutting antiquated sand thick liquid recovery processing device Download PDF

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Publication number
CN205046080U
CN205046080U CN201520846523.8U CN201520846523U CN205046080U CN 205046080 U CN205046080 U CN 205046080U CN 201520846523 U CN201520846523 U CN 201520846523U CN 205046080 U CN205046080 U CN 205046080U
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China
Prior art keywords
mortar
storage tank
processing device
connects
silicon wafers
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Expired - Fee Related
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CN201520846523.8U
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Chinese (zh)
Inventor
郇伟伟
李洁
李春锐
周岩
丁海军
杨宇翔
吕伟伟
关莹
郭建忠
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Zhejiang A&F University ZAFU
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Zhejiang A&F University ZAFU
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Abstract

The utility model provides a solar energy silicon chip cutting antiquated sand thick liquid recovery processing device, antiquated sand thick liquid storage tank discharge gate connection charge pump, charge pump connect the ultrasonator feed inlet, and the high -speed centrifuge feed inlet is connected to the ultrasonator discharge gate, and centrifugation liquid storage tank inlet is connected to the high -speed centrifuge liquid outlet, and high -speed centrifuge goes out mortar mouth connection mortar storage tank and advances the mortar mouth. The utility model has the advantages of antiquated sand thick liquid gets into and carries out ultrasonic vibration through ultrasonator to the antiquated sand thick liquid earlier before the high -speed centrifuge and handle, peels off out at the tiny particle silica flour on large granule carborundum surface adhesion in the antiquated sand thick liquid with the carborundum granule is effectual, and then gets into high -speed centrifuge and carry out centrifugation, reduce the proportion of tiny particle silica flour in the carborundum granule that centrifugation came out, has improved the carborundum granule that obtains was starched to the antiquated sand after the recovery processing quality.

Description

A kind of solar silicon wafers cutting waste mortar recycling and processing device
Technical field
The utility model relates to a kind of device improving solar silicon wafers cutting waste mortar recycling effect.
Background technology
Along with the development of photovoltaic industry in recent years, solar-grade polysilicon sheet has become the upstream resource that Ge great Photovoltaics Com Inc. falls over each other to fight for, monocrystalline, the section production cost of polysilicon chip oneself become the primary link affecting photovoltaic industry.Produce single crystal, therefore polysilicon chip necessary cutting mortar consumption have also been obtained and increases sharply.
Photovoltaic solar silicon wafers cutting be generally use hardness high, granularity is little and the silicon carbide micro-powder of centralized particle diameter as main Cutting Medium.Silicon carbide micro-powder is joined in cutting liquid according to a certain percentage, and makes it fully disperse, be mixed with uniform and stable cutting mortar, cut for silicon chip.Use silicon carbide micro-powder is the high-speed motion of the firm line of utilization cutting in the mechanism of solar silicon wafers Linear cut as medium, silicon carbide micro-powder particle is driven to impact continuously and healthily silicon rod surface, the rigid characteristic of silicon-carbide particle and sharp water caltrop is utilized progressively to be blocked by silicon rod, this process can discharge along with larger heat of friction, therefore, cutting mortar need possess and have good dispersiveness to silicon-carbide particle, and can take away the amount of heat produced in cutting process.Wherein, silicon-carbide particle except adding in the composition of the useless cutting mortar after section, further comprises copper and iron fines that a large amount of tiny silica flours produced in cutting process and the silicon carbide crushed particles to produce owing to colliding and rub and cutting steel wire split away off in friction process.These solid particulates in mortar to the generation physical abuse of silicon chip surface, therefore can reclaim when mortar continues to utilize and need removing as far as possible to reclaim the various impurity in mortar.
Utility model content
The utility model, for above problem, provides a kind of device improving solar silicon wafers cutting waste mortar recycling effect.
Utility model object of the present utility model is realized by following scheme: a kind of solar silicon wafers cutting waste mortar recycling and processing device, comprise waste mortar storage tank, fresh feed pump, ultrasonator, supercentrifuge, mortar storage tank and centrifugation liquid storage tank, waste mortar reservoir outlet connects fresh feed pump, fresh feed pump connects ultrasonator opening for feed, ultrasonator discharge port connects high speed centrifugation machine inlet capable, supercentrifuge liquid outlet connects centrifugation liquid storage tank fluid inlet, and supercentrifuge goes out mortar mouth connection mortar storage tank and enters mortar mouth.
Further, under meter is provided with between fresh feed pump and ultrasonator.
Further, opening for feed is offered in ultrasonator upper end, and discharge port is offered in lower end.
Further, supercentrifuge goes out mortar mouth and mortar storage tank and enters mortar mouth and be provided with under meter.
Further, mortar storage tank fluid inlet connects cutting liquid storage tank liquid outlet, and pump and under meter are established in centre.
Further, mortar tank bottom middle position is provided with stir shaft, and stir shaft is provided with 1-3 layer mixing page, and paddle is by mortar storage tank decile, and stir shaft connects driving arrangement, and mortar tank bottom offers discharge port.
Further, establish heating unit in centrifugation liquid storage tank, centrifugation liquid storage tank liquid outlet connects pressure filter, and pressure filter connects ion exchange pot, and ion exchange pot connects multiple-effect evaporator, and multiple-effect evaporator connects ceramic membrane ultrafitration equipment.
Further, activated carbon filter layer is provided with between centrifugation liquid storage tank and pressure filter.
Further, supercentrifuge is provided with water-in, and water-in connects water outlet equipment.
Further, ceramic membrane ultrafitration equipment liquid outlet connects cutting liquid storage tank fluid inlet.
The beneficial effects of the utility model are: waste mortar first carries out sonic oscillation process through ultrasonator to waste mortar before entering supercentrifuge, the small-particle silica flour and silicon-carbide particle that stick to macrobead silicon carbide in waste mortar are effectively peeled away, and then enter supercentrifuge and carry out centrifugation, reduce the ratio of centrifugation silicon-carbide particle small particles silica flour out, the quality of the silicon-carbide particle obtained after improve waste mortar recycling.
Accompanying drawing explanation
Fig. 1 is schematic diagram of the present utility model.
Embodiment
Below in conjunction with specific embodiments and the drawings, the utility model is described in further detail:
With reference to shown in accompanying drawing 1, a kind of solar silicon wafers cutting waste mortar recycling and processing device of the present utility model, comprise waste mortar storage tank 1, fresh feed pump 2, ultrasonator 4, supercentrifuge 5, mortar storage tank 7 and centrifugation liquid storage tank 8, waste mortar storage tank 1 discharge port connects fresh feed pump 2, fresh feed pump 2 connects ultrasonator 4 opening for feed, ultrasonator 4 discharge port connects supercentrifuge 5 opening for feed, supercentrifuge 5 liquid outlet connects centrifugation liquid storage tank 8 fluid inlet, and supercentrifuge 5 goes out mortar mouth connection mortar storage tank 7 and enters mortar mouth.Sonic oscillation was adopted before high speed centrifugation, the effect of separating silicon carbide and silica flour when obviously can improve high-speed separation, in the silicon carbide be out separated after sonic oscillation the small particle content such as silica flour than without sonic oscillation or after being separated sonic oscillation again silicon carbide in low percent 2-of the small particle content such as silica flour percent 5, effectively improve the quality reclaiming mortar.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, is provided with under meter 3 between fresh feed pump 2 and ultrasonator 4.Can the import volume of accurate-metering waste mortar.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, opening for feed is offered in ultrasonator 4 upper end, and discharge port is offered in lower end.Make waste mortar effectively and all through sonic oscillation.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, supercentrifuge 5 goes out mortar mouth and mortar storage tank 7 and enters mortar mouth and be provided with under meter.The amount of mortar can be isolated by accurate-metering, add cutting liquid according to its quantity.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, mortar storage tank 7 fluid inlet connects cutting liquid storage tank 6 liquid outlet, and pump and under meter are established in centre, cutting liquid are imported to mortar storage tank 7, and accurate-metering and control slurry density.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, mortar storage tank 7 lower center position is provided with stir shaft, stir shaft is provided with 1-3 layer mixing page, paddle is by mortar storage tank decile, stir shaft connects driving arrangement, offer discharge port bottom mortar storage tank 7, churning time at least continues 4 hours, makes cutting liquid and mortar be thoroughly mixed to form spendable solar silicon wafers cutting mortar.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, heating unit is established in centrifugation liquid storage tank 8, centrifugation liquid storage tank 8 liquid outlet connects pressure filter, pressure filter connects ion exchange pot, ion exchange pot connects multiple-effect evaporator, multiple-effect evaporator connects ceramic membrane ultrafitration equipment, can further by the cutting liquid in parting liquid and silica flour Separation and Recovery.。
A kind of solar silicon wafers cutting waste mortar recycling and processing device, is provided with activated carbon filter layer between centrifugation liquid storage tank 8 and pressure filter.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, supercentrifuge 5 is provided with water-in, and water-in connects water outlet equipment.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, ceramic membrane ultrafitration equipment liquid outlet connects cutting liquid storage tank 6 fluid inlet, is provided with magnet bottom cutting liquid storage tank 6, and the metallic impurity in cutting liquid are reclaimed in absorption.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, supercentrifuge 5 is vertical centrifugal separating machine, horizontal centrifugal separating machine, settlement separator or hydroseparator, and supercentrifuge rotating speed is 500-4800 rev/min.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, fresh feed pump 2 flow is 800-1200L/h, and the volume of ultrasonator 4 is 200-300L, and ultrasonic frequency is 28-35KHz, and power density is 0.4-0.5W/cm 2.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, fresh feed pump 2 flow is 1000-1400L/h, and the volume of ultrasonator 4 is 250-350L, and ultrasonic frequency is 32-40KHz, and power density is 0.45-0.55W/cm 2.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, the volume of ultrasonator 4 is 200-350L, and ultrasonic frequency is 28-40KHz, and power density is 0.4-0.55W/cm 2.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, adopts pipeline to connect between each parts.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, is provided with strong magnetosphere between supercentrifuge 5 and mortar storage tank 7.The metal powder in mortar is reclaimed in absorption.
A kind of solar silicon wafers cutting waste mortar recycling and processing device, waste mortar through ultrasonator 4, supercentrifuge 5 according to the difference of silica flour and silicon carbide micro-powder pellet density, silicon carbide micro-powder in waste mortar is separated with the wire cutting liquid of silicon powder-containing, is recycled mortar and parting liquid; Be separated the liquid obtained, be heated to 30 ~ 70 DEG C, squeeze into pressure filter, again be separated, make the limpid no suspended substance of the liquid of discharge, adopt the method that natural subsidence and press filtration combine, silica flour is separated the filtrate obtaining secondary separation and obtain with wire cutting liquid, filtrate carries out desolventing technology, ion-exchange, multiple-effect evaporation dehydration, ultrafiltration, filling, obtained product line cutting liquid successively, and concrete steps are as follows:
A. decolour
The active carbon layer that the filtrate that secondary separation obtains passes through 1% ~ 5% of its weight decolours, and then squeeze into pressure filter, filtrate is for subsequent use;
B. ion-exchange
Filtrate after being decoloured by step a, squeezes into ion exchange pot, to the ion be mixed in silicon chip Linear cut process and in later stage sepn process, carries out ion-exchange, removes the liquid after ion, treats subsequent handling process;
C. multiple-effect evaporation dehydration
Liquid after ion-exchange is squeezed into multiple-effect evaporator, the portion of water in liquid is deviate from, make water ratio reach wire cutting liquid index, standby ultrafiltration;
D. ultrafiltration, filling
Liquid after dehydration is squeezed into ceramic membrane ultrafitration equipment, and the liquid after filtration is wire cutting liquid finished product, filling.
Although the utility model has illustrated by reference to preferred embodiment and has described, but those of ordinary skill in the art should understand, the description of above-described embodiment can be not limited to, in the scope of claims, the various changes in form and details can be made.

Claims (10)

1. a solar silicon wafers cutting waste mortar recycling and processing device, comprise waste mortar storage tank, fresh feed pump, ultrasonator, supercentrifuge, mortar storage tank and centrifugation liquid storage tank, it is characterized in that: waste mortar reservoir outlet connects fresh feed pump, fresh feed pump connects ultrasonator opening for feed, ultrasonator discharge port connects high speed centrifugation machine inlet capable, supercentrifuge liquid outlet connects centrifugation liquid storage tank fluid inlet, and supercentrifuge goes out mortar mouth connection mortar storage tank and enters mortar mouth.
2. solar silicon wafers cutting waste mortar recycling and processing device according to claim 1, is characterized in that: be provided with under meter between fresh feed pump and ultrasonator.
3. solar silicon wafers cutting waste mortar recycling and processing device according to claim 1, is characterized in that: opening for feed is offered in ultrasonator upper end, and discharge port is offered in lower end.
4. solar silicon wafers according to claim 1 cutting waste mortar recycling and processing device, is characterized in that: supercentrifuge goes out mortar mouth and mortar storage tank and enters mortar mouth and be provided with under meter.
5. solar silicon wafers cutting waste mortar recycling and processing device according to claim 1, is characterized in that: mortar storage tank fluid inlet connects cutting liquid storage tank liquid outlet, and pump and under meter are established in centre.
6. solar silicon wafers cutting waste mortar recycling and processing device according to claim 1, it is characterized in that: mortar tank bottom middle position is provided with stir shaft, stir shaft is provided with 1-3 layer mixing page, paddle is by mortar storage tank decile, stir shaft connects driving arrangement, and mortar tank bottom offers discharge port.
7. solar silicon wafers cutting waste mortar recycling and processing device according to claim 1, it is characterized in that: in centrifugation liquid storage tank, establish heating unit, centrifugation liquid storage tank liquid outlet connects pressure filter, pressure filter connects ion exchange pot, ion exchange pot connects multiple-effect evaporator, and multiple-effect evaporator connects ceramic membrane ultrafitration equipment.
8. solar silicon wafers cutting waste mortar recycling and processing device according to claim 7, is characterized in that: be provided with activated carbon filter layer between centrifugation liquid storage tank and pressure filter.
9. solar silicon wafers cutting waste mortar recycling and processing device according to claim 1, it is characterized in that: supercentrifuge is provided with water-in, water-in connects water outlet equipment.
10. solar silicon wafers cutting waste mortar recycling and processing device according to claim 1, is characterized in that: ceramic membrane ultrafitration equipment liquid outlet connects cutting liquid storage tank fluid inlet.
CN201520846523.8U 2015-10-29 2015-10-29 Solar energy silicon chip cutting antiquated sand thick liquid recovery processing device Expired - Fee Related CN205046080U (en)

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Application Number Priority Date Filing Date Title
CN201520846523.8U CN205046080U (en) 2015-10-29 2015-10-29 Solar energy silicon chip cutting antiquated sand thick liquid recovery processing device

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111359563A (en) * 2018-12-25 2020-07-03 汉能新材料科技有限公司 Reaction device and method for recycling waste solar chips
CN115404120A (en) * 2022-08-26 2022-11-29 江阴东为资源再生技术有限公司 Mortar recovery method, system, electronic device and storage medium

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111359563A (en) * 2018-12-25 2020-07-03 汉能新材料科技有限公司 Reaction device and method for recycling waste solar chips
CN111359563B (en) * 2018-12-25 2023-12-12 东君新能源有限公司 Reaction device and method for recycling solar waste chips
CN115404120A (en) * 2022-08-26 2022-11-29 江阴东为资源再生技术有限公司 Mortar recovery method, system, electronic device and storage medium

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160224

Termination date: 20161029

CF01 Termination of patent right due to non-payment of annual fee