CN205038132U - Novel imbibition experiment device - Google Patents

Novel imbibition experiment device Download PDF

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Publication number
CN205038132U
CN205038132U CN201520828223.7U CN201520828223U CN205038132U CN 205038132 U CN205038132 U CN 205038132U CN 201520828223 U CN201520828223 U CN 201520828223U CN 205038132 U CN205038132 U CN 205038132U
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China
Prior art keywords
imbibition
cup
rock core
novel
electronic balance
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Expired - Fee Related
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CN201520828223.7U
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Chinese (zh)
Inventor
谢坤
牛丽伟
喻琴
周彦霞
张宝岩
潘赫
卓艳男
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Northeast Petroleum University
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Northeast Petroleum University
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Abstract

The utility model relates to a novel imbibition experiment device. Solved mainly that solution gas in the imbibition liquid that exists, rock core are inside gets rid of the problem that gas and rock core surface adhesion oil influence imbibition oil pump capacity numerical result precision among the prior art. Its characterized in that: closed box (2) middle part sets up the baffle, the baffle overhead has electronic balance (3), and electronic balance passes through connecting rod (9) and connects rock core (8), closed box (2) inner bottom is deployed there are imbibition cup (5), stirring rake (4) have been put at the bottom center in the imbibition cup, bottom both sides fixed connection fixed bolster (6) in the stirring rake upper portion imbibition cup, and the fixed bolster passes imbibition cup lateral wall perpendicularly through the shank of bolt to be connected on the imbibition cup, two fixed bolster middle part centre gripping fixed rock core (8). This novel imbibition experiment device can get rid of the bubble and the oil that attach to the rock core surface and drip, improves imbibition experiment precision.

Description

A kind of novel imbibition experimental provision
Technical field
The utility model relates to a kind of experimental provision, particularly a kind of novel imbibition experimental provision of the application of chemical experiment field.
Background technology
In recent years, day by day to increase and conventional gas and oil resource workable reserve successively decreases year by year along with energy demand, the energy position of unconventional petroleum resources is important all the more, and wherein the exploitation of low permeability oil field has received the great attention of oil field scientific worker.Low permeability oil field is less due to reservoir core pore throat radius, there is stronger capillary force, so recover the oil by imbibition improve low permeability oil field oil recovery factor further.Usual field practice needs Related Experimental Study to provide fundamental basis, and is optimized extremely is necessary so carry out indoor imbibition oil recovery experimental study parameters.Porous medium spontaneous imbibition oil recovery research method is mainly volumetric method and mass method two kinds, and wherein mass method is because laboratory automation degree is high and reason easy to operate is widely used in current imbibition research.But also there is certain defect in mass method at present: in (1) imbibition process, the change of core quality difference is little, is subject to extraneous factors impact (slight perturbations just can bring larger reading error) such as vibrations, air and water vapor; 2. can not enter imbibition liquid by desorption completely from the inner imbibition of rock core to appearance crude oil, part be attached to core surface, and it produces viscous force can affect core quality measuring accuracy.
Summary of the invention
Technical problem to be solved in the utility model be overcome solution gas in the imbibition liquid that exists in background technology, gas is got rid of in rock core inside and core surface attaching oil affects the problem of imbibition oil pump capacity computational solution precision, and a kind of novel imbibition experimental provision is provided, this novel imbibition experimental provision, by stirring imbibition liquid in experimentation in good time, get rid of the bubble and the oil droplet that are attached to core surface, imbibition experimental precision can be improved.
The invention for solving the technical problem reaches by following technical scheme: this novel imbibition experimental provision comprises closed box, electronic balance and imbibition cup, in the middle part of described closed box, dividing plate is set, described dividing plate is equipped with electronic balance, and electronic balance connects rock core by connecting link; Closed box inner bottom part is equipped with imbibition cup, described imbibition cup inner bottom part center is equipped with paddle, paddle top imbibition cup inner bottom part both sides are fixedly connected with fixed support, fixed support passes perpendicularly through imbibition cup sidewall by body of bolt and is connected on imbibition cup, grips rock core in the middle part of described two fixed supports.
The utility model can have following beneficial effect compared with above-mentioned background technology: this novel imbibition experimental provision, and owing to adopting said structure, imbibition cup heat effect can meet different experiments temperature requirement; Paddle can drive imbibition liquid to flow, and makes to enter imbibition liquid smoothly from rock core internal penetration to the oil droplet of outside in imbibition experimentation, eliminates it and is adsorbed on rock core appearance and tests the impact brought to core quality, finally reaches and improves experimental precision object.Computer acquisition system gathers different experiments moment electronic balance registration automatically, alleviates experimenter's working strength.In experimentation, stir imbibition liquid in good time, get rid of the bubble and the oil droplet that are attached to core surface, and then improve imbibition experimental precision.
Accompanying drawing explanation
Accompanying drawing 1 is structural representation of the present utility model.
In figure: 1-computer acquisition system, 2-closed box, 3-electronic balance, 4-paddle, 5-imbibition cup, 6-fixed support, 7-imbibition liquid, 8-rock core, 9-connecting link.
Embodiment
Below in conjunction with accompanying drawing, the utility model is described in further detail:
As shown in Figure 1, this novel imbibition experimental provision comprises closed box 2 and electronic balance 3, imbibition cup 5, arranges dividing plate, described dividing plate is equipped with electronic balance 3 in the middle part of described closed box 2, and electronic balance 3 connects rock core 8 by coupling arrangement; Closed box 2 inner bottom part is equipped with imbibition cup 5, described imbibition cup 5 inner bottom part center is equipped with paddle 4, paddle 4 top imbibition cup 5 inner bottom part both sides are fixedly connected with fixed support 6, fixed support 6 passes perpendicularly through imbibition cup 5 sidewall by body of bolt and is connected on imbibition cup 5 body, grips rock core 8 in the middle part of described two fixed supports 6; Described computer acquisition system 1 connects collection electronic balance 3; Described electronic balance 3 precision is 0.0001g; Closed box 2 is made up of the glass that light transmission, thermotolerance and intensity are good; Paddle 4, imbibition cup 5, fixed mount 6 and connecting link 9 are made by heat-proof corrosion resistant erosion metal material; Imbibition liquid 7 is filled in described imbibition cup 5.
When this novel imbibition experimental provision uses, imbibition cup is splendid attire imbibition liquid and experiment rock core in experimentation; Described closed box is used for placing all devices except computer acquisition system, with the interference preventing the factor such as air vapor and external shock from producing; Computer acquisition system in order to gather the electronic balance registration in different imbibition moment, and then calculates core quality change; Paddle rises and stirs imbibition liquid, utilizes the flowing of imbibition liquid to remove and is attached to the bubble of core surface and the effect of oil droplet; Imbibition cup splendid attire and heating imbibition liquid; Coupling arrangement is in order to connect electronic balance and imbibition rock core.
Concrete operation step is:
(1) start-up simulation machine acquisition system 1, debugging electronic balance 3;
(2) imbibition liquid is poured into (liquid volume is no more than container volume 2/3) in imbibition cup, heating imbibition liquid 7 to target reservoir temperature;
(3) utilize connecting link 9 to connect the rock core 8 of electronic balance 3 and saturated crude oil, subsequently rock core is put into imbibition liquid, start imbibition experiment and regularly gather electronic balance 3 registration by computer acquisition system 1;
(4) in experimentation, before each image data of computer acquisition system 1, first fixed support 6 is used to fix rock core, open the agitating function 60s of paddle 5 subsequently, when utilizing imbibition liquid to rotate, between itself and rock core, friction force eliminates the bubble and oil droplet that core surface adheres to, after each stopping stirring imbibition for seep recovery is static, unclamp fixed support 6, carry out core quality and weigh and data record;
(5) data of process computer acquisition system collection, calculate recovery of core, and then understanding imbibition rule.

Claims (3)

1. a novel imbibition experimental provision, comprise closed box (2), electronic balance (3) and imbibition cup (5), it is characterized in that: described closed box (2) middle part arranges dividing plate, described dividing plate is equipped with electronic balance (3), and electronic balance (3) connects rock core (8) by connecting link (9); Closed box (2) inner bottom part is equipped with imbibition cup (5), described imbibition cup (5) inner bottom part center is equipped with paddle (4), paddle (4) top imbibition cup (5) inner bottom part both sides are fixedly connected with fixed support (6), fixed support (6) passes perpendicularly through imbibition cup (5) sidewall by body of bolt and is connected on imbibition cup (5) body, and described two fixed supports (6) middle part grips rock core (8).
2. novel imbibition experimental provision according to claim 1, is characterized in that: described electronic balance (3) connects computer acquisition system (1).
3. novel imbibition experimental provision according to claim 1, is characterized in that: fill imbibition liquid (7) in described imbibition cup (5).
CN201520828223.7U 2015-10-23 2015-10-23 Novel imbibition experiment device Expired - Fee Related CN205038132U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520828223.7U CN205038132U (en) 2015-10-23 2015-10-23 Novel imbibition experiment device

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Application Number Priority Date Filing Date Title
CN201520828223.7U CN205038132U (en) 2015-10-23 2015-10-23 Novel imbibition experiment device

Publications (1)

Publication Number Publication Date
CN205038132U true CN205038132U (en) 2016-02-17

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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106706498A (en) * 2017-01-16 2017-05-24 哈尔滨工业大学 Steady state water permeability coefficient testing device and method of concrete type material
CN106769752A (en) * 2016-11-29 2017-05-31 中国石油大学(北京) Rotatable imbibition experimental provision
CN106841009A (en) * 2017-04-10 2017-06-13 中国石油大学(华东) A kind of experimental provision and method for vibrating auxiliary porous medium imbibition
CN107340223A (en) * 2017-08-15 2017-11-10 哈尔滨工业大学 The monitoring system and method for monitoring Concrete Material unstable state water permeability coefficient in real time
CN107607428A (en) * 2017-08-15 2018-01-19 哈尔滨工业大学 A kind of monitoring system and method for the Concrete Material water absorption rate of monitoring in real time
CN108195732A (en) * 2017-11-30 2018-06-22 中国石油天然气股份有限公司 A kind of compact rock core imbibition experimental provision and imbibition weight testing method
CN109374490A (en) * 2018-08-27 2019-02-22 中国石油大学(北京) Imbibition extraction equipment and imbibition extraction experiments method
CN109856030A (en) * 2019-02-15 2019-06-07 中国石油大学(北京) The determination method of imbibition experimental provision and imbibition recovery percent of reserves
CN110174430A (en) * 2019-06-03 2019-08-27 西南石油大学 The measuring device and method of rock core imbibition simulated experiment under a kind of high-temperature and high-pressure conditions
CN110470585A (en) * 2019-09-04 2019-11-19 西南石油大学 A kind of experiment test device and method of shale dynamic imbibition ability
CN111024545A (en) * 2019-12-02 2020-04-17 中国石油大学(北京) Extraction experiment system and extraction experiment method

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106769752A (en) * 2016-11-29 2017-05-31 中国石油大学(北京) Rotatable imbibition experimental provision
CN106706498A (en) * 2017-01-16 2017-05-24 哈尔滨工业大学 Steady state water permeability coefficient testing device and method of concrete type material
CN106841009A (en) * 2017-04-10 2017-06-13 中国石油大学(华东) A kind of experimental provision and method for vibrating auxiliary porous medium imbibition
CN106841009B (en) * 2017-04-10 2023-10-03 中国石油大学(华东) Experimental device and method for vibration-assisted porous medium imbibition
CN107340223A (en) * 2017-08-15 2017-11-10 哈尔滨工业大学 The monitoring system and method for monitoring Concrete Material unstable state water permeability coefficient in real time
CN107607428A (en) * 2017-08-15 2018-01-19 哈尔滨工业大学 A kind of monitoring system and method for the Concrete Material water absorption rate of monitoring in real time
CN108195732B (en) * 2017-11-30 2021-09-28 中国石油天然气股份有限公司 Compact rock core imbibition experimental device and imbibition amount testing method
CN108195732A (en) * 2017-11-30 2018-06-22 中国石油天然气股份有限公司 A kind of compact rock core imbibition experimental provision and imbibition weight testing method
CN109374490A (en) * 2018-08-27 2019-02-22 中国石油大学(北京) Imbibition extraction equipment and imbibition extraction experiments method
CN109856030A (en) * 2019-02-15 2019-06-07 中国石油大学(北京) The determination method of imbibition experimental provision and imbibition recovery percent of reserves
CN110174430A (en) * 2019-06-03 2019-08-27 西南石油大学 The measuring device and method of rock core imbibition simulated experiment under a kind of high-temperature and high-pressure conditions
CN110174430B (en) * 2019-06-03 2022-08-16 西南石油大学 Measuring device and method for core imbibition simulation experiment under high-temperature and high-pressure conditions
CN110470585A (en) * 2019-09-04 2019-11-19 西南石油大学 A kind of experiment test device and method of shale dynamic imbibition ability
US11009443B2 (en) 2019-09-04 2021-05-18 Southwest Petroleum University Method for dynamic imbibition capacity of shale
CN111024545A (en) * 2019-12-02 2020-04-17 中国石油大学(北京) Extraction experiment system and extraction experiment method

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Granted publication date: 20160217

Termination date: 20161023