CN204911487U - High -efficient general many functional response cauldron device - Google Patents
High -efficient general many functional response cauldron device Download PDFInfo
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- CN204911487U CN204911487U CN201520511724.2U CN201520511724U CN204911487U CN 204911487 U CN204911487 U CN 204911487U CN 201520511724 U CN201520511724 U CN 201520511724U CN 204911487 U CN204911487 U CN 204911487U
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Abstract
The utility model provides a high -efficient general many functional response cauldron device, is including jar body and a PLC program controller, jar internal circulating water cooling coil pipe that is equipped with the heat conduction oil coil pipe who has oil inlet and oil -out and has water inlet and delivery port, heat conduction oil coil pipe's oil inlet is connected with hot oil sources of thermal conductance and cold heat conduction oil sources through hot oil valve of thermal conductance and cold heat conduction oil valve respectively, the water inlet of circulating water cooling coil pipe passes through inlet valve and is connected with the water source, the internal survey temperature regulating device who is provided with the agitating unit who is connected with PLC program controller and is connected with PLC program controller of jar, jar body top is equipped with circulation condenser and raw materials import, is equipped with the regulation and control valve that prevents the discharge gate and block up bottom the jar is personally experienced sth. Part of the body. The utility model discloses can extensively be used for various through the synthetic chemical products of chemical reaction production and liquid material and liquid through various viscosity, solid -state mixtures homogenization is composite and the various production methods such as production of formation product.
Description
Technical field
The utility model belongs to technical field of fine, is specifically related to a kind of for fine chemical product synthesis and composite novel universal polyfunctional reactant kettle device.
Background technology
Reactor apparatus system is the equipment that chemical industry is commonly used, and generally comprises reactor tank body and the heating be connected with reactor by pipeline, the facilities such as cooling.Tank body top usual She Zhi You rotation flow condenser and escaping gas separated and collected device; Tank interior does not also have homogenizing material to promote the agitator of the various types of chemical reaction.Needs are reacted in certain temperature range, circulating-heating is also set in tank body and surveys temperature regulating device.
But the configuration of the reactor device that current chemical industry is used and function are all more single, and versatility is poor, result of use is general, and operation modulation process is complicated, and device is safeguarded inconvenient.Therefore, for the production of the fine chemical product of some new and high technology types, often band is served product quality and yield rate and is difficult to promote, problems.And dissimilar reactor device to be used to produce for different new high-tech product.Therefore enterprise operation high cost is caused, uneconomical.
As the example of reactor device with the problems referred to above and defect, following three kinds can be enumerated and be explained.The first has the reactor of heating and cooling device, its temperature adjusting of such still usual applying high voltage high-temperature steam circulating-heating reaction mass synthesis chemical products is easier to, but under high-temperature situation (as about 200 DEG C), such reactor equipment safety hidden danger is larger.They are two years old, heated up by conduction oil circulating-heating in still internal jacket, the synthetic reaction that needs at high temperature to carry out can be made easy to implement, but its greatest drawback is to give realization to having reacted the technological process difficulty that rear urgent need cools fast, thus product quality and yield rate can be had influence on.It three is that agitator type structure in reactor device and application function are more single, as more for low viscosity material stirring homogenizing dynamics, but it is just very poor to high viscosity liquid material or liquid, solid-state mixed material stirring dispersion homogenizing dynamics, thus some harmful side reaction will be caused to occur, and then affect quality and the yield rate of some fine chemical product, as to get rid of the problems referred to above just must separately change a kind of have produce compared with the reactor of strong mixing dynamics.
In addition, the reactor device that current chemical industry uses also has a fatal defect, namely reacting tank body goes out item when producing high-viscosity chemical product, because dropping into the high viscosity liquid material in tank body, especially high-melting-point solid material, easily at the chemical reaction initial stage, mid-term, because temperature does not reach solution temperature, in addition dynamics is stirred inadequate, thus cause solid-liquid material to be difficult to disperse homogenizing, so in intensification and stir blind area and material outlet and valve cavity place, the solid-state material deposition of easy generation herein, in addition easily there is parcel and even tie lump phenomenon together with high viscosity liquid material, thus easily there is blocking discharging opening and valve cavity, so when chemical products produce end and discharging is filling, steel fibre must be used to dredge discharging opening and valve by artificial.The method often causes high-temperature material to spray the serious accident injuring human body instantaneously.
Utility model content:
For solving the problem, the utility model provides a kind of efficient general polyfunctional reactant kettle device, various operation function rationally can be superposed cooperation and reaches efficient regulation and control reaction temperature fast and improve the operational effects such as homogenizing dynamics by this device, thus realize abolishing conventional reactor device system kinetic energy single with variety classes chemical production technology parameter adaptation the chronic disease such as not good enough, improve the extensive use of reactor device further and improve the quality of products and yield rate.
The technical solution adopted in the utility model is as follows: a kind of efficient general type polyfunctional reactant kettle device, comprises in tank body and PLC cyclelog tank body and is provided with the conduction oil coil pipe with oil-in and oil-out and the circulating water coil pipe with water inlet and delivery port; The oil-in of conduction oil coil pipe is connected with thermal conductance deep fat source and cold heat conduction oil sources with cold conduction oil valve respectively by thermal conductance deep fat valve; The water inlet of circulating water coil pipe is connected with water source by inlet valve; The agitating device be connected with PLC cyclelog and the survey temperature regulating device be connected with PLC cyclelog is provided with in tank body; Be provided with cycle condenser and material inlet above tank body, tank base is provided with the control valve preventing discharging opening from blocking; Described control valve comprises valve body, is arranged on the circular arc type seal cover at valve body top, the connecting rod be connected with circular arc type seal cover and the driving mechanism be connected with connecting rod.
Described circular arc type seal cover is provided with for contacting with valve body and the sealing ring sealed.
The mobile modulator that described driving mechanism is in transmission connection by handle and handle forms.
This valve top is directly connected with tank body discharging opening, valve top is provided with arc-shaped tile-type seal cover, and its diameter is greater than tank body inner outlet diameter, and this lid is connected on valve cavity eccentric wheel by link rod, and can be moved up and down by regulation device, guarantee that discharging opening is accurately opened and closes.
Described agitating device by the motor be connected with PLC cyclelog, the shaft be connected with motor-driven, be fixedly connected on the translamella oar on shaft and the anchor formula oar be fixedly connected bottom shaft forms.
The described translamella oar be fixedly connected on shaft is two, and translamella oar is positioned at above anchor formula oar, and one of them translamella oar is positioned at the first half of tank interior, and another translamella oar is positioned at the Lower Half of tank interior.
Described tank body top is provided with cycle condenser and volatile gas collection device.
Described cycle condenser and volatile gas collection utensil have a common cavity, cavity and reacting tank body UNICOM, cavity bottom is provided with condensate outlet, and cavity has cooling water inlet and coolant outlet, is provided with the cooling coil be communicated with coolant outlet with cooling water inlet respectively in cavity.
The beneficial effects of the utility model have:
Reactor apparatus structure is reasonable in design, and pipeline is well-equipped and adopt the functionality advantage of at present conventional reactor device and superposed, Full-automatic continuous control manipulation, so operation is flexible, and failure rate is low and easy to maintenance.
This reactor device can realize safety and environmental protection formula and produce, and a still is multiplex thus improve the quality of product and yield rate, and manufacturing enterprise's technical economic benefit is significantly promoted.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Fig. 2 is the structural representation of the control valve that the utility model prevents discharging opening from blocking.
Detailed description of the invention
Do to set forth further to the utility model below in conjunction with accompanying drawing:
As shown in Figure 1, the utility model includes tank body 1 and PLC cyclelog 11, is provided with the conduction oil coil pipe 20 with oil-in 18 and oil-out 19 and the circulating water coil pipe 21 with water inlet 16 and delivery port 17 in tank body 1; The oil-in 18 of conduction oil coil pipe 20 is connected with thermal conductance deep fat source and cold heat conduction oil sources with cold conduction oil valve 23 respectively by thermal conductance deep fat valve 8; The oil-out 19 of conduction oil coil pipe 20 is connected with thermal conductance deep fat source or cold heat conduction oil sources by valve 9; The water inlet 16 of circulating water coil pipe 21 is connected with water source by inlet valve 6, and the delivery port 17 of circulating water coil pipe 21 is connected with outlet pipe 22 by flowing water Valve 7; The agitating device 2 be connected with PLC cyclelog 11 and the survey temperature regulating device 10 be connected with PLC cyclelog 11 is provided with in tank body 1; Be provided with cycle condenser 12 and material inlet 4 above tank body 1, bottom tank body 1, be provided with the control valve 5 preventing discharging opening from blocking; As shown in Figure 2, described control valve 5 comprise valve body 5.3, be arranged on the circular arc type seal cover 5.1 at valve body top, the connecting rod 5.4 be connected with circular arc type seal cover and the driving mechanism be connected with connecting rod 5.4.Circular arc type seal cover 5.1 is provided with for contacting with valve body 5.3 and the sealing ring 5.2 sealed.Described driving mechanism can adopt the mobile modulator 5.5 making it move up and down by handle 5.6.
Described agitating device 2 by the motor 3 be connected with PLC cyclelog 11, the shaft be in transmission connection with motor 3, be fixedly connected on the translamella oar on shaft and the anchor formula oar be fixedly connected bottom shaft forms.
The described translamella oar be fixedly connected on shaft is two, and translamella oar is positioned at above anchor formula oar, and one of them translamella oar is positioned at the first half of tank interior, and another translamella oar is positioned at the Lower Half of tank interior.
Described tank body top is provided with cycle condenser and volatile gas collection device.
Described cycle condenser and volatile gas collection utensil have a common cavity 12, cavity 12 is communicated with tank body 1, condensate outlet 15 is provided with bottom cavity 12, cavity 12 has cooling water inlet 13 and coolant outlet 14, is provided with the cooling coil be communicated with coolant outlet 14 with cooling water inlet 13 respectively in cavity 12.
In the utility model, each pipeline all can be connected with PLC cyclelog, is controlled the automatic running status of adjustment whole system by PLC.
The advantage of various agitating devices used for current reactor superposes by agitating device of the present utility model, learns from other's strong points to offset one's weaknesses, upgrading, thus well can adapt to the manufacturing technique requirent of different fine chemicals.
The utility model can solve General reactions still temperature control and stir the problem that homogenizing blind area easily produces high viscosity liquid, solid material produces glue link lump in tank base exit and discharging control valve door cavity, thus make the utility model when producing the chemical products of any state, can not produce because of discharge blockage cause serious accident and affect the accident of product quality.
The utility model by PLC cyclelog, by temperature adjusting, stirs dynamics regulation and control and the regulation and control of reactor top condensation cycle and volatile gas collection device and the regulation and control etc. of critical valves, forms logic, regulate and control operation automatically by controller by programming.Thus making whole reactor apparatus body tie up in chemical products production process, safe operation, guarantees the lifting of product quality and yield rate.
When the utility model is used for the synthesis production of fine chemical product, first the discharging opening control valve 5 of tank base is closed, then PLC cyclelog 11 is started, restart agitating device 2 and agitating device regulation and control drive motors in reactor subsequently, 3 and heater terminal valve 6 and 7 and survey temperature regulating device 10.Followed by material inlet on tank body 4, by the order of throwing solid feed after first throwing liquid material, add synthetic reaction material; After material adds, add a cover closed charging aperture immediately, the cold water terminal valve 13 and 14 of the cycle condenser mouth on unlatching tank body top carries out the volatile material liquefied that condensation cycle is guaranteed to generate in synthetic reaction simultaneously, then is recycled by recovery tube 15.
When synthetic reaction material, especially full-bodied liquid, solid-state compound, at the preliminary stage of temperature reaction, due to the adhesion of liquid, solid material, when wrapping up and be difficult to dispersion homogenizing, the power of the drive motors of available PLC regulation and control agitator, to increase stirring dynamics, thus reaches the required limit of processing parameter and optimizes reaction process.
After reaction mass synthesis reaction temperature reaches the high-temperature area of production technology setting, can in time by surveying the temperature of temperature regulating device and heater appropriateness adjustment heat medium, thus the temperature of reaction mass is controlled within the temperature range of best production technology defined, and stop the high-temperature oxydation because temperature of charge retardation change and bounce-back cause with this, the appearance of the negative reactions such as polymerization.
It should be noted that the control valve that conscientiously must to make to make good use of the utility model when carrying out sintetics with high-viscosity material and high melting-point solid material in this reactor and prevent discharging opening from blocking.Before feeding intake, first thoroughly clean up reactor inner chamber, then move down mobile modulator closed seal cover on discharging opening with hand is bright, for the material having Acidity of Aikalinity and pyroreaction, preferably select the sealing ring of fit on acid and alkali-resistance and high temperature.After synthetic reaction terminates, close pipeloop and running gear, start modulator with handle, move on seal cover connecting rod, make seal cover moves and depart from discharging oral thermometer face and transverse shifting at a certain angle, thoroughly open discharging opening blowing.
Through field sampling inspection, after preliminary judgement synthetic reaction completes substantially, being opened by PLC immediately can the tank inner coil pipe cooling device of high efficiency cooling material, carries out Rapid Circulation cooling.
In order to accelerate material cooling velocity in tank, avoid the various adverse reactions that the high temperature of instantaneous bounce-back may cause as far as possible, while coil pipe water-cooled, started by PLC extent control device again and adjust temperature regulating device, high-temperature hot oil medium is pumped from tank internal jacket, and the cold conduction oil of importing carries out pipeline circulating cooling in time, till synthesis material reaches the temperature required by production technology.
After synthetic reaction completes, close pipeloop and running gear, open discharging opening control valve, qualified production product after inspection is carried out canned.
Above efficient general multifunctional reaction still apparatus system provided by the utility model is described in detail, and only application specific case has carried out some explanations to principle of the present utility model and embodiment, it is just for helping those skilled in the art to understand method of the present utility model and core concept, simultaneously can according to thinking of the present utility model, can do some to change in detailed description of the invention and range of application, but these still belong within the special interest field of utility model.In sum, content of the present utility model should not be construed as restriction of the present utility model.
Claims (7)
1. an efficient general polyfunctional reactant kettle device, comprises tank body and PLC cyclelog, it is characterized in that: be provided with the conduction oil coil pipe with oil-in and oil-out and the circulating water coil pipe with water inlet and delivery port in tank body; The oil-in of conduction oil coil pipe is connected with thermal conductance deep fat source and cold heat conduction oil sources with cold conduction oil valve respectively by thermal conductance deep fat valve; The water inlet of circulating water coil pipe is connected with water source by inlet valve; The agitating device be connected with PLC cyclelog and the survey temperature regulating device be connected with PLC cyclelog is provided with in tank body; Be provided with cycle condenser and material inlet above tank body, tank base is provided with the control valve preventing discharging opening from blocking; Described control valve comprises valve body, is arranged on the circular arc type seal cover at valve body top, the connecting rod be connected with circular arc type seal cover and the driving mechanism be connected with connecting rod.
2. efficient general polyfunctional reactant kettle device according to claim 1, is characterized in that: described circular arc type seal cover is provided with for contacting with valve body and the sealing ring sealed.
3. efficient general polyfunctional reactant kettle device according to claim 1 and 2, is characterized in that: the mobile modulator that described driving mechanism is in transmission connection by handle and handle forms.
4. efficient general polyfunctional reactant kettle device according to claim 1 and 2, is characterized in that: described agitating device by the motor be connected with PLC cyclelog, the shaft be connected with motor-driven, be fixedly connected on the translamella oar on shaft and the anchor formula oar be fixedly connected bottom shaft forms.
5. efficient general polyfunctional reactant kettle device according to claim 4, it is characterized in that: the translamella oar be fixedly connected on shaft is two, translamella oar is positioned at above anchor formula oar, and one of them translamella oar is positioned at the first half of tank interior, another translamella oar is positioned at the Lower Half of tank interior.
6. efficient general polyfunctional reactant kettle device according to claim 1 and 2, is characterized in that: tank body top is provided with cycle condenser and volatile gas collection device.
7. efficient general polyfunctional reactant kettle device according to claim 6, it is characterized in that: described cycle condenser and volatile gas collection utensil have a common cavity, cavity and tank body UNICOM, cavity bottom is provided with condensate outlet, cavity has cooling water inlet and coolant outlet, is provided with the cooling coil be communicated with coolant outlet with cooling water inlet respectively in cavity.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520511724.2U CN204911487U (en) | 2015-07-15 | 2015-07-15 | High -efficient general many functional response cauldron device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520511724.2U CN204911487U (en) | 2015-07-15 | 2015-07-15 | High -efficient general many functional response cauldron device |
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| Publication Number | Publication Date |
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| CN204911487U true CN204911487U (en) | 2015-12-30 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201520511724.2U Expired - Fee Related CN204911487U (en) | 2015-07-15 | 2015-07-15 | High -efficient general many functional response cauldron device |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107987811A (en) * | 2017-12-07 | 2018-05-04 | 联技精细材料(珠海)有限公司 | A kind of inexpensive emulsifying agent applied to oil base drilling fluid and preparation method thereof |
| CN108620015A (en) * | 2018-07-20 | 2018-10-09 | 广西壮族自治区农业科学院 | A kind of liquid selenium-rich nutritive chelating fertilizer reaction kettle |
| CN110302736A (en) * | 2019-08-07 | 2019-10-08 | 上海蓝科石化环保科技股份有限公司 | Exchange heat polymerization reaction system and method in a kind of kettle for strongly exothermic polymerization reaction |
-
2015
- 2015-07-15 CN CN201520511724.2U patent/CN204911487U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107987811A (en) * | 2017-12-07 | 2018-05-04 | 联技精细材料(珠海)有限公司 | A kind of inexpensive emulsifying agent applied to oil base drilling fluid and preparation method thereof |
| CN108620015A (en) * | 2018-07-20 | 2018-10-09 | 广西壮族自治区农业科学院 | A kind of liquid selenium-rich nutritive chelating fertilizer reaction kettle |
| CN110302736A (en) * | 2019-08-07 | 2019-10-08 | 上海蓝科石化环保科技股份有限公司 | Exchange heat polymerization reaction system and method in a kind of kettle for strongly exothermic polymerization reaction |
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| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151230 Termination date: 20170715 |
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| CF01 | Termination of patent right due to non-payment of annual fee |