CN216224335U

CN216224335U - Temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis material

Info

Publication number: CN216224335U
Application number: CN202121710485.5U
Authority: CN
Inventors: 朱凯成; 王晓莹
Original assignee: Nanjing Bolton Fuzhe Material Technology Co ltd
Current assignee: Nanjing Bolton Fuzhe Material Technology Co ltd
Priority date: 2021-07-27
Filing date: 2021-07-27
Publication date: 2022-04-08
Anticipated expiration: 2031-07-27

Abstract

The utility model relates to the technical field of reaction kettles, in particular to a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials, which comprises a reaction kettle body, wherein the surface of the reaction kettle body is detachably connected with a reaction kettle cover, the surface of the reaction kettle body is fixedly connected with a reaction kettle jacket, the inner wall of the reaction kettle cover is fixedly embedded with a temperature sensor, the inner wall of the reaction kettle cover is fixedly embedded with a pressure sensor, one side of the reaction kettle cover, which is far away from the reaction kettle jacket, is detachably connected with a speed reducer through a bolt, the surface of the reaction kettle body is provided with a temperature adjusting device, and the surface of the reaction kettle body is provided with a supporting device. The utility model has the functions of temperature regulation and convenient cleaning on the basis of a common reaction kettle, and solves the defects that the temperature is difficult to regulate and the biomass MOFs is easy to adsorb on the inner wall of the reaction kettle in the heating reaction process of the biomass MOFs.

Description

Temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis material

Technical Field

The utility model relates to the technical field of reaction kettles, in particular to a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials.

Background

The reaction kettle is widely applied to the fields of petroleum, chemical industry, rubber, pesticides, dyes, medicines, foods and the like, and is a pressure container for completing technological processes of vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposition kettle, a polymerization kettle and the like; the material is generally carbon manganese steel, stainless steel, zirconium, nickel-based (Hastelloy, Monel, Inconel) alloy and other composite materials.

Reation kettle on the existing market is difficult to adjust the temperature in carrying out the heating reaction process to living beings MOFs, when carrying out different reaction experiments, needs to be different to the height of temperature, is carrying out the heating process in, and living beings MOFs adsorbs easily at reation kettle's inner wall, needs the manual work to clear up.

SUMMERY OF THE UTILITY MODEL

To solve the problems set forth in the background art described above. The utility model provides a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials, which has the functions of temperature adjustment and convenience in cleaning and solves the defects that the temperature is difficult to adjust and the biomass MOFs are easy to adsorb on the inner wall of the reaction kettle in the process of heating the biomass MOFs.

In order to achieve the purpose, the utility model adopts the following technical scheme:

a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials is designed, and comprises a reaction kettle body, wherein a reaction kettle cover is detachably connected to the surface of the reaction kettle body, a reaction kettle jacket is fixedly connected to the surface of the reaction kettle body, a plurality of supporting legs are fixedly connected to the surface of the reaction kettle jacket, a temperature sensor is fixedly embedded in the inner wall of the reaction kettle cover, a pressure sensor is fixedly embedded in the inner wall of the reaction kettle cover, a speed reducer is detachably connected to one side, away from the reaction kettle jacket, of the reaction kettle cover through a bolt, a motor is detachably connected to one side, away from the reaction kettle cover, of the speed reducer through a bolt, a rotating shaft is fixedly connected to an output shaft of the motor, one end of the rotating shaft is connected with a detachable connecting shaft of the speed reducer, and a coupler is detachably connected to an output shaft of the speed reducer, the detachable bull stick that is connected with of inner wall of shaft coupling, the fixed surface of bull stick is connected with cauldron wall cleaning device, the fixed surface of reation kettle cover is connected with the feed inlet, the surface of feed inlet is rotated and is connected with the closing cap, the surface of the reation kettle cauldron body is equipped with temperature regulation apparatus, the surface of the reation kettle cauldron body is equipped with strutting arrangement, the fixed inlaying of inner wall of the reation kettle cauldron body has the discharge gate.

Preferably, cauldron wall cleaning device is including solid fixed ring, stirring vane and clearance board, the fixed surface of bull stick is connected with a plurality of solid fixed rings, gu fixed ring's surperficial symmetry fixedly connected with stirring vane, one side fixedly connected with clearance board that solid fixed ring was kept away from to stirring vane.

Preferably, the quantity of cleaning plate is four, one side that stirring vane was kept away from to the cleaning plate is the laminating design with the inner wall of the reation kettle cauldron body.

Preferably, the temperature regulation device comprises a partition plate, heating pipes, a heating oil inlet pipe, a heating oil outlet pipe and a cooling water circulation pipe, the fixed surface of the reaction kettle body is connected with a plurality of partition plates, the symmetrical surface of the reaction kettle body is fixedly connected with a plurality of heating pipes, the symmetrical surface of the reaction kettle jacket is fixedly connected with a heating oil inlet pipe, the symmetrical surface of the reaction kettle jacket is fixedly connected with a heating oil outlet pipe, the symmetrical surface of the reaction kettle body is fixedly connected with a cooling water circulation pipe, and two ends of the cooling water circulation pipe penetrate through the reaction kettle jacket.

Preferably, the supporting device comprises a fixing plate, a supporting frame and a mounting hole, the surface of the reaction kettle jacket is fixedly connected with a plurality of fixing plates, one side of each fixing plate, far away from the reaction kettle jacket, is fixedly connected with the supporting frame, and one side of each supporting frame is provided with the mounting hole.

Preferably, the reaction kettle body and the reaction kettle cover are both made of carbon steel, and the reaction kettle jacket is made of heat insulation materials.

Compared with the prior art, the utility model has the beneficial effects that:

1. through setting up temperature sensor and pressure sensor, be convenient for carry out can real-time detection to the internal atmospheric pressure and the temperature of reation kettle cauldron, through setting up feed inlet and closing cap, be convenient for put into the material of waiting to react, the material after the reaction is discharged from the discharge gate, through setting up the reduction gear, the shaft coupling of the internal portion of reation kettle is driven to motor and pivot, the bull stick, gu fixed ring, stirring vane and cleaning plate cleaning device rotate the stirring and be convenient for the material to carry out more evenly that mixes, the material of being convenient for heats, can not cause the material temperature to differ and lead to the fact the inhomogeneous phenomenon of heating, be convenient for clear up the cauldron wall, prevent that long-time material from solidifying and being difficult to clear up on the cauldron wall, perhaps open the reation kettle lid and clear up the internal portion of reation kettle.

2. When needs heat, inject into heating oil through the heating oil inlet pipe toward reation kettle cauldron body and reation kettle between pressing from both sides the cover, then heat the heating oil through the heating pipe and heat up, material heating to the internal portion of reation kettle cauldron through the heat transfer, when needs cool down, be connected with devices such as outside water pump and water tower through the both ends with the cooling water circulating pipe, then cool down the reation kettle cauldron body through the inside cooling water circulation of cooling water circulating pipe, also can adjust through the temperature of adjusting the heating pipe, dual cooling mode cools down, the temperature regulation of being convenient for, be suitable for the temperature that the different reaction times of material needs, through setting up the heating oil discharging pipe, be convenient for change the processing to heating oil.

The parts of the device not involved are the same as or can be implemented using prior art.

Drawings

The accompanying drawings, which are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate embodiments of the utility model and together with the description serve to explain the principles of the utility model and not to limit the utility model. In the drawings:

FIG. 1 is a structural front view of a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials, which is provided by the utility model;

FIG. 2 is a cross-sectional view of a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials, which is provided by the utility model;

FIG. 3 is a front sectional view of a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials, which is provided by the utility model;

FIG. 4 is a sectional plan view of a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials, which is provided by the utility model;

FIG. 5 is a schematic structural surface view of a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials provided by the utility model.

In the figure: the device comprises a reaction kettle body 1, a reaction kettle cover 2, a

reaction kettle jacket

3, 4 supporting legs, 5 temperature sensors, 6 pressure sensors, 7 speed reducers, 8 motors, 9 rotating shafts, 10 couplers, 11 rotating rods, 12 fixing rings, 13 stirring blades, 14 cleaning plates, 15 feed inlets, 16 sealing covers, 17 partition plates, 18 heating pipes, 19 heating oil feed pipes, 20 heating oil discharge pipes, 21 cooling water circulating pipes, 22 fixing plates, 23 supporting frames, 24 mounting holes and 25 discharge outlets.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1-5, a temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials comprises a reaction kettle body 1, a reaction kettle cover 2 detachably connected to the surface of the reaction kettle body 1, a reaction kettle jacket 3 fixedly connected to the surface of the reaction kettle body 1, a plurality of support legs 4 fixedly connected to the surface of the reaction kettle jacket 3, a temperature sensor 5 fixedly embedded in the inner wall of the reaction kettle cover 2, a pressure sensor 6 fixedly embedded in the inner wall of the reaction kettle cover 2, a reducer 7 detachably connected to one side of the reaction kettle cover 2 away from the reaction kettle jacket 3 through bolts, a motor 8 detachably connected to one side of the reducer 7 away from the reaction kettle cover 2 through bolts, a rotating shaft 9 fixedly connected to an output shaft of the motor 8, one end of the rotating shaft 9 detachably connected to a connecting shaft of the reducer 7, and a coupler 10 detachably connected to an output shaft of the reducer 7, the detachable bull stick 11 that is connected with of inner wall of shaft coupling 10, the fixed surface of bull stick 11 is connected with cauldron wall cleaning device, and the fixed surface of reation kettle cover 2 is connected with feed inlet 15, and the surperficial rotation of feed inlet 15 is connected with closing cap 16, and the surface of the reation kettle body 1 is equipped with temperature regulation apparatus, and the surface of the reation kettle body 1 is equipped with strutting arrangement, and the fixed inlaying of the inner wall of the reation kettle body 1 has discharge gate 25. Through setting up temperature sensor 5 and pressure sensor 6, be convenient for carry out can real-time detection to the atmospheric pressure and the temperature of the internal portion of reation kettle cauldron, through setting up feed inlet 15 and closing cap 16, be convenient for put into the material of treating the reaction, the material after the reaction is discharged from discharge gate 25, through setting up reduction gear 7, motor 8 and pivot 9 drive the shaft coupling 10, bull stick 11 and the cauldron wall cleaning device of the internal portion of reation kettle cauldron 1 and rotate the stirring material.

In order to better stir the materials and clean the kettle wall; specifically, cauldron wall cleaning device is including solid fixed ring 12, stirring vane 13 and clearance board 14, and the fixed surface of bull stick 11 is connected with a plurality of solid fixed rings 12, and solid fixed ring 12's fixed surface symmetry fixedly connected with stirring vane 13, one side fixedly connected with clearance board 14 that solid fixed ring 12 was kept away from to stirring vane 13. Through setting up solid fixed ring 12 and stirring vane 13 and stirring the material, the material of being convenient for carries out mixing more evenly, and the material heating of being convenient for can not cause the material temperature to differ and lead to the fact the inhomogeneous phenomenon of heating, through setting up cleaning plate 14, is convenient for clear up the cauldron wall, prevents that long-time material from solidifying and being difficult to clear up on the cauldron wall.

Specifically, the quantity of cleaning plate 14 is four, and one side that stirring vane 13 was kept away from to cleaning plate 14 is the laminating design with the inner wall of the reation kettle cauldron body 1. The cleaning of four cleaning plates 14 is more convenient, and the laminating design is more comprehensive.

In order to regulate the temperature of the material; specifically, temperature regulation apparatus includes baffle 17, heating pipe 18, add hot oil inlet pipe 19, add hot oil discharging pipe 20 and cooling water circulating pipe 21, the fixed surface of the reation kettle body 1 is connected with a plurality of baffles 17, the fixed surface of the reation kettle body 1 is connected with a plurality of heating pipes 18, the fixed surface of the symmetrical fixed surface of the reation kettle jacket 3 is connected with hot oil inlet pipe 19, the fixed surface of the symmetrical fixed surface of the reation kettle jacket 3 is connected with hot oil discharging pipe 20, the fixed surface of the symmetrical surface of the reation kettle body 1 is connected with cooling water circulating pipe 21, reation kettle jacket 3 is all run through at the both ends of cooling water circulating pipe 21. When needs heat, it adds hot oil to pour into through heating oil inlet pipe 19 toward reation kettle cauldron body 1 and reation kettle between pressing from both sides the cover 3, then heat the heating oil through heating pipe 18 and heat up, material heating to reation kettle cauldron body 1 inside through the heat transfer, when needs cool down, be connected with devices such as outside water pump and water tower through the both ends with cooling water circulating pipe 21, then cool down reation kettle cauldron body 1 through the inside cooling water circulation of cooling water circulating pipe 21, also can adjust through the temperature of adjusting heating pipe 18, dual cooling mode cools down, the temperature regulation of being convenient for, be suitable for the temperature that the different reaction of material needs, through setting up heating oil discharging pipe 20, be convenient for change the processing to heating oil.

In order to ensure that the reaction kettle is more stably installed; specifically, strutting arrangement includes fixed plate 22, support frame 23 and mounting hole 24, and the fixed surface that reation kettle pressed from both sides cover 3 is connected with a plurality of fixed plates 22, and the equal fixedly connected with support frame 23 in one side that reation kettle pressed from both sides cover 3 was kept away from to fixed plate 22, and mounting hole 24 has all been seted up to one side of support frame 23. Support reation kettle through setting up fixed plate 22 and support frame 23, through setting up mounting hole 24, cooperate with the bolt and install reation kettle, the installation is more stable.

Specifically, the reaction kettle body 1 and the reaction kettle cover 2 are made of carbon steel, the carbon steel is higher in hardness compared with other metals, the high-temperature resistant effect is achieved, the service life is longer, the reaction kettle jacket 3 is made of heat insulation materials, the temperature is prevented from being high, injury to personnel is avoided, and the use is safer.

The use principle and the use flow of the utility model are as follows: opening a sealing cover 16, putting biomass MOFs from a feeding hole 15, starting a motor 8, driving a coupler 10, a rotating rod 11, a fixing ring 12, a stirring blade 13 and a cleaning plate 14 to rotate through a speed reducer 7, stirring materials by arranging the fixing ring 12 and the stirring blade 13, cleaning the kettle wall by arranging the cleaning plate 14, detecting the air pressure and the temperature inside the kettle body 1 of the reaction kettle in real time by arranging a temperature sensor 5 and a pressure sensor 6, injecting heating oil between the kettle body 1 and a kettle jacket 3 through a heating oil feeding pipe 19 when heating is needed, heating the heating oil through a heating pipe 18, heating the materials inside the kettle body 1 of the reaction kettle through heat transfer, and connecting two ends of a cooling water circulating pipe 21 with devices such as an external water pump, a water tower and the like when cooling is needed, then cool down the reation kettle cauldron body 1 through the inside cooling water circulation of cooling water circulating pipe 21, also can adjust through the temperature of adjusting heating pipe 18, dual cooling mode cools down, through setting up heating oil discharging pipe 20, changes the processing to heating oil, supports reation kettle through setting up fixed plate 22 and support frame 23, through setting up mounting hole 24, cooperates with the bolt and installs reation kettle.

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the utility model. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. The temperature-adjustable reaction kettle for biomass MOFs adsorption-catalysis materials comprises a reaction kettle body (1) and is characterized in that a reaction kettle cover (2) is detachably connected to the surface of the reaction kettle body (1), a reaction kettle jacket (3) is fixedly connected to the surface of the reaction kettle body (1), a plurality of supporting legs (4) are fixedly connected to the surface of the reaction kettle jacket (3), a temperature sensor (5) is fixedly embedded in the inner wall of the reaction kettle cover (2), a pressure sensor (6) is fixedly embedded in the inner wall of the reaction kettle cover (2), a speed reducer (7) is detachably connected to one side, far away from the reaction kettle jacket (3), of the reaction kettle cover (2) through bolts, and a motor (8) is detachably connected to one side, far away from the reaction kettle cover (2), of the speed reducer (7), the output shaft of the motor (8) is fixedly connected with a rotating shaft (9), one end of the rotating shaft (9) is detachably connected with a connecting shaft of the speed reducer (7), the output shaft of the speed reducer (7) is detachably connected with a coupler (10), the inner wall of the coupler (10) is detachably connected with a rotating rod (11), the surface of the rotating rod (11) is fixedly connected with a kettle wall cleaning device, the surface of the reaction kettle cover (2) is fixedly connected with a feed inlet (15), the surface of the feed inlet (15) is rotatably connected with a sealing cover (16), the surface of the reaction kettle body (1) is provided with a temperature regulating device, the surface of the reaction kettle body (1) is provided with a supporting device, the inner wall of the reaction kettle body (1) is fixedly embedded with a discharge outlet (25), the kettle wall cleaning device comprises a fixing ring (12), stirring blades (13) and a cleaning plate (14), the surface of the rotating rod (11) is fixedly connected with a plurality of fixing rings (12), the surface of each fixing ring (12) is symmetrically and fixedly connected with a stirring blade (13), one side, far away from the fixing rings (12), of each stirring blade (13) is fixedly connected with a cleaning plate (14), each temperature adjusting device comprises a partition plate (17), a heating pipe (18), a heating oil inlet pipe (19), a heating oil outlet pipe (20) and a cooling water circulating pipe (21), the surface of the reaction kettle body (1) is fixedly connected with a plurality of partition plates (17), the surface of the reaction kettle body (1) is symmetrically and fixedly connected with a plurality of heating pipes (18), the surface of the reaction kettle jacket (3) is symmetrically and fixedly connected with heating oil inlet pipes (19), the surface of the reaction kettle jacket (3) is symmetrically and fixedly connected with heating oil outlet pipes (20), and the surface of the reaction kettle body (1) is symmetrically and fixedly connected with cooling water circulating pipes (21), both ends of the cooling water circulating pipe (21) penetrate through the jacket (3) of the reaction kettle.

2. The temperature-adjustable reaction kettle for the biomass MOFs adsorption-catalysis materials according to claim 1, wherein the number of the cleaning plates (14) is four, and one side of each cleaning plate (14) far away from the stirring blade (13) is in a fit design with the inner wall of the reaction kettle body (1).

3. The temperature-adjustable reaction kettle for the biomass MOFs adsorption-catalysis materials according to claim 1, wherein the supporting device comprises fixing plates (22), supporting frames (23) and mounting holes (24), the surfaces of the reaction kettle jackets (3) are fixedly connected with the fixing plates (22), the supporting frames (23) are fixedly connected to one sides of the fixing plates (22) far away from the reaction kettle jackets (3), and the mounting holes (24) are formed in one sides of the supporting frames (23).

4. The temperature-adjustable reaction kettle for the biomass MOFs adsorption-catalysis material according to claim 1, wherein the reaction kettle body (1) and the reaction kettle cover (2) are both made of carbon steel, and the reaction kettle jacket (3) is made of heat insulation material.