CN204799233U - Oxidation reaction unit with protect function - Google Patents
Oxidation reaction unit with protect function Download PDFInfo
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- CN204799233U CN204799233U CN201520470810.3U CN201520470810U CN204799233U CN 204799233 U CN204799233 U CN 204799233U CN 201520470810 U CN201520470810 U CN 201520470810U CN 204799233 U CN204799233 U CN 204799233U
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- cooling water
- tubulation
- catalyst layer
- reaction
- circulating cooling
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Abstract
The utility model discloses an oxidation reaction unit with protect function, including reactor noumenon and waste -heat oven steam pocket, the reactor noumenon package is established in the waste -heat oven steam pocket, and reactor has catalytic reaction zoon and establishes the quench zone in the catalytic reaction zoon lower part, and catalytic reaction zoon includes the catalyst layer, and the quench zone includes the tubulation cooler, is equipped with circulating cooling water pipe in the catalyst layer, and the recirculated cooling water groove is arranged in to the tubulation cooler, and gas uniform distributor is established to catalytic reaction zoon's top, the tubulation cooler includes a plurality of tubulations, is equipped with air current speed -raising stick in the tubulation. The utility model discloses can make the reaction gas evenly distributed who gets into reactor react in getting into the catalyst layer, moreover because being equipped with circulating cooling water pipe in the catalyst layer, can preventing that the catalyst layer is overheated, the recirculated cooling water groove is placed in to the tubulation cooler, can make reaction gas autocatalysis agent layer come out to cool off rapidly the 100 -130 degree and control, but can not reach higher temperature, has prevented that formaldehyde from taking place side reactions such as deep oxidation under high temperature.
Description
Technical field
The utility model belongs to silver-colored formaldehyde production technical field, is specifically related to a kind of oxidation reaction apparatus with defencive function.
Background technology
In the production process of silver legal system formaldehyde, air capacity, reaction effect between water vapour amount and methyl alcohol evaporation capacity have impact on efficiency and the quality of formaldehyde processed greatly, it directly affects the reaction temperature of oxidator, product quality, output, the consumption of raw material, the problem such as catalyst life and production safety, so just there is strict requirement to oxidator, the catalysis of silver method is due to variations in temperature, easily poly-reaction, cause occurring crack, affect production and the making of formaldehyde, wherein in oxidation reaction, the position of catalyst and oxidizing temperature change are sport technique segments particularly important in oxidation reaction, reaction temperature rises too fast, reaction speed is accelerated, but the too high meeting of reaction temperature causes side reaction to increase, impurity is too many, be unfavorable for that the life-span of catalyst is unfavorable, reaction temperature is too low, reaction speed is slower, do not reach productive target, so the control of oxidator also seems particularly important.
Utility model content
The purpose of this utility model is solve above-mentioned technical problem and provide a kind of oxidation reaction apparatus with defencive function preventing formaldehyde from the side reactions such as deep oxidation at high temperature occurring.
For achieving the above object, the utility model adopts following technical scheme:
A kind of oxidation reaction apparatus with defencive function, comprise reactor body and waste-heat oven drum, described reactor body is packaged in described waste-heat oven drum, described reactor body has reacting gas inlet, reaction gas outlet, there is in described reactor body catalyst reaction section and be located at the quench zone of described catalytic reaction pars infrasegmentalis, described catalyst reaction section comprises catalyst layer, described quench zone comprises tubulation cooler, circulating cooling water pipe is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank, the top of described catalyst reaction section is provided with even gas distribution device, described even gas distribution device is cone-shaped structure, surface is provided with multiple airflow hole, described tubulation cooler comprises multiple tubulation, is provided with gas flow speeding rod in described tubulation, and described tubulation and gas flow speeding rod are red copper material and make.
Described circulating cooling tank connects cooling water inlet and the coolant outlet of recirculated cooling water.
Described circulating cooling water pipe connects cooling water inlet and the coolant outlet of recirculated cooling water.
Described reacting gas inlet, reaction gas outlet are located on the sidewall of described reactor body respectively.
The utility model is packaged in described waste-heat oven drum by reactor body, there is catalyst reaction section in reactor and be located at the quench zone of described catalytic reaction pars infrasegmentalis, described catalyst reaction section comprises catalyst layer, described quench zone comprises tubulation cooler, circulating cooling water pipe is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank, the top of described catalyst reaction section is provided with even gas distribution device, described even gas distribution device is cone-shaped structure, surface is provided with multiple airflow hole, described tubulation cooler comprises multiple tubulation, gas flow speeding rod is provided with in described tubulation, described tubulation and gas flow speeding rod are red copper material and make, the reacting gas entered in reactor can be made to be uniformly distributed enter in catalyst layer to react, and owing to being provided with circulating cooling water pipe in described catalyst layer, catalyst layer can be prevented overheated, described tubulation cooler is placed in circulating cooling tank, reacting gas self-catalysis oxidant layer can be made out promptly to flow through in tubulation, improve heat exchange efficiency, and about being promptly cooled to 100-130 degree, but higher temperature can not be reached, formaldehyde is prevented at high temperature the side reactions such as deep oxidation to occur, effectively ensure that the quality of production of formaldehyde, there is great production practices and realistic meaning.
Accompanying drawing explanation
Figure 1 shows that a kind of structural representation with the oxidation reaction apparatus of defencive function that the utility model embodiment provides.
Detailed description of the invention
Below, in conjunction with example, substantive distinguishing features of the present utility model and advantage are further described, but the utility model is not limited to listed embodiment.
Refer to shown in Fig. 1, a kind of oxidation reaction apparatus with defencive function, comprise reactor body 1 and waste-heat oven drum 15, described reactor body 1 is packaged in described waste-heat oven drum 15, described reactor body has reacting gas inlet 2, reaction gas outlet 3, in described reactor body 1, there is catalyst reaction section and be located at the quench zone of described catalytic reaction pars infrasegmentalis, described catalyst reaction section comprises catalyst layer 13, be located in catalyst bed 6, described quench zone comprises tubulation cooler, circulating cooling water pipe 5 is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank 10, the top of described catalyst reaction section is provided with even gas distribution device 4, described even gas distribution device 4 is cone-shaped structure, surface is provided with multiple airflow hole, described tubulation cooler comprises multiple tubulation 14, is provided with gas flow speeding rod 9 in described tubulation 14, and described tubulation 14 is red copper material with gas flow speeding rod 9 and makes.
Described circulating cooling tank connects the cooling water inlet 11 of recirculated cooling water and the coolant outlet 12 of circulating cooling tank of circulating cooling tank.
Described circulating cooling water pipe connects the cooling water inlet 7 of recirculated cooling water and the coolant outlet 8 of circulating cooling water pipe of circulating cooling water pipe.
Described reacting gas inlet 2, reaction gas outlet 3 are located on the sidewall of described reactor body 1 respectively.
The utility model is packaged in waste-heat oven drum by reactor body, there is catalyst reaction section in reactor and be located at the quench zone of described catalytic reaction pars infrasegmentalis, described catalyst reaction section comprises catalyst layer, described quench zone comprises tubulation cooler, circulating cooling water pipe is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank, the top of described catalyst reaction section is provided with even gas distribution device, described even gas distribution device is cone-shaped structure, surface is provided with multiple airflow hole, described tubulation cooler comprises multiple tubulation, gas flow speeding rod is provided with in described tubulation, described tubulation and gas flow speeding rod are red copper material and make, the reacting gas entered in reactor can be made to be uniformly distributed enter in catalyst layer to react, and owing to being provided with circulating cooling water pipe in described catalyst layer, catalyst layer can be prevented overheated, described tubulation cooler is placed in circulating cooling tank, reacting gas self-catalysis oxidant layer can be made out promptly to flow through in tubulation, improve heat exchange efficiency, and about being promptly cooled to 100-130 degree, but higher temperature can not be reached, formaldehyde is prevented at high temperature the side reactions such as deep oxidation to occur, effectively ensure that the quality of production of formaldehyde, by reactor body being packaged in waste-heat oven drum, reactor body is surrounded wherein by waste-heat oven drum completely, can need not open reactor cap like this to carry out processing and directly producing when the short time stops, the temporary break of production can not be caused, there is great production practices and realistic meaning.
Although be described the utility model with reference to embodiment of the present utility model here, but, should be appreciated that, those skilled in the art can design a lot of other amendment and embodiment, these amendments and embodiment will drop within spirit disclosed in the present application and spirit.
More particularly, in the scope of, accompanying drawing open in the application and claim, multiple modification and improvement can be carried out to the building block of subject combination layout and/or layout.Except the modification of carrying out building block and/or layout is with except improvement, to those skilled in the art, other purposes also will be obvious.
Claims (4)
1. one kind has the oxidation reaction apparatus of defencive function, it is characterized in that, comprise reactor body and waste-heat oven drum, described reactor body is packaged in described waste-heat oven drum, described reactor body has reacting gas inlet, reaction gas outlet, there is in described reactor body catalyst reaction section and be located at the quench zone of described catalytic reaction pars infrasegmentalis, described catalyst reaction section comprises catalyst layer, described quench zone comprises tubulation cooler, circulating cooling water pipe is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank, the top of described catalyst reaction section is provided with even gas distribution device, described even gas distribution device is cone-shaped structure, surface is provided with multiple airflow hole, described tubulation cooler comprises multiple tubulation, is provided with gas flow speeding rod in described tubulation, and described tubulation and gas flow speeding rod are red copper material and make.
2. have the oxidation reaction apparatus of defencive function as claimed in claim 1, it is characterized in that, described circulating cooling tank connects cooling water inlet and the coolant outlet of recirculated cooling water.
3. have the oxidation reaction apparatus of defencive function as claimed in claim 2, it is characterized in that, described circulating cooling water pipe connects cooling water inlet and the coolant outlet of recirculated cooling water.
4. have the oxidation reaction apparatus of defencive function as claimed in claim 3, it is characterized in that, described reacting gas inlet, reaction gas outlet are located on the sidewall of described reactor body respectively.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520470810.3U CN204799233U (en) | 2015-06-26 | 2015-06-26 | Oxidation reaction unit with protect function |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520470810.3U CN204799233U (en) | 2015-06-26 | 2015-06-26 | Oxidation reaction unit with protect function |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204799233U true CN204799233U (en) | 2015-11-25 |
Family
ID=54584125
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520470810.3U Expired - Fee Related CN204799233U (en) | 2015-06-26 | 2015-06-26 | Oxidation reaction unit with protect function |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204799233U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114797691A (en) * | 2022-05-09 | 2022-07-29 | 漳州市龙文翰苑化工有限公司 | Oxidation reactor and process for formaldehyde production |
-
2015
- 2015-06-26 CN CN201520470810.3U patent/CN204799233U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114797691A (en) * | 2022-05-09 | 2022-07-29 | 漳州市龙文翰苑化工有限公司 | Oxidation reactor and process for formaldehyde production |
| CN114797691B (en) * | 2022-05-09 | 2024-02-27 | 漳州市龙文翰苑化工有限公司 | Oxidation reactor and process for formaldehyde production |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151125 Termination date: 20170626 |