CN204799231U - Oxidation reactor is used in formaldehyde production - Google Patents

Oxidation reactor is used in formaldehyde production Download PDF

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Publication number
CN204799231U
CN204799231U CN201520470808.6U CN201520470808U CN204799231U CN 204799231 U CN204799231 U CN 204799231U CN 201520470808 U CN201520470808 U CN 201520470808U CN 204799231 U CN204799231 U CN 204799231U
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CN
China
Prior art keywords
cooling water
catalyst layer
circulating cooling
reaction
reactor
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Expired - Fee Related
Application number
CN201520470808.6U
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Chinese (zh)
Inventor
刘建
黄贵柱
刘超然
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianjin Fulin Chaoran Technology Development Co Ltd
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Tianjin Fulin Chaoran Technology Development Co Ltd
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Priority to CN201520470808.6U priority Critical patent/CN204799231U/en
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Publication of CN204799231U publication Critical patent/CN204799231U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses an oxidation reactor is used in formaldehyde production, including the reactor, reactor has catalytic reaction zoon and establishes the quench zone of catalytic reaction zoon lower part, catalytic reaction zoon includes the catalyst layer, the quench zone includes the tubulation cooler, be equipped with circulating cooling water pipe in the catalyst layer, the recirculated cooling water groove is arranged in to the tubulation cooler, gas uniform distributor is established to catalytic reaction zoon's top. The utility model discloses can make the reaction gas evenly distributed who gets into reactor react in getting into the catalyst layer, in addition because being equipped with circulating cooling water pipe in the catalyst layer, can preventing that the catalyst layer is overheated, the recirculated cooling water groove is placed in to the tubulation cooler, can make reaction gas autocatalysis agent layer come out to cool off the 100 -130 degree and control, but can not reach higher temperature, has prevented that formaldehyde from taking place side reactions such as deep oxidation under high temperature.

Description

A kind of oxidation reactor used for formaldehyde production
Technical field
The utility model belongs to silver-colored formaldehyde production technical field, is specifically related to a kind of oxidation reactor used for formaldehyde production.
Background technology
In the production process of silver legal system formaldehyde, air capacity, reaction effect between water vapour amount and methyl alcohol evaporation capacity have impact on efficiency and the quality of formaldehyde processed greatly, it directly affects the reaction temperature of oxidator, product quality, output, the consumption of raw material, the problem such as catalyst life and production safety, so just there is strict requirement to oxidator, the catalysis of silver method is due to variations in temperature, easily poly-reaction, cause occurring crack, affect production and the making of formaldehyde, wherein in oxidation reaction, the position of catalyst and oxidizing temperature change are sport technique segments particularly important in oxidation reaction, reaction temperature rises too fast, reaction speed is accelerated, but the too high meeting of reaction temperature causes side reaction to increase, impurity is too many, be unfavorable for that the life-span of catalyst is unfavorable, reaction temperature is too low, reaction speed is slower, do not reach productive target, so the control of oxidator also seems particularly important.
Utility model content
The purpose of this utility model is solve above-mentioned technical problem and provide one can prevent formaldehyde from the side reactions such as deep oxidation oxidation reactor used for formaldehyde production at high temperature occurring.
For achieving the above object, the utility model adopts following technical scheme:
A kind of oxidation reactor used for formaldehyde production, comprise reactor body, described reactor body has reacting gas inlet, reaction gas outlet, there is in described reactor body catalyst reaction section and be located at the quench zone of described catalytic reaction pars infrasegmentalis, described catalyst reaction section comprises catalyst layer, described quench zone comprises tubulation cooler, circulating cooling water pipe is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank, the top of described catalyst reaction section is provided with even gas distribution device, described even gas distribution device is cone-shaped structure, surface is provided with multiple airflow hole.
Described circulating cooling tank connects cooling water inlet and the coolant outlet of recirculated cooling water.
Described circulating cooling water pipe connects cooling water inlet and the coolant outlet of recirculated cooling water.
Described reacting gas inlet, reaction gas outlet are located on the sidewall of described reactor body respectively.
The utility model by having catalyst reaction section and being located at the quench zone of described catalytic reaction pars infrasegmentalis in reactor, described catalyst reaction section comprises catalyst layer, described quench zone comprises tubulation cooler, circulating cooling water pipe is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank, the top of described catalyst reaction section is provided with even gas distribution device, described even gas distribution device is cone-shaped structure, surface is provided with multiple airflow hole, the reacting gas entered in reactor can be made to be uniformly distributed enter in catalyst layer to react, and owing to being provided with circulating cooling water pipe in described catalyst layer, catalyst layer can be prevented overheated, described tubulation cooler is placed in circulating cooling tank, reacting gas self-catalysis oxidant layer can be made out to be cooled to 100-130 degree about, but higher temperature can not be reached, formaldehyde is prevented at high temperature the side reactions such as deep oxidation to occur, effectively ensure that the quality of production of formaldehyde, there is great production practices and realistic meaning.
Accompanying drawing explanation
Figure 1 shows that the structural representation of the oxidation reactor a kind of used for formaldehyde production that the utility model embodiment provides.
Detailed description of the invention
Below, in conjunction with example, substantive distinguishing features of the present utility model and advantage are further described, but the utility model is not limited to listed embodiment.
Refer to shown in Fig. 1, a kind of oxidation reactor used for formaldehyde production, comprise reactor body 1, described reactor body has reacting gas inlet 2, reaction gas outlet 3, in described reactor body 1, there is catalyst reaction section and be located at the quench zone of described catalytic reaction pars infrasegmentalis, described catalyst reaction section comprises catalyst layer 13, be located in catalyst bed 6, described quench zone comprises tubulation cooler 9, circulating cooling water pipe 5 is provided with in described catalyst layer, described tubulation cooler 9 is placed in circulating cooling tank 10, the top of described catalyst reaction section is provided with even gas distribution device 4, described even gas distribution device 4 is cone-shaped structure, surface is provided with multiple airflow hole.
Described circulating cooling tank connects the cooling water inlet 11 of recirculated cooling water and the coolant outlet 12 of circulating cooling tank of circulating cooling tank.
Described circulating cooling water pipe connects the cooling water inlet 7 of recirculated cooling water and the coolant outlet 8 of circulating cooling water pipe of circulating cooling water pipe.
Described reacting gas inlet 2, reaction gas outlet 3 are located on the sidewall of described reactor body 1 respectively.
The utility model by having catalyst reaction section and being located at the quench zone of described catalytic reaction pars infrasegmentalis in reactor, described catalyst reaction section comprises catalyst layer, described quench zone comprises tubulation cooler, circulating cooling water pipe is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank, the top of described catalyst reaction section is provided with even gas distribution device, described even gas distribution device is cone-shaped structure, surface is provided with multiple airflow hole, the reacting gas entered in reactor can be made to be uniformly distributed enter in catalyst layer to react, and owing to being provided with circulating cooling water pipe in described catalyst layer, catalyst layer can be prevented overheated, described tubulation cooler is placed in circulating cooling tank, reacting gas self-catalysis oxidant layer can be made out to be cooled to 100-130 degree about, but higher temperature can not be reached, formaldehyde is prevented at high temperature the side reactions such as deep oxidation to occur, effectively ensure that the quality of production of formaldehyde, there is great production practices and realistic meaning.
Although be described the utility model with reference to embodiment of the present utility model here, but, should be appreciated that, those skilled in the art can design a lot of other amendment and embodiment, these amendments and embodiment will drop within spirit disclosed in the present application and spirit.
More particularly, in the scope of, accompanying drawing open in the application and claim, multiple modification and improvement can be carried out to the building block of subject combination layout and/or layout.Except the modification of carrying out building block and/or layout is with except improvement, to those skilled in the art, other purposes also will be obvious.

Claims (4)

1. an oxidation reactor used for formaldehyde production, it is characterized in that, comprise reactor body, described reactor body has reacting gas inlet, reaction gas outlet, there is in described reactor body catalyst reaction section and be located at the quench zone of described catalytic reaction pars infrasegmentalis, described catalyst reaction section comprises catalyst layer, described quench zone comprises tubulation cooler, circulating cooling water pipe is provided with in described catalyst layer, described tubulation cooler is placed in circulating cooling tank, the top of described catalyst reaction section is provided with even gas distribution device, described even gas distribution device is cone-shaped structure, surface is provided with multiple airflow hole.
2. oxidation reactor used for formaldehyde production as claimed in claim 1, is characterized in that, described circulating cooling tank connects cooling water inlet and the coolant outlet of recirculated cooling water.
3. oxidation reactor used for formaldehyde production as claimed in claim 2, is characterized in that, described circulating cooling water pipe connects cooling water inlet and the coolant outlet of recirculated cooling water.
4. oxidation reactor used for formaldehyde production as claimed in claim 3, it is characterized in that, described reacting gas inlet, reaction gas outlet are located on the sidewall of described reactor body respectively.
CN201520470808.6U 2015-06-26 2015-06-26 Oxidation reactor is used in formaldehyde production Expired - Fee Related CN204799231U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520470808.6U CN204799231U (en) 2015-06-26 2015-06-26 Oxidation reactor is used in formaldehyde production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520470808.6U CN204799231U (en) 2015-06-26 2015-06-26 Oxidation reactor is used in formaldehyde production

Publications (1)

Publication Number Publication Date
CN204799231U true CN204799231U (en) 2015-11-25

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201520470808.6U Expired - Fee Related CN204799231U (en) 2015-06-26 2015-06-26 Oxidation reactor is used in formaldehyde production

Country Status (1)

Country Link
CN (1) CN204799231U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114797691A (en) * 2022-05-09 2022-07-29 漳州市龙文翰苑化工有限公司 Oxidation reactor and process for formaldehyde production

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114797691A (en) * 2022-05-09 2022-07-29 漳州市龙文翰苑化工有限公司 Oxidation reactor and process for formaldehyde production
CN114797691B (en) * 2022-05-09 2024-02-27 漳州市龙文翰苑化工有限公司 Oxidation reactor and process for formaldehyde production

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20151125

Termination date: 20170626

CF01 Termination of patent right due to non-payment of annual fee