CN204767595U - Extraction device for chemistry experiments - Google Patents

Extraction device for chemistry experiments Download PDF

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Publication number
CN204767595U
CN204767595U CN201520351954.7U CN201520351954U CN204767595U CN 204767595 U CN204767595 U CN 204767595U CN 201520351954 U CN201520351954 U CN 201520351954U CN 204767595 U CN204767595 U CN 204767595U
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CN
China
Prior art keywords
fistulae
clamping device
glass stopper
bucket body
cock
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201520351954.7U
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Chinese (zh)
Inventor
吴姣艳
李庆宁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningbo University
Original Assignee
Ningbo University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ningbo University filed Critical Ningbo University
Priority to CN201520351954.7U priority Critical patent/CN204767595U/en
Application granted granted Critical
Publication of CN204767595U publication Critical patent/CN204767595U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model provides an extraction device for chemistry experiments, includes support frame and separating funnel, the support frame includes the vertical bracing piece that is provided with on base, and bracing piece upper portion clamp is equipped with clamping device, clamping device's inner wall is equipped with the heating jacket, and separating funnel passes through clamping device to be fixed on the support frame, separating funnel includes glass stopper, bucket body and fistulae, and the glass stopper is equipped with the spiral coil, and the import of spiral coil is seted up in the side of glass stopper, and the bottom at the glass stopper is seted up in the export, the bucket body lower part is equipped with the external screw thread, and fistulae upper portion is equipped with the internal thread with the external screw thread adaptation, and the fistulae closes with outer thread sealing through the internal thread with the bucket body soon, and the fistulae middle part is equipped with the cock, and the cock lower part is equipped with the syringe, the utility model discloses can heat the extract, divide liquid effectual, solution leaks in the time of avoiding the volatility extraction, guarantees the experiment precision, avoided the extraction in -process frequently to draw the cork, split type design is convenient for carry out the part change when fistulae damages, saves the cost more.

Description

A kind of chemical experiment extraction equipment
Technical field
The utility model relates to a kind of chemical experimental instrument, specifically a kind of chemical experiment extraction equipment.
Background technology
Separatory funnel is extraction equipment the most frequently used in chemical industry.During extraction, need first will the solvent of separatory to be needed to pour in separatory funnel, then with hand-held firmly separatory funnel, vibration solution, separatory after standing certain hour, easily produce gas for volatile solvent soln when rocking, the deflation course that causes drawing the cork may occur that solution goes out the phenomenon of separatory funnel, not only have impact on the experiment degree of accuracy but also existed operating personnel's personal safety to threaten; The effect of extracting temperature influence of some solution, and existing separatory funnel is not easy to heating; Some liquid is high due to its viscosity, adds the reason of pressure in funnel, and when being separated to liquid level layering critical surface, flow velocity is excessively slow, separatory difficulty; Its cock of the separatory funnel of prior art and fistulae easily in use damage, and often just cause whole separatory funnel and scrap, use cost is high, easily causes waste;
Utility model content
The chemical experiment extraction equipment that the purpose of this utility model is to provide a kind of to be convenient to heat, security is high, simple to operate, can reduce use cost, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the utility model provides following technical scheme:
A kind of chemical experiment extraction equipment, comprise bracing frame and separatory funnel, support frame as described above comprises base, support bar and clamping device, and base is vertically provided with support bar, and support bar top has clamped clamping device; The pinch zones of described clamping device is set to inverted circular cone shape, and the inwall of clamping device is for being provided with heating jacket; Described separatory funnel is fixed on bracing frame by clamping device, and separatory funnel comprises glass stopper, bucket body and fistulae, is provided with spiral coil in glass stopper, and the import of spiral coil is opened in the side of glass stopper, and outlet is opened in the bottom of glass stopper; Described bucket body bottom is provided with external screw thread, fistulae top is provided with the internal thread with external screw thread adaptation, fistulae and bucket body are sealed by internal thread and external screw thread and screw, cock is provided with in the middle part of described fistulae, cock bottom is provided with syringe, described syringe is made up of the foraminate syringe of front end band and the piston core bar matched and piston handle, and described syringe is connected with fistulae.
As further program of the utility model: described heating jacket comprises the first insulating barrier, zone of heating and the second insulating barrier that set gradually from outside to inside.
As the utility model further scheme: be provided with heat-reflecting layer between described zone of heating and the second insulating barrier, described heating jacket is provided with temperature-adjusting device, and temperature-adjusting device is arranged on the side of clamping device.
As the utility model further scheme: described glass stopper, bucket body and fistulae adopt polypropylene material to make; Cock adopts polytetrafluoroethylene (PTFE) material to make.
Compared with prior art, the beneficial effects of the utility model are: the utility model can fully meet extraction experiments requirement, can heat, control heating-up temperature, separatory is effective to extract in separatory funnel; Glass stopper part is provided with spiral coil, avoid and rock the situation that separatory funnel process need extracts glass stopper repeatedly, and the gas in funnel diffuses to outside separatory funnel by spiral coil, avoid solution when extracting glass stopper and go out the situation of separatory funnel because of air pressure, ensure that the accuracy of experiment and the personal safety of operating personnel; Split-type design is convenient to carry out local replacing when fistulae damages, and more saves cost, avoids waste; Syringe the separation that can be conducive to the high liquid of viscosity is set, two-phase laminated flow is more accurate, avoids the error that manual rotation knob causes, accelerates separatory speed.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model;
Fig. 2 is the structural representation of heating jacket in the utility model.
Detailed description of the invention
Be described in more detail below in conjunction with the technical scheme of detailed description of the invention to this patent.
Refer to Fig. 1-2, a kind of chemical experiment extraction equipment, comprise bracing frame 1 and separatory funnel 2, support frame as described above 1 comprises base 3, support bar 4 and clamping device 5, and base 3 is vertically provided with support bar 4, and support bar 4 top has clamped clamping device 5; The pinch zones of described clamping device 5 is set to inverted circular cone shape, the inwall of clamping device 5 is for being provided with heating jacket 6, described heating jacket 6 comprises the first insulating barrier 18, zone of heating 19 and the second insulating barrier 20 that set gradually from outside to inside, heat-reflecting layer 21 is provided with between zone of heating 19 and the second insulating barrier 20, described heating jacket 6 is provided with temperature-adjusting device 22, and temperature-adjusting device 22 is arranged on the side of clamping device 5; Described separatory funnel 2 is fixed on bracing frame 1 by clamping device 5, separatory funnel comprises glass stopper 7, bucket body 8 and fistulae 9, be provided with spiral coil 10 in glass stopper 7, the import 11 of spiral coil 10 is opened in the side of glass stopper 7, and outlet 12 is opened in the bottom of glass stopper 7; Described bucket body 8 bottom is provided with external screw thread, fistulae 9 top is provided with the internal thread with external screw thread adaptation, fistulae 9 and bucket body 8 are sealed by internal thread and external screw thread and screw, cock 13 is provided with in the middle part of described fistulae 9, cock 13 bottom is provided with syringe 14, described syringe 14 is made up of the foraminate syringe 15 of front end band and the piston core bar 16 matched and piston handle 17, and described syringe is connected with fistulae 9; Described glass stopper 7, bucket body 8 and fistulae 9 adopt polypropylene material to make; Cock 13 adopts polytetrafluoroethylene (PTFE) material to make.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art possesses, various change can also be made under the prerequisite not departing from this patent aim.

Claims (4)

1. a chemical experiment extraction equipment, comprise bracing frame (1) and separatory funnel (2), support frame as described above (1) comprises base (3), support bar (4) and clamping device (5), base (3) is vertically provided with support bar (4), support bar (4) top has clamped clamping device (5); It is characterized in that: the pinch zones of described clamping device (5) is set to inverted circular cone shape, the inwall of clamping device (5) is for being provided with heating jacket (6); Described separatory funnel (2) is fixed on bracing frame (1) by clamping device (5), separatory funnel comprises glass stopper (7), bucket body (8) and fistulae (9), spiral coil (10) is provided with in glass stopper (7), the import (11) of spiral coil (10) is opened in the side of glass stopper (7), and outlet (12) is opened in the bottom of glass stopper (7); Described bucket body (8) bottom is provided with external screw thread, fistulae (9) top is provided with the internal thread with external screw thread adaptation, fistulae (9) and bucket body (8) are sealed by internal thread and external screw thread and screw, described fistulae (9) middle part is provided with cock (13), cock (13) bottom is provided with syringe (14), described syringe (14) is made up of the foraminate syringe of front end band (15) and the piston core bar (16) matched and piston handle (17), and described syringe is connected with fistulae (9).
2. chemical experiment extraction equipment according to claim 1, it is characterized in that, described heating jacket (6) comprises the first insulating barrier (18), zone of heating (19) and the second insulating barrier (20) that set gradually from outside to inside.
3. chemical experiment extraction equipment according to claim 2, it is characterized in that, heat-reflecting layer (21) is provided with between described zone of heating (19) and the second insulating barrier (20), described heating jacket (6) is provided with temperature-adjusting device (22), and temperature-adjusting device (22) is arranged on the side of clamping device (5).
4. chemical experiment extraction equipment according to claim 1, is characterized in that, described glass stopper (7), bucket body (8) and fistulae (9) adopt polypropylene material to make; Cock (13) adopts polytetrafluoroethylene (PTFE) material to make.
CN201520351954.7U 2015-05-27 2015-05-27 Extraction device for chemistry experiments Expired - Fee Related CN204767595U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520351954.7U CN204767595U (en) 2015-05-27 2015-05-27 Extraction device for chemistry experiments

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520351954.7U CN204767595U (en) 2015-05-27 2015-05-27 Extraction device for chemistry experiments

Publications (1)

Publication Number Publication Date
CN204767595U true CN204767595U (en) 2015-11-18

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201520351954.7U Expired - Fee Related CN204767595U (en) 2015-05-27 2015-05-27 Extraction device for chemistry experiments

Country Status (1)

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CN (1) CN204767595U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108525345A (en) * 2018-04-27 2018-09-14 陕西师范大学 One kind can automatic extraction apparatus and its control method
CN108705714A (en) * 2018-07-17 2018-10-26 安徽理工大学 A kind of asphalt test piece fast pouring funnel device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108525345A (en) * 2018-04-27 2018-09-14 陕西师范大学 One kind can automatic extraction apparatus and its control method
CN108525345B (en) * 2018-04-27 2021-05-04 陕西师范大学 Automatic extraction device and control method thereof
CN108705714A (en) * 2018-07-17 2018-10-26 安徽理工大学 A kind of asphalt test piece fast pouring funnel device

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20151118

Termination date: 20180527

CF01 Termination of patent right due to non-payment of annual fee