CN204727968U - A kind of electric deposition device - Google Patents
A kind of electric deposition device Download PDFInfo
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- CN204727968U CN204727968U CN201520357693.XU CN201520357693U CN204727968U CN 204727968 U CN204727968 U CN 204727968U CN 201520357693 U CN201520357693 U CN 201520357693U CN 204727968 U CN204727968 U CN 204727968U
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Abstract
The utility model belongs to hydrometallurgy electro-deposition techniques field, particularly relates to a kind of electric deposition device.Comprise electrolytic trial groove, described electrolytic trial groove comprises circulation of elecrolyte groove, and electrolysis cycle groove is provided with solution fluid inlet, solution liquid outlet, venting port, settling chamber's evacuation port, circulation of elecrolyte groove is by arranging dividing plate, circulation groove is isolated into three rooms, be respectively precipitation insulated chamber, floating matter insulated chamber and clear liquid insulated chamber, dividing plate comprises two and is respectively the first dividing plate and second partition, first dividing plate comprises opening upward, second partition comprises opening down, first dividing plate can be isolated the precipitation inside electrolytic solution, second partition can be isolated floating impurity, solution fluid inlet is placed in the top of precipitation insulated chamber, solution liquid outlet is placed in the lower right-hand side of clear liquid insulated chamber, venting port 1c is placed in the top of floating matter insulated chamber, settling chamber's evacuation port is placed in the below of precipitation insulated chamber.
Description
Technical field
The utility model belongs to hydrometallurgy electro-deposition techniques field, particularly relates to a kind of electric deposition device.
Background technology
In hydrometallurgy, electrodeposition process carries out in aqueous solution electrolytic cell, and electrolyzer is square plate frame electrolyzer, the circulation of elecrolyte mode adopting upper entering and lower leaving in electrolytic deposition process more, flute length wall is provided with bus, and hanging parallel alternately on it and is suspended on negative electrode on cross bar and anode.It is large that this kind of electrolyzer has liquid storage amount, and current efficiency is low, and electrolyte flow rate is low, and bath voltage is high, and electrolytic process acid mist cannot the shortcoming such as efficient recovery.
Utility model content
The object of utility model: in order to provide a kind of electric deposition device of better effects if, specific purposes are shown in multiple substantial technological effects of concrete implementation section.
In order to reach as above object, the utility model takes following technical scheme:
A kind of electric deposition device, it is characterized in that, comprise electrolytic trial groove, described electrolytic trial groove comprises circulation of elecrolyte groove, and electrolysis cycle groove is provided with solution fluid inlet, solution liquid outlet, venting port, settling chamber's evacuation port, circulation of elecrolyte groove is by arranging dividing plate, circulation groove is isolated into three rooms, be respectively precipitation insulated chamber, floating matter insulated chamber and clear liquid insulated chamber, dividing plate comprises two and is respectively the first dividing plate and second partition, first dividing plate comprises opening upward, second partition comprises opening down, first dividing plate can be isolated the precipitation inside electrolytic solution, second partition can be isolated floating impurity, solution fluid inlet is placed in the top of precipitation insulated chamber, solution liquid outlet is placed in the lower right-hand side of clear liquid insulated chamber, venting port 1c is placed in the top of floating matter insulated chamber, settling chamber's evacuation port is placed in the below of precipitation insulated chamber.
The further technical scheme of the utility model is, comprise first channel solution and filter inner circulation structure, described first channel solution filters inner circulation structure structure and comprises solution liquid outlet, described solution liquid outlet connects solution circulation pump by pipeline, solution circulation pump connects PP cotton filter subsequently, accesses solution fluid inlet after connecting liquid returning tube rapid-acting coupling subsequently by pipeline.
The further technical scheme of the utility model is, pipeline out connects second passage solution galvanic deposit internal recycle vacuum breaker, spinner-type flowmeter and solution return valve afterwards from solution circulation pump; Pipeline after solution return valve stretches under drum electrolyzer and enters drum electrolyzer after seat, electrolyzer is connected to after stretching out pipeline from the drum electrolyzer seat of honour, pipeline gets back to circulation groove solid phase precipitation room by liquid returning tube rapid-acting coupling from solution fluid inlet subsequently, electrolyzer negative and positive crimp respectively by seat under drum electrolyzer and anode electrolytic cell point bolt, and the vacuum pump stretching out pipeline connection from venting port is connected to acid mist cuvette further.
The further technical scheme of the utility model is, also comprise solution discharge part, described solution discharge part comprises settling chamber's evacuation port, connect connected drainage body mouth after the tap valve of solid phase precipitation room after described settling chamber evacuation port connecting tube, described solution liquid outlet connects connected drainage body mouth after floating matter insulated chamber and clear liquid insulated chamber tapping valve by pipeline.
Adopt the utility model of as above technical scheme, have following beneficial effect relative to prior art: the utility model has the beneficial effect that electrolyte flow rate is high, electrolytic process liquid storage amount is little, Faradaic current efficiency is high, the acid mist of electrolytic process generation can effectively process.To solve in prior art Problems existing in electrolytic trial device.
Accompanying drawing explanation
In order to further illustrate the utility model, be described further below in conjunction with accompanying drawing:
Fig. 1 is electrolyzer example conduit line map of the present utility model;
Fig. 2 is electrolyzer anode and cathode wiring scheme;
Fig. 3 is that first channel solution filters internal recycle line construction view;
Fig. 4 is second passage solution galvanic deposit internal recycle line assumption diagram;
Fig. 5 is third channel solution discharge line assumption diagram;
Wherein: 1 circulation of elecrolyte groove; 1a solution fluid inlet; 1b solution liquid outlet; 1c venting port; 1d settling chamber evacuation port; 2 circulation of elecrolyte bottom land valves; 3 solution circulation pumps; 4 first channel solution filtration channels filter foreline valve; 5 second passage solution galvanic deposit internal recycle vacuum breaker; 6 PP cotton filters; 7 first channel solution filtration channels filter rearmounted valve; 8 spinner-type flowmeters; 9 solution return valves; 10 drum electrolyzers; 10a anode electrolytic cell; 10b anode terminal; 10c cathode terminal; Seat under 10d drum electrolyzer; The 10e drum electrolyzer seat of honour; 11 solid phase precipitation room tap valves; 12 floating matter insulated chambers and clear liquid insulated chamber tapping valve; 13 drum electrolyzer tapping valves; 14 liquid returning tube rapid-acting couplings; 15 vacuum pumps; 16 acid mist cuvettes.
Embodiment
Be described embodiment of the present utility model below in conjunction with accompanying drawing, embodiment does not form restriction of the present utility model:
A kind of electric deposition device, it is characterized in that, comprise electrolytic trial groove, described electrolytic trial groove comprises circulation of elecrolyte groove, and electrolysis cycle groove is provided with solution fluid inlet 1a, solution liquid outlet 1b, venting port 1c, settling chamber evacuation port 1d, circulation of elecrolyte groove is by arranging dividing plate, circulation groove is isolated into three rooms, be respectively precipitation insulated chamber, floating matter insulated chamber and clear liquid insulated chamber, dividing plate comprises two and is respectively the first dividing plate and second partition, first dividing plate comprises opening upward, second partition comprises opening down, first dividing plate can be isolated the precipitation inside electrolytic solution, second partition can be isolated floating impurity, solution fluid inlet 1a is placed in the top of precipitation insulated chamber, solution liquid outlet 1b is placed in the lower right-hand side of clear liquid insulated chamber, venting port 1c is placed in the top of floating matter insulated chamber, settling chamber's evacuation port is placed in the below of precipitation insulated chamber.The technique effect of the essence that the technical scheme at this place plays and implementation procedure thereof are as follows: provide at least a kind of novel Thoughs, it is the individuality that can sell separately, and inside comprises multiple division plate.Electrolysis cycle liquid is isolated the precipitation of the inside and floating impurity by insulated chamber, and effectively ensure to enter the pure of the solution of electrolytic system, in operation process, electrolytic solution is by valve, enters electrolyte circulating pump; Enter electrolyte filter from electrolyte circulating pump liquid out by first channel valve to filter, after filtering, solution enters spinner-type flowmeter by valve, enters electrolysis cycle groove by valve.Comprise first channel solution and filter inner circulation structure, described first channel solution filters inner circulation structure structure and comprises solution liquid outlet 1b, described solution liquid outlet 1b connects solution circulation pump 3 by pipeline, solution circulation pump 3 connects PP cotton filter 6 subsequently, accesses solution fluid inlet 1a after connecting liquid returning tube rapid-acting coupling subsequently by pipeline.
Pipeline out connects second passage solution galvanic deposit internal recycle vacuum breaker 5, spinner-type flowmeter 8 and solution return valve 9 afterwards from solution circulation pump 3; Pipeline after solution return valve 9 stretches under drum electrolyzer and enters drum electrolyzer 10 after seat 10d, electrolyzer is connected to after drum electrolyzer seat of honour 10e stretches out pipeline, pipeline gets back to circulation groove solid phase precipitation room by liquid returning tube rapid-acting coupling 14 from solution fluid inlet 1a subsequently, electrolyzer negative and positive crimp respectively by seat 10d under drum electrolyzer and anode electrolytic cell 10a point bolt, and the vacuum pump 15 stretching out pipeline connection from venting port 1c is connected to acid mist cuvette 16 further.Solution after having filtered, by valve, enters electrolyte circulating pump; Spinner-type flowmeter is entered by second passage valve from electrolyte circulating pump liquid out, the fluid inlet entering seat under electrolyzer is adjusted by valve, the solution entering electrolyzer is discharged at the liquid outlet by the electrolyzer seat of honour, and enters circulation of elecrolyte groove by circulation of elecrolyte notch.
Also comprise solution discharge part, described solution discharge part comprises settling chamber evacuation port 1d, connect the rear connected drainage body mouth of solid phase precipitation room tap valve 11 after described settling chamber evacuation port 1d connecting tube, described solution liquid outlet 1b connects floating matter insulated chamber and the rear connected drainage body mouth of clear liquid insulated chamber tapping valve 12 by pipeline.Electrolyzer comprises electric tank cathode, anode electrolytic cell; Anode electrolytic cell terminals; Anode electrolytic cell terminals; Seat under electrolyzer; The electrolyzer seat of honour, electrolytic solution rectification exports the anode and cathode relying on wire to be connected to electrolyzer.Cell body is welding flange on stainless steel tube/titanium pipe, and the upper and lower seat of electrolyzer relies on bolt to be fixed on the flange face up and down of electrolytic cell body, forms a kind of electrolytic arrangement of structure closed.The acid mist that circulation of elecrolyte groove upper air vent is discharged, pass through vacuum pump, be evacuated to acid mist cuvette, finally emit, solid precipitation room liquid in electrolysis cycle groove passes through electrolyzer circulation groove leakage fluid dram, valve, and electrolysis cycle groove floating matter insulated chamber and clear liquid insulated chamber solution are by electrolysis cycle groove liquid outlet, valve, in electrolyzer, solution all discharges electrolytic trial device by valve.
More detailed explanation is:
1. circulation of elecrolyte groove separates precipitation insulated chamber, floating matter insulated chamber and clear liquid insulated chamber.
2. first electrolytic solution enter filtering system by valve, pump, returns electrolysis cycle groove after having filtered, and forms first channel and filter internal recycle.
3. after filtering, electrolytic solution enters electrolyzer by second passage, forms second passage electrolytic solution internal recycle.
4. circulation of elecrolyte flow is controlled by liquid returning tube and under meter.
5. cell body is stainless steel/titanium pipe, welding flange.
6. the upper and lower seat of electrolyzer is PP/ synthetic glass, by bolt and electrolytic cell body compact siro spinning technology.
7. anode electrolytic cell is titanium coating cylindrical anode, and anode conducting is directly fixed in anode posts.
8. electrolytic cell body is directly as electric tank cathode, and negative electrode conduction is bolted on cathode flange face.
9. cell body is closed structure.
10. the acid mist of electrolytic process output all enters in circulation of elecrolyte groove.
11. electrolysis acid fogs are evacuated to acid mist cuvette by vacuum pump.
Liquid in 12. electrolysis cycle grooves, electrolyzer discharges electrolytic trial device by passage three.
It is clear that the technique effect that above structure realizes realizes, if do not consider the technical scheme of adding, this patent title can also be a kind of electrolyzer, and namely wherein the part of electrolyzer also can be applied for a patent separately.
Not shown part details.
It should be noted that, multiple schemes that this patent provides comprise general planning own, separate, mutually do not restrict, but it also can combine when not conflicting mutually, reaching multiple effect and jointly realizing.
more than show and describe ultimate principle of the present utility model, principal character and advantage of the present utility model.Those skilled in the art should understand the utility model and not be restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present utility model; under the prerequisite not departing from the utility model spirit and scope; the utility model also has various changes and modifications, and these changes and improvements all fall in claimed scope.
Claims (4)
1. an electric deposition device, is characterized in that, comprises electrolytic trial groove, and described electrolytic trial groove comprises circulation of elecrolyte groove, and electrolysis cycle groove is provided with solution fluid inlet (1a), solution liquid outlet (1b), venting port (1c), settling chamber's evacuation port (1d), circulation of elecrolyte groove is by arranging dividing plate, circulation groove is isolated into three rooms, be respectively precipitation insulated chamber, floating matter insulated chamber and clear liquid insulated chamber, dividing plate comprises two and is respectively the first dividing plate and second partition, first dividing plate comprises opening upward, second partition comprises opening down, first dividing plate can be isolated the precipitation inside electrolytic solution, second partition can be isolated floating impurity, solution fluid inlet (1a) is placed in the top of precipitation insulated chamber, solution liquid outlet (1b) is placed in the lower right-hand side of clear liquid insulated chamber, venting port (1c) is placed in the top of floating matter insulated chamber, settling chamber's evacuation port is placed in the below of precipitation insulated chamber.
2. a kind of electric deposition device as claimed in claim 1, it is characterized in that, comprise first channel solution and filter inner circulation structure, described first channel solution filters inner circulation structure structure and comprises solution liquid outlet (1b), described solution liquid outlet (1b) connects solution circulation pump (3) by pipeline, solution circulation pump (3) connects PP cotton filter (6) subsequently, accesses solution fluid inlet (1a) after connecting liquid returning tube rapid-acting coupling subsequently by pipeline.
3. a kind of electric deposition device as claimed in claim 1, is characterized in that, pipeline out connects second passage solution galvanic deposit internal recycle vacuum breaker (5), spinner-type flowmeter (8) and solution return valve (9) afterwards from solution circulation pump (3); Pipeline after solution return valve (9) stretches under drum electrolyzer and enters drum electrolyzer (10) after seat (10d), electrolyzer is connected to after stretching out pipeline from the drum electrolyzer seat of honour (10e), pipeline gets back to circulation groove solid phase precipitation room by liquid returning tube rapid-acting coupling (14) from solution fluid inlet (1a) subsequently, electrolyzer negative and positive crimp respectively by seat (10d) under drum electrolyzer and anode electrolytic cell (10a) some bolt, and the vacuum pump (15) stretching out pipeline connection from venting port (1c) is connected to acid mist cuvette (16) further.
4. a kind of electric deposition device as claimed in claim 1, it is characterized in that, also comprise solution discharge part, described solution discharge part comprises settling chamber's evacuation port (1d), connect solid phase precipitation room tap valve (11) connected drainage body mouth afterwards after described settling chamber evacuation port (1d) connecting tube, described solution liquid outlet (1b) connects floating matter insulated chamber and clear liquid insulated chamber tapping valve (12) connected drainage body mouth afterwards by pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520357693.XU CN204727968U (en) | 2015-05-29 | 2015-05-29 | A kind of electric deposition device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520357693.XU CN204727968U (en) | 2015-05-29 | 2015-05-29 | A kind of electric deposition device |
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| CN204727968U true CN204727968U (en) | 2015-10-28 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106654464A (en) * | 2017-03-14 | 2017-05-10 | 哈尔滨工业大学 | Aluminum air battery electrolyte circulating system based on hydrocyclone effect |
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2015
- 2015-05-29 CN CN201520357693.XU patent/CN204727968U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106654464A (en) * | 2017-03-14 | 2017-05-10 | 哈尔滨工业大学 | Aluminum air battery electrolyte circulating system based on hydrocyclone effect |
| CN106654464B (en) * | 2017-03-14 | 2018-10-19 | 哈尔滨工业大学 | A kind of aluminium-air cell electrolyte circulation system based on hydraulic cyclone effect |
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