CN205974696U - Torrent electrodeposition small test device - Google Patents
Torrent electrodeposition small test device Download PDFInfo
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- CN205974696U CN205974696U CN201620720856.0U CN201620720856U CN205974696U CN 205974696 U CN205974696 U CN 205974696U CN 201620720856 U CN201620720856 U CN 201620720856U CN 205974696 U CN205974696 U CN 205974696U
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Abstract
The utility model belongs to an electrochemical technique field especially relates to a torrent electrodeposition small test device. By soluble anode bar, inert cathode barrel, starting sheet, magnetic drive pump, circulating slot, valve, flowmeter etc. Are not formed. The electrolysis trough electrode is concentric tubulose, and titanium or stainless steel starting sheet have been inserted to the inslot wall, and the positive pole is fixed in the middle of the cell body. At the electrodeposition in -process, electrolyte in tank bottom entering electrolysis trough, rotatory high -speed flow of inslot, pushes up from the groove and discharges under the effect of transfer pump. Concentration polarization's influence is eliminated through high -speed liquid stream to the difference of the theoretical deposition potential of the various metal ion of BEW torrent electrodeposition test device make full use of, and the purpose that reaches selectivity electrowinning metal can be carried out direct electrical integration to low concentration metal ion solution and multiple metal coexistence solution and left.
Description
Technical field
The utility model belongs to technical field of electrochemistry, more particularly, to a kind of turbulent flow electrodeposition small test device.
Background technology
Traditional electrodeposition technology is that anode and cathode is placed in the slow cell body flowing or stagnating, in the presence of electric field,
Anion to anode displacement, cation to negative electrode displacement, by controlling certain technical conditions, the metal to be obtained
Cation obtains electronic deposition in negative electrode and separates out, thus obtaining electrodeposition product.
There is high cost in traditional electrodeposition technology, efficiency is low, operating environment is poor, the low shortcoming of automaticity.
Utility model content
The purpose of utility model:In order to provide a kind of effect more preferable turbulent flow electrodeposition small test device, specific purposes are shown in
It is embodied as multiple substantial technological effects of part.
In order to reach as above purpose, the utility model adopts the following technical scheme that:
A kind of turbulent flow electrodeposition small test device it is characterised in that:Comprise turbulent flow Winning cell body, turbulent flow Winning cell body
Including anode, negative electrode cylinder, starting sheet, anode terminal, cathode terminal, solution inlet port, solution refluxing opening, in cathode tube body
Starting sheet is posted in portion, and anode is located at the middle part of negative electrode cylinder, and anode terminal and cathode terminal connection are stretched out line and connected outside,
Comprise solution inlet port below negative electrode cylinder, above negative electrode cylinder, comprise solution refluxing opening;Electrodeposition circulating slot is by precipitating isolation ward, drift
Floating isolation ward, clear liquid room composition, but each room is separated by dividing plate comprises opening on dividing plate;The outlet of magnetic drive pump and turbulent flow Winning cell
The solution inlet port of body is connected by pipeline;The entrance of magnetic drive pump is connected by pipeline with the clear liquid room of electrodeposition circulating slot;Turbulent flow
The solution refluxing opening of Winning cell body is connected by pipeline with the precipitation isolation ward of electrodeposition circulating slot.
The further technical scheme of the utility model is, the lower partition between described precipitation isolation ward and floating isolation ward
Opening;Dividing plate upper opening between floating isolation ward and clear liquid room.
The further technical scheme of the utility model is, described electrodeposition circulating slot is provided with cover plate, enables to system
Seal and prevent acid fog outflow.
The further technical scheme of the utility model is, the output of described anode terminal, cathode terminal and rectifier
Terminal connects.
The further technical scheme of the utility model is, the pipeline that Winning cell solution inlet port connects is also equipped with bypass
Valve, tapping valve and leakage fluid dram, for the emptying of solution in device.
The further technical scheme of the utility model is, the pipeline that Winning cell solution inlet port connects also is sequentially installed with stream
Gauge, flow control valve.
Using the utility model of as above technical scheme, have the advantages that with respect to prior art:Change tradition
The thinking of upper box electrodeposition, electrolyzer electric extremely concentric tube-shaped, groove inwall is inserted with titanium negative plate, and anode is fixed in the middle of cell body.
In electrolytic deposition process, electrolyte, in the presence of infusion pump, enters in electrolytic cell from bottom land, rotates flow at high speed in groove, from
Groove top row goes out.Electrodeposition apparatus make full use of the difference of each metal ion species theory deposition potential, are eliminated dense by high speed liquid flow
The impact of difference polarization, the purpose reaching selective electrolysis extraction metal can be common to low-concentration metallic solion and various metals
Deposit solution and carry out direct electrowinning separation, output metallic plate or powder.Its process is simple, reliable stable, compare traditional electrodeposition
Technique has prominent advantage.
Brief description
In order to further illustrate the utility model, it is further illustrated below in conjunction with the accompanying drawings:
Fig. 1 is device structure schematic diagram of the present utility model;
Wherein:1st, negative electrode cylinder;2nd, starting sheet;3rd, anode;4th, solution inlet port;5th, solution refluxing opening;6 、
Anode terminal;7th, cathode terminal;8th, rectifier;9th, circulating slot;9-1, precipitation isolation ward;9-2, floating every
From room;9-3, clear liquid room;10th, magnetic drive pump;11st, flowmeter;12nd, flow control valve;13rd, filter;14th, manage
Road;15th, bypass valve;16th, tapping valve;17th, leakage fluid dram.
Specific embodiment
Below in conjunction with the accompanying drawings embodiment of the present utility model is illustrated, embodiment is not constituted to limit of the present utility model
System:
A kind of turbulent flow electrodeposition small test device it is characterised in that:Comprise turbulent flow Winning cell body, turbulent flow Winning cell body
Including anode, negative electrode cylinder, starting sheet, anode terminal, cathode terminal, solution inlet port, solution refluxing opening, in cathode tube body
Starting sheet is posted in portion, and anode is located at the middle part of negative electrode cylinder, and anode terminal and cathode terminal connection are stretched out line and connected outside,
Comprise solution inlet port below negative electrode cylinder, above negative electrode cylinder, comprise solution refluxing opening;Electrodeposition circulating slot is by precipitating isolation ward, drift
Floating isolation ward, clear liquid room composition, but each room is separated by dividing plate comprises opening on dividing plate;The outlet of magnetic drive pump and turbulent flow Winning cell
The solution inlet port of body is connected by pipeline;The entrance of magnetic drive pump is connected by pipeline with the clear liquid room of electrodeposition circulating slot;Turbulent flow
The solution refluxing opening of Winning cell body is connected by pipeline with the precipitation isolation ward of electrodeposition circulating slot.The technical scheme at this place is risen
To the technique effect of essence and its process of realizing be as follows:Change the thinking of traditionally box electrodeposition, electrolyzer electric is extremely
Concentric tube-shaped, groove inwall is inserted with titanium negative plate, and anode is fixed in the middle of cell body.In electrolytic deposition process, electrolyte is in infusion pump
Under effect, enter in electrolytic cell from bottom land, rotate flow at high speed in groove, go out from groove top row.Electrodeposition apparatus make full use of respectively
The difference of metal ion species theory deposition potential, is eliminated the impact of concentration polarization, reaches selective electrolysis and carry by high speed liquid flow
The purpose taking metal can coexist solution and carries out direct electrowinning and separates to low-concentration metallic solion and various metals, output gold
Belong to plate or powder.Its process is simple, reliable stable, compare traditional electrodeposition process and there is prominent advantage.
The lower partition opening between described precipitation isolation ward and floating isolation ward;Between floating isolation ward and clear liquid room
Dividing plate upper opening.The technique effect of the essence that the technical scheme at this place is played and its process of realizing are as follows:Lower openings
Liquid is facilitated to flow, upper opening facilitates gas to flow out.
It is provided with cover plate on described electrodeposition circulating slot, enable to system sealing and prevent acid fog outflow.
Described anode terminal, cathode terminal are connected with the lead-out terminal of rectifier.Winning cell solution inlet port connects
Bypass valve, tapping valve and leakage fluid dram are also equipped with pipeline, for the emptying of solution in device.
Also it is sequentially installed with flowmeter, flow control valve on the pipeline that Winning cell solution inlet port connects.
In a creative way, each effect above is individually present moreover it is possible to complete the combination of the above results with a nested structure.
It is clear that the technique effect that above structure is realized is realized, and discounting for additional technical scheme, this patent title is also
Can be a kind of electrodeposition apparatus.In figure not shown part details.
It should be noted that multiple schemes that this patent provides comprise the basic scheme of itself, separate, not mutually
Restriction, but it can also be mutually combined in the case of not conflicting, and reach multiple effects and jointly realize.
Of the present utility model general principle, principal character and of the present utility model advantage have been shown and described above.Ability
The technical staff in domain it should be recognized that the utility model is not restricted to the described embodiments, described in above-described embodiment and specification
Principle of the present utility model is simply described, on the premise of without departing from the utility model spirit and scope, the utility model also can
There are various changes and modifications, these changes and improvements both fall within claimed scope.
Claims (6)
1. a kind of turbulent flow electrodeposition small test device it is characterised in that:Comprise turbulent flow Winning cell body, turbulent flow Winning cell body bag
Include anode, negative electrode cylinder, starting sheet, anode terminal, cathode terminal, solution inlet port, solution refluxing opening, negative electrode inner barrel
Post starting sheet, anode is located at the middle part of negative electrode cylinder, anode terminal and cathode terminal connection are stretched out line and connected outside, the moon
Comprise solution inlet port below the cylinder of pole, above negative electrode cylinder, comprise solution refluxing opening;Electrodeposition circulating slot is by precipitating isolation ward, floating
Isolation ward, clear liquid room composition, but each room is separated by dividing plate comprises opening on dividing plate;The outlet of magnetic drive pump is with turbulent flow Winning cell originally
The solution inlet port of body is connected by pipeline;The entrance of magnetic drive pump is connected by pipeline with the clear liquid room of electrodeposition circulating slot;Turbulent flow electricity
The solution refluxing opening of long-pending groove body is connected by pipeline with the precipitation isolation ward of electrodeposition circulating slot.
2. as claimed in claim 1 a kind of turbulent flow electrodeposition small test device it is characterised in that:Described precipitation isolation ward and drift
The lower partition opening between floating isolation ward;Dividing plate upper opening between floating isolation ward and clear liquid room.
3. as claimed in claim 1 a kind of turbulent flow electrodeposition small test device it is characterised in that:Set on described electrodeposition circulating slot
It is equipped with cover plate, enable to system sealing and prevent acid fog outflow.
4. as claimed in claim 1 a kind of turbulent flow electrodeposition small test device it is characterised in that:Described anode terminal, the moon
Pole binding post is connected with the lead-out terminal of rectifier.
5. as claimed in claim 1 a kind of turbulent flow electrodeposition small test device it is characterised in that:Winning cell solution inlet port connects
Pipeline on be also equipped with bypass valve, tapping valve and leakage fluid dram, for the emptying of solution in device.
6. as claimed in claim 1 a kind of turbulent flow electrodeposition small test device it is characterised in that:Winning cell solution inlet port connects
Pipeline on be also sequentially installed with flowmeter, flow control valve.
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CN201620720856.0U CN205974696U (en) | 2016-07-11 | 2016-07-11 | Torrent electrodeposition small test device |
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CN201620720856.0U CN205974696U (en) | 2016-07-11 | 2016-07-11 | Torrent electrodeposition small test device |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106835255A (en) * | 2017-02-21 | 2017-06-13 | 西安互达环保科技有限公司 | A kind of turbulent flow electrodeposition method and corollary apparatus and modularization expand scheme |
CN108842171A (en) * | 2018-09-13 | 2018-11-20 | 陕西瑞凯环保科技有限公司 | A kind of method and apparatus that turbulent flow electrodeposition prepares metal-powder |
CN110042426A (en) * | 2019-06-06 | 2019-07-23 | 深圳市中金岭南有色金属股份有限公司丹霞冶炼厂 | A kind of closed electrodeposition pipe and gallium electrodeposition system |
CN117779121A (en) * | 2024-02-26 | 2024-03-29 | 成都中核高通同位素股份有限公司 | Dynamic electrolytic separation and purification device and system |
-
2016
- 2016-07-11 CN CN201620720856.0U patent/CN205974696U/en active Active
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106835255A (en) * | 2017-02-21 | 2017-06-13 | 西安互达环保科技有限公司 | A kind of turbulent flow electrodeposition method and corollary apparatus and modularization expand scheme |
CN108842171A (en) * | 2018-09-13 | 2018-11-20 | 陕西瑞凯环保科技有限公司 | A kind of method and apparatus that turbulent flow electrodeposition prepares metal-powder |
CN110042426A (en) * | 2019-06-06 | 2019-07-23 | 深圳市中金岭南有色金属股份有限公司丹霞冶炼厂 | A kind of closed electrodeposition pipe and gallium electrodeposition system |
CN117779121A (en) * | 2024-02-26 | 2024-03-29 | 成都中核高通同位素股份有限公司 | Dynamic electrolytic separation and purification device and system |
CN117779121B (en) * | 2024-02-26 | 2024-05-17 | 成都中核高通同位素股份有限公司 | Dynamic electrolytic separation and purification device and system |
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