CN204509351U - A kind of enzyme reaction automatic device system - Google Patents
A kind of enzyme reaction automatic device system Download PDFInfo
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- CN204509351U CN204509351U CN201520173783.3U CN201520173783U CN204509351U CN 204509351 U CN204509351 U CN 204509351U CN 201520173783 U CN201520173783 U CN 201520173783U CN 204509351 U CN204509351 U CN 204509351U
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- enzyme
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Abstract
The utility model provides a kind of enzyme reaction automatic device system, comprises reaction unit, whipping appts, resin column, pump; Described whipping appts is positioned at described synthetic reaction device; Potting resin in described resin column; Outlet is arranged at the bottom of described reaction unit, and described pump is positioned at the described downstream of reaction unit outlet and the upstream of described resin column.The utility model is applicable to pharmacy, makeup and field of fine chemical.
Description
Technical field
The utility model relates to a kind of chemical reaction equipment, is specifically related to a kind of enzyme reaction automatic device system and its preparation method and application.
Background technology
In pharmacy, makeup and other field of fine chemical, conventional processing routes is complicated, and process control link is many, produces the three wastes large to environmental influence.In recent years, the research of international developed country adopts enzyme to catalyze and synthesize, and can shorten original pure chemistry technique, mild condition, is more conducive to Artificial Control operation.But in existing enzymic catalytic reaction, the consumption of enzyme hold and control techniques more difficult, operator will grasp the amount that enzyme consumes during the course, need to supplement appropriate enzyme in time, the workload of increase operator.Once the consumption of enzyme is improper, too much very few, all can affect the carrying out of reaction and the quality of target product.
Summary of the invention
In order to solve the problem, first object of the present utility model is to provide a kind of enzyme reaction automatic device system.
The enzyme reaction automatic device system technical scheme that the utility model provides:
Comprise reaction unit, whipping appts, resin column, pump; Described whipping appts is positioned at described reaction unit; Potting resin in described resin column; Outlet is arranged at the bottom of described reaction unit, and described pump is positioned at the described downstream of reaction unit outlet and the upstream of described resin column.
As preferably, the outlet of described reaction unit is connected to threeway, and other two ports of this threeway connect one end of outlet end and described pump respectively, and the upstream of described outlet end is provided with control valve.
As preferably, the resin of filling in described resin column is immobilized enzyme resin, is full of enzyme liquid in this resin column.
The preparation method of the employing enzyme reaction automatic device system that the utility model provides
Reaction solution in described reaction unit (1) is extracted into described resin column (3) by described pump (4), upwards fully contact with described mixed with resin from the bottom of this resin column (3), enzyme liquid is added in reaction solution, and get back to described reaction unit (1) from the top of described resin column (3), complete a circulation; Described whipping appts (2) Keep agitation reaction solution, reaction solution circulates through described resin column, evenly supplements enzyme liquid.
The application of the enzyme reaction automatic device system that the utility model provides: described enzyme reaction automatic device system is applied to the synthesis technique adopting the pharmacy of enzyme reaction, makeup and fine chemistry industry.
Advantageous Effects of the present utility model:
The utility model pump as reaction solution transmitting power, can automatic continuous circulation by reaction solution from reaction unit to resin column, return reaction unit, also can visual response situation, stop the operation of pump.In reaction unit, enzyme liquid plays the effect catalyzed and synthesized, along with the carrying out of building-up reactions, enzyme liquid is consumed, under the effect of pump, reaction solution is through resin column, can supplement enzyme liquid, the velocity of flow according to reaction solution regulates, and carrys out the amount that equal control supplements enzyme liquid, save the troublesome operation that artificial process adds enzyme, also avoid the situation because misoperation causes enzyme amount too much or very few.When in reaction solution, target product concentration reaches certain value, the operation of pump can be stopped, opening control valve, collect reaction solution from outlet end, refine for further separating-purifying, obtain finished product.
Accompanying drawing explanation
Fig. 1 is practical schematic diagram.
Embodiment
Below in conjunction with specific embodiment, set forth the utility model further.Should be understood that these embodiments are only not used in restriction scope of the present utility model for illustration of this practicality.
Embodiment 1
As shown in Figure 1, a kind of enzyme reaction automatic device system, comprises reaction unit 1, whipping appts 2, resin column 3, pump 4; Described whipping appts 2 is positioned at described reaction unit 1; Potting resin in described resin column 3, in the present embodiment, the resin of filling in described resin column 3 is immobilized enzyme resin, is full of enzyme liquid in this resin column 3.Outlet is arranged at the bottom of described reaction unit 1, in the present embodiment, this outlet is connected to threeway, and other two ports of this threeway connect one end of outlet end 5 and described pump 4 respectively, the other end of described pump 4 is positioned at the upstream of described resin column 3, and the upstream of described outlet end 5 is provided with control valve 6.
The preparation method of the employing enzyme reaction automatic device system that the utility model provides.
Reaction solution in described reaction unit 1 is extracted into described resin column 3 by described pump 4, upwards fully contact with described mixed with resin from the bottom of this resin column 3, add enzyme liquid in reaction solution, and get back to described reaction unit 1 from the top of described resin column 3, complete a circulation; Described whipping appts 2 Keep agitation reaction solution, reaction solution circulates through described resin column, evenly supplements enzyme liquid.
The utility model with pump 4 as reaction solution transmitting power, can automatic continuous circulation by reaction solution from reaction unit 1 to resin column 3, return reaction unit 1, also can visual response situation, stop the operation of pump.In reaction unit 1, enzyme liquid plays the effect catalyzed and synthesized, along with the carrying out of building-up reactions, enzyme liquid is consumed, under the effect of pump 4, reaction solution is when resin column 3, can supplement enzyme liquid, the velocity of flow according to reaction solution regulates, and carrys out the amount that equal control supplements enzyme liquid, save the troublesome operation that artificial process adds enzyme, also avoid the situation because misoperation causes enzyme amount too much or very few.When in reaction solution, target product concentration reaches certain value, the operation of pump 4 can be stopped, collecting reaction solution from outlet end, refine for further separating-purifying, obtain finished product.
The application of the enzyme reaction automatic device system that the utility model provides: described enzyme reaction automatic device system is applied to the synthesis technique adopting the pharmacy of enzyme reaction, makeup and fine chemistry industry.
Present specification describes some embodiments, but should be understood that those skilled in the art pass through to read the various improvement that this specification sheets can know design and the scope not deviating from this practicality.Therefore, these other embodiments also should be included within the scope of appended claims.
Claims (3)
1. an enzyme reaction automatic device system, is characterized by: comprise reaction unit (1), whipping appts (2), resin column (3), pump (4); Described whipping appts (2) is positioned at described synthetic reaction device (1); Described resin column (3) interior potting resin; Outlet is arranged at the bottom of described reaction unit (1), and described pump (4) is positioned at the upstream of downstream that described reaction unit (1) exports and described resin column (3).
2. enzyme reaction automatic device system according to claim 1, it is characterized in that, the outlet of described reaction unit (1) is connected to threeway, other two ports of this threeway connect one end of outlet end (5) and described pump (4) respectively, and the upstream of described outlet end (5) is provided with control valve (6).
3. enzyme reaction automatic device system according to claim 1, is characterized in that, the resin of filling in described resin column (3) is immobilized enzyme resin, and this resin column is full of enzyme liquid in (3).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520173783.3U CN204509351U (en) | 2015-03-26 | 2015-03-26 | A kind of enzyme reaction automatic device system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520173783.3U CN204509351U (en) | 2015-03-26 | 2015-03-26 | A kind of enzyme reaction automatic device system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204509351U true CN204509351U (en) | 2015-07-29 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520173783.3U Active CN204509351U (en) | 2015-03-26 | 2015-03-26 | A kind of enzyme reaction automatic device system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204509351U (en) |
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2015
- 2015-03-26 CN CN201520173783.3U patent/CN204509351U/en active Active
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |