CN204428900U - A kind of immiscible liquid separating and measuring device - Google Patents
A kind of immiscible liquid separating and measuring device Download PDFInfo
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- CN204428900U CN204428900U CN201520046299.4U CN201520046299U CN204428900U CN 204428900 U CN204428900 U CN 204428900U CN 201520046299 U CN201520046299 U CN 201520046299U CN 204428900 U CN204428900 U CN 204428900U
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Abstract
The utility model discloses a kind of immiscible liquid separating and measuring device, object is that solving current existing apparatus effectively cannot be separated two kinds of solution, and the problem of Accurate Measurement.The utility model can efficient solution never mutually soluble liquids be separated and the problem of cubing.It comprises parts one, S shape blast pipe, rubber tube, only liquid device, and parts one comprise the container, one-level pipe, the diode that are connected successively.The utility model has accurate range section, and separation degree is high, simultaneously can effective measurement volumes, is specially adapted to separation and the stereometry of micro oil water mixed liquid in scientific research.Meanwhile, volume, by selecting suitable scale division value, can accurately be read to 2 significant digits by the utility model, and estimate and to read to decimal point three, the precision greatly improving measurement is high, can meet the needs of scientific research.The utility model is reasonable in design, is skillfully constructed, and breaches the native mode of existing glass apparatus, has broad application prospects.
Description
Technical field
The utility model relates to fluid separation applications fields of measurement, is specially a kind of immiscible liquid separating and measuring device, and it can be that vierics are measured in a kind of micro-water-oil separating.
Background technology
Oil water separator is a kind of device oil and water (or two kinds immiscible liquid) separated.At present, when the miscella of two kinds of non soluble liquids is measured, after needing just both separation, then measure.For the mixture of plants essential oil and water, the separation method of current plants essential oil and water mainly comprises Physical and chemical method.Wherein, Physical utilizes the different of plants essential oil and aqueous fusion point, and under 4 DEG C of conditions, make oil water mixture stratification, plants essential oil solidifies rear removing moisture, the separation of both realizations.Chemical method reaches the object of water-oil separating by some chemical reagent, as: in oil-water mixture, add excessive Na
2sO
4draw the moisture in plants essential oil, then add absolute ether, make plants essential oil be dissolved in ether, naturally volatilize or rotary evaporation finally by absolute ether, realize being separated of plants essential oil and water.But these two kinds of separation methods bring certain difficulty all to the measurement of plants essential oil, can only measure the weight of plants essential oil, and can not measure its volume.At present, the survey tool that simultaneously can be separated also Accurate Measurement trace oil content (as plants essential oil) volume is lacked in laboratory.
For this reason, Chinese patent CN 203400528 U discloses a kind of oil water separator, mainly comprises discharge chamber, oil collect port and layering pond, and when after oil-water mixture layering, when pasta is higher than funnel-form oil collect port, oil can flow out from oil collect port.But the oil in oil-water mixture can not be separated totally by this separator, and also cannot measure the volume of oil after being separated, and collector tubing is longer, the oil of separation is easily bonded at and causes damage on tube wall.Chinese patent CN 203564866 U discloses a kind of oil water separator, and it mainly comprises and holds the container of oil-water mixture and the funnel of tapping, and container lower end connects funnel, and hopper outlet is provided with valve, and container upper end is provided with screen cloth.In this patent, oil-water mixture is layering in a reservoir, opens the valve of funnel lower end, releases the water below oil reservoir and impurity, makes oil-water mixture separately, but and be not suitable for the plants essential oil of trace and being separated of water, and cannot measure and be separated fuel-displaced volume.
Therefore, lack at present and effectively can be separated two kinds of immiscible liquids, and the device of Accurate Measurement.
Utility model content
Goal of the invention of the present utility model is: effectively cannot be separated two kinds of solution for current existing apparatus, and the problem of Accurate Measurement, a kind of immiscible liquid separating and measuring device is provided.The utility model can efficient solution never mutually soluble liquids be separated and the problem of cubing.The utility model has accurate range section, and separation degree is high, effectively can measure volume simultaneously, be specially adapted to separation and the stereometry of micro oil water mixed liquid in scientific research.Meanwhile, volume, by selecting suitable scale division value, can accurately be read to 2 significant digits by the utility model, and estimate and to read to decimal point three, the precision greatly improving measurement is high, can meet the needs of scientific research.The utility model is reasonable in design, is skillfully constructed, and breaches the native mode of existing glass apparatus, has broad application prospects.
To achieve these goals, the utility model adopts following technical scheme:
A kind of immiscible liquid separating and measuring device, comprise parts one, S shape blast pipe, rubber tube, only liquid device, described parts one comprise container, one-level pipe, diode, described container, one-level pipe, diode are fixedly connected sequentially, described one-level pipe, diode are respectively arranged with scale, and described one-level pipe, diode share zero graduation line;
One end of described S shape blast pipe is connected with diode, and the other end of S shape blast pipe is connected with rubber tube, and described only liquid device is arranged on rubber tube;
The caliber of described one-level pipe is greater than the caliber of diode.
Described S shape blast pipe is flexibly connected with adopting between diode.
Described S shape blast pipe is threaded with adopting between diode.
The pipe end of described diode is provided with external screw thread, and described S shape blast pipe is provided with the internal thread matched with diode.
Described only liquid device is liquid stopping clamp.
The sharp mouth glass-tube that described only liquid device comprises bead, is connected with rubber tube, described bead is arranged in rubber tube.
Described S shape blast pipe adopts glass material to be prepared from.
Described S shape blast pipe adopts quartz glass to be prepared from.
The range of described one-level pipe is 1 ~ 50mL, and the scale division value of one-level pipe is 0.1 ~ 0.5mL, and the range of described diode is 0.1 ~ 1mL, and the scale division value of diode is 0.01 ~ 0.05mL.
The range of described one-level pipe is 1mL or 10mL, and the scale division value of one-level pipe is 0.1mL, and the range of diode is 0.1 mL or 1mL, and the scale division value of diode is 0.01mL.
For foregoing problems, the utility model provides a kind of immiscible liquid separating and measuring device.It comprises parts one, S shape blast pipe, rubber tube, only liquid device, and parts one comprise container, one-level pipe, diode, and container, one-level pipe, diode are fixedly connected sequentially integral.One-level pipe, diode are respectively arranged with scale, and one-level pipe, diode share zero graduation line, and the caliber of one-level pipe is greater than the caliber of diode.Adopt this structure, the junction of one-level pipe, diode is 0 graduation mark.The two ends of S shape blast pipe are connected with diode, rubber tube respectively, and only liquid device is arranged on rubber tube.
With one-level pipe for primaries journey section, diode is accurate range section, and accurate range section is arranged on below primaries journey section, and primaries journey section is arranged on below container.For the mixture (it is the one in immiscible liquid) of plants essential oil and water, during utility model works, the mixed liquor of plants essential oil and water is put into parts one, open the only liquid device on rubber tube, discharge one-level pipe, diode, air in S shape blast pipe, treat that water is full of container with lower part, i.e. one-level pipe, diode, S shape blast pipe, after rubber tube, open only liquid device the upper surface of essential oil is equal with a certain scale of primaries journey section, and oil water surface is adjusted in accurate range section, primaries journey section and accurate range section reading are read in conjunction, obtain the volume reading of essential oil.The utility model utilizes the effect of oil content and water objectionable intermingling and gravitational field sedimentation, and natural separation also measures the volume of plants essential oil, effectively solves prior art Problems existing.
With the range of one-level pipe for 1mL, the scale division value of one-level pipe is 0.1mL, the range of diode is 0.1mL, and the scale division value of diode is 0.01mL is example, and namely primaries journey section identifies reading is from top to bottom 1.0,0.9,0.8,0.7,0.6,0.5,0.4,0.3,0.2,0.1,0; It is 0,0.01,0.02,0.03,0.04,0.05,0.06,0.07,0.08,0.09,0.10 that accurate range section identifies reading from top to bottom, and total measurement range is 0.010 ~ 1.100 mL.If the range of one-level pipe is 10mL, the range of diode is 1.0mL, then total measurement range is 0.010 ~ 11mL.
Further, S shape blast pipe is flexibly connected with adopting between diode, is preferably threaded.The pipe end of diode is provided with external screw thread, and S shape blast pipe is provided with the internal thread matched with diode.Air in one-level pipe, diode can be discharged smoothly by S shape blast pipe, and rubber tube is arranged on the lower end of S shape blast pipe, effectively can control speed in container under liquid stream and position by only liquid device, carry out the volume of separating and measuring essential oil.Flow out after accurate range section completely until water, screw out S shape blast pipe, the plants essential oil stayed wherein is flowed out, thus realize the object that plants essential oil is separated with water mixed liquid, the volume of Simultaneously test plants essential oil.
Further, S shape blast pipe adopts glass material to be prepared from.Only liquid device is liquid stopping clamp, effectively can be controlled the flowing of liquid by liquid stopping clamp.Or the only liquid device sharp mouth glass-tube that comprises bead, be connected with rubber tube, bead is arranged in rubber tube, adopts this structure, by the bead in control rubber tube, effectively can control the outflow of liquid.
During utility model works, be first connected to S shape blast pipe lower end by with the rubber tube stopping liquid device, complete the assembly working of instrument.Then in parts one, load warm water, slowly open only liquid device, discharge the air in one-level pipe, diode, S shape blast pipe, treat that water is full of container with lower part.By this step, effectively can discharge the air in one-level pipe, diode, S shape blast pipe, avoid causing error to measurement; Improve the temperature of instrument itself simultaneously, after avoiding essential oil to meet glass cools, be bonded on glass inner wall.Again oil-water mixture is put into parts one, after profit layering, slowly open only liquid device, the upper liquid level of adjustment oil content in primaries journey section scale, simultaneously oil water surface should be in any position in accurate range section, primaries journey section and accurate range section reading are read in conjunction, obtain the volume reading of oil content.When oil water surface moves to accurate range section and S shape blast pipe hickey place, S shape blast pipe of outwarding winding, collects the oil content separated.
Compared with prior art, the utility model can realize effectively being separated of plants essential oil and water, and the plants essential oil being simultaneously bonded at loss on tube wall is few; The accurate measurement of essential oil volume can be realized simultaneously, and by the cooperation of one-level pipe, diode, make reading can be accurate to decimal point second, can estimate and read, to decimal point the 3rd, greatly to improve certainty of measurement; One-level pipe, diode share zero graduation line (i.e. " 0 " point), close and read one-level pipe reading and diode reading, be essential oil volume reading.The utility model is specially adapted to the separation of each several part in micro oil water mixed liquid in scientific research and the mensuration (as steam method extracts the separating and measuring of plants essential oil) of volume, also the separating and measuring of two kinds of non soluble liquids is applicable to, and simple to operation, measure effective.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Fig. 2 is the enlarged diagram after the local of I in Fig. 1 splits.
Fig. 3 is the schematic diagram of the utility model measurement volumes reading.
Mark in figure: 1 is container, and 2 is one-level pipe, and 3 is diode, and 4 is zero graduation line, and 5 is S shape blast pipe, and 6 is rubber tube, liquid device till 7.
Detailed description of the invention
Below in conjunction with accompanying drawing, the utility model is described in detail.
In order to make the purpose of this utility model, technical scheme and advantage clearly understand, below in conjunction with drawings and Examples, the utility model is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the utility model, and be not used in restriction the utility model.
Embodiment 1
As shown in the figure, this measuring appliance comprises parts one, S shape blast pipe, rubber tube, only liquid device, and parts one comprise container, one-level pipe, diode, and container, one-level pipe, diode are connected successively, and one-level pipe, diode are respectively arranged with scale.In the present embodiment, the caliber of one-level pipe is greater than the caliber of diode, and the range of one-level pipe is 1mL, and its scale division value is 0.1mL; The range of diode is 0.1 mL, and its scale division value is 0.01mL, and one-level pipe, diode share zero graduation line.The two ends of S shape blast pipe are connected with diode, rubber tube respectively, and wherein the pipe end of diode is provided with external screw thread, and S shape blast pipe is provided with the internal thread matched with diode.In the present embodiment, only liquid device adopts liquid stopping clamp, and liquid stopping clamp is arranged on rubber tube.
In the present embodiment, one-level pipe is designated as primaries journey section, diode is designated as accurate range section, and accurate range section is arranged on below primaries journey section, and primaries journey section is arranged on below container.As shown in the figure, range of the present utility model is determined by primaries journey section and accurate range section, and namely total range of the present embodiment is 1.100 mL.In this enforcement, also primaries journey section can be designed to 10mL ~ 50mL, accurate range section is designed to 1.0mL ~ 10mL, and total range can be 11.0mL ~ 60mL.
When the device of the present embodiment works, the rubber tube with liquid stopping clamp is connected to the lower end of S shape blast pipe, completes assembly work.Then in device, load warm water, slowly open liquid stopping clamp, discharge the air in primaries journey section, accurate range section, S shape blast pipe, be full of after primaries journey section, accurate range section, S shape blast pipe, rubber tube until water, oil-water mixture put into parts one.After profit layering, slowly open liquid stopping clamp, the upper liquid level of oil content is equal with a certain scale of primaries journey section, and oil water surface is adjusted in accurate range section, close and read primaries journey section and accurate range section reading, obtain the volume reading of oil content.When oil water surface moves to accurate range section and S shape blast pipe hickey place, S shape blast pipe of outwarding winding, collects the oil separated.Give a concrete measurement result in Fig. 3, pin-point reading is 0.52mL, and estimating reading is 0.523mL.
The foregoing is only preferred embodiment of the present utility model; not in order to limit the utility model; all do within spirit of the present utility model and principle any amendment, equivalent to replace and improvement etc., all should be included within protection domain of the present utility model.
Claims (10)
1. an immiscible liquid separating and measuring device, it is characterized in that, comprise parts one, S shape blast pipe, rubber tube, only liquid device, described parts one comprise container, one-level pipe, diode, described container, one-level pipe, diode are fixedly connected sequentially, described one-level pipe, diode are respectively arranged with scale, and described one-level pipe, diode share zero graduation line;
One end of described S shape blast pipe is connected with diode, and the other end of S shape blast pipe is connected with rubber tube, and described only liquid device is arranged on rubber tube;
The caliber of described one-level pipe is greater than the caliber of diode.
2. immiscible liquid separating and measuring device according to claim 1, is characterized in that, described S shape blast pipe is flexibly connected with adopting between diode.
3. immiscible liquid separating and measuring device according to claim 2, is characterized in that, described S shape blast pipe is threaded with adopting between diode.
4. immiscible liquid separating and measuring device according to claim 3, it is characterized in that, the pipe end of described diode is provided with external screw thread, and described S shape blast pipe is provided with the internal thread matched with diode.
5. immiscible liquid separating and measuring device according to claim 1, is characterized in that, described only liquid device is liquid stopping clamp.
6. immiscible liquid separating and measuring device according to claim 1, is characterized in that, the sharp mouth glass-tube that described only liquid device comprises bead, is connected with rubber tube, and described bead is arranged in rubber tube.
7. immiscible liquid separating and measuring device according to claim 1, is characterized in that, described S shape blast pipe adopts glass material to be prepared from.
8. immiscible liquid separating and measuring device according to claim 7, is characterized in that, described S shape blast pipe adopts quartz glass to be prepared from.
9. immiscible liquid separating and measuring device according to any one of claim 1-8, it is characterized in that, the range of described one-level pipe is 1 ~ 50mL, and the scale division value of one-level pipe is 0.1 ~ 0.5mL, the range of described diode is 0.1 ~ 1mL, and the scale division value of diode is 0.01 ~ 0.05mL.
10. immiscible liquid separating and measuring device according to claim 9, it is characterized in that, the range of described one-level pipe is 1mL or 10mL, and the scale division value of one-level pipe is 0.1mL, and the range of diode is 0.1 mL or 1mL, and the scale division value of diode is 0.01mL.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520046299.4U CN204428900U (en) | 2015-01-23 | 2015-01-23 | A kind of immiscible liquid separating and measuring device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520046299.4U CN204428900U (en) | 2015-01-23 | 2015-01-23 | A kind of immiscible liquid separating and measuring device |
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| Publication Number | Publication Date |
|---|---|
| CN204428900U true CN204428900U (en) | 2015-07-01 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520046299.4U Expired - Fee Related CN204428900U (en) | 2015-01-23 | 2015-01-23 | A kind of immiscible liquid separating and measuring device |
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| Country | Link |
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| CN (1) | CN204428900U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109260766A (en) * | 2017-07-18 | 2019-01-25 | 中国石油化工股份有限公司 | A kind of oily-water seperating equipment |
-
2015
- 2015-01-23 CN CN201520046299.4U patent/CN204428900U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109260766A (en) * | 2017-07-18 | 2019-01-25 | 中国石油化工股份有限公司 | A kind of oily-water seperating equipment |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150701 Termination date: 20160123 |
|
| EXPY | Termination of patent right or utility model |